• 청정기술
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• 제14권3호
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• pp.171-175
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• 2008

본 연구에서는 첨가물이 전기화학적 성능에 미치는 효과를 알아보기 위해 실험변수로서 첨가물 $Al^{3+}$를 사용하였다. Zero-strain 삽입 혼합물로 알려진 $Li_{4}Ti_{5]O_{12}$에 $Al^{3+}$가 첨가된 $Li_{3.95}Al_{0.15}Ti_{4.9}O_{12}$를 high energy ball milling (HEBM)을 사용하여 고상반응으로 제조한 후에, $800,\;900,\;1000^{\circ}C$에서 열처리하여 시료를 제조하였다. 합성물질의 구조적 특성과 입자의 표면분석을 하기 위해 XRD (X-ray diffraction)와 SEM (scanning electron microscopy)을 사용하였으며, 이때의 입자의 분포는 대략 $0.2{\sim}0.6\;{\mu}m$ 정도로 측정되었다. 충/방전 실험은 $1.0{\sim}3.0 V$에서 하였으며, 가역용량, 사이클 안정성, 평탄 전압 등을 알아보았다. $Li_{3.95}Al_{0.15}Ti_{4.9}O_{12}$의 충방전 용량은 138 mAh/g이었다.

• 대한전자공학회논문지SD
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• 제47권11호
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• pp.1-5
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• 2010

본 논문에서는 외팔보 배열 구조를 가지는 MEMS 테스트 소켓을 SOI 웨이퍼를 이용하여 개발하였다. 외팔보는 연결부분의 기계적 취약점을 보완하기 위해 모서리가 둥근 형태를 가지고 있다. 측정에 사용 된 BGA IC 패키지는 볼 수 121개, 피치가 $650{\mu}m$, 볼 직경 $300{\mu}m$, 높이 $200{\mu}m$ 을 가지고 있다. 제작된 외팔보는 길이 $350{\mu}m$, 최대 폭 $200{\mu}m$, 최소 폭 $100{\mu}m$, 두께가 $10{\mu}m$인 곡선 형태의 외팔보이다. MEMS 테스트 소켓은 lift-off 기술과 Deep RIE 기술 등의 미세전기기계시스템(MEMS) 기술로 제작되었다. MEMS 테스트 소켓은 간단한 구조와 낮은 제작비, 미세 피치, 높은 핀 수와 빠른 프로토타입을 제작할 수 있다는 장점이 있다. MEMS 테스트의 특성을 평가하기 위해 deflection에 따른 접촉힘과 금속과 팁 사이의 저항과 접촉저항을 측정하였다. 제작된 외팔보는 $90{\mu}m$ deflection에 1.3 gf의 접촉힘을 나타내었다. 신호경로저항은 $17{\Omega}$ 이하였고 접촉저항은 평균 $0.73{\Omega}$ 정도였다. 제작된 테스트 소켓은 향 후 BGA IC 패키지 테스트에 적용 가능 할 것이다.

• Tribology and Lubricants
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• 제1권1호
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• pp.38-45
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• 1985

Ferrography 방법은 유체중 마모입자를 Substrate glass 위에 Van der Waals 힘에 의하여 분산교착 시키므로써 윤활 Systems에서의 기계요소들의 동특성적 마모진행과정및 mechanism의 정성적및 정량적인 분석을 가능케 한다. 정성적 방법으로는 광학현미경으로부터 SEM, X-Ray Emissiom, EDAX등의 분석방법이 적용되고 있으나, 정량적으로는 마모입자의 크기별 분포함수에 따른 Variance, Kurtosis, Skewness와 같은 인자함수의 변이가 마모진행 과정과 진행될 마모형태기구의 예측인자로서 연구되고 있다. 수치적 Model로 마모진행기구를 예측할 경우 third moment의 Skewness 가 Size 및 number분포에 따라 예민하게 반응을 나타내는 결과를 보이고 있다. 이러한 정량분석을 위하여는 실험 Sample에 따라서, 즉 오염도에 따른 Sample희석이 따르는데, 이러한 Sample 희석이 정량적 분포에 미치는 영향에 관한 연구결과는 아직 없다. 따라서 본연구에는 용제희석이 정량적 마모입자 분포에 미치는 영향을 image analyser인 Quantimat 720을 이용하여 검토하였으며 전영역의 희석률에 적용될 수 있는 Standard Calibration function에 따른 수학적 model을 유도하였다.

• 패션비즈니스
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• 제2권2호
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• pp.77-84
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• 1998

As a result of surveying the process for sewing, the problems involving the outlook of sewn apparels were error off the standard dimensions and uneven sizes, which verifies the need for urgent technological guidance and development. On the other hand, the majority of the businesses were operating their sewing machines at the speed of 2,000 rpm or higher. Such a conventional working method may not well reflect the properties of the stretch fabrics, causing poorer quality products. Moreover, most of the businesses were using the ball-point needles which should be replaced with appropriate ones for stretch fabric. The types of feed dog which were used most were Drop feed, Union feed, Confound feed, Differential feed in their oder. Anyway, the automatized dog should urgently replace these inefficient ones for stretch fabric. Meanwhile, the types of presser foot which were used most were Plain foot, Teflon foot, Roller foot, Ring foot in their order, which also necessitates their replacement which Teflon foot. 2. As a result of surveying the process for finishing and inspection, while the causes scores less than 3 points, those due to pressers scored more than 3 points. This results suggests that a technological guidance is needed for the pressing work. Lastly, the causes of defect due to poor outlook attributable to such notions as button or zipper and those due to the uneven sizes scored more than 3 points, which suggests that the entire of needle works should be reformed through scientific research and technological guidance.

• 한국분말재료학회지
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• 제29권5호
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• pp.382-389
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• 2022

A typical trade-off relationship exists between strength and elongation in face-centered cubic metals. Studies have recently been conducted to enhance strength without ductility reduction through surface-treatment-based ultrasonic nanocrystalline surface modification (UNSM), which creates a gradient microstructure in which grains become smaller from the inside to the surface. The transformation-induced plasticity effect in Fe-Mn alloys results in excellent strength and ductility due to their high work-hardening rate. This rate is achieved through strain-induced martensitic transformation when an alloy is plastically deformed. In this study, Fe-6%Mn powders with different sizes were prepared by high-energy ball milling and sintered through spark plasma sintering to produce Fe-6%Mn samples. A gradient microstructure was obtained by stacking the different-sized powders to achieve similar effects as those derived from UNSM. A compressive test was performed to investigate the mechanical properties, including the yielding behavior. The deformed microstructure was observed through electron backscatter diffraction to determine the effects of gradient plastic deformation.

• 대한치과보철학회지
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• 제39권6호
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• pp.599-610
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• 2001

Due to an increasing interest in esthetics and concerns about toxic and allergic reactions to certain alloys, patients and dentists have been looking for metal-free tooth-colored restorations. Recent improvement in technology of new all-ceramic materials and composite materials has broadened the options for esthetic single crown restorations. The aim of this investigation was to study the fracture strength of the metal-free posterior single crowns fabricated using two recently introduced systems, Empress 2 ceramic and Targis-Vectris. Forty premolar-shaped stainless steel dies with the 1mm-wide circumferential shoulder were prepared. Ten cylindrical crowns having a diameter of 8.0mm and total height of 7.5mm were fabricated for each crown system respectively(PFM, Empress staining technique, Empress 2 layering technique, and Targis- Vectris). The crowns were filled with cement and placed on the stainless steel dies with firm finger pressure. The crowns were then stored in distilled water at room temperature for 24 hours before testing. The crowns were tested for fracture strength in an Instron universal testing machine (Instron 6022). With a crosshead speed of 1mm/min the center of the occlusal surface of the crown was loaded using a 4-mm-diameter stainless steel ball until fracture occurred. The fracture surfaces of the crowns were gold coated and examined using scanning electron microscopy(Jeol JSM-840 Joel Ltd., Akishima, Tokyo, Japan). Within the parameters of this study the following conclusions were drawn: 1. The mean fracture strength for PFM crowns was 5829(${\pm}906$)N; for Empress staining technique the fracture strength was 1697(${\pm}604$)N; for Empress 2 Layering technique the fracture strength was 1781N(${\pm}400$)N, and the fracture strength for Targis- Vectris was 3093(${\pm}475$)N. 2. The fracture strength of the PFM crowns was significantly higher than that of the Empress 2 and the Targis-Vectris crowns (P<0.05). 3. The fracture strength of the Targis-Vectris crowns was significantly higher than that of the Empress 2 crowns (P<0.05). 4. No statistical difference was found when Empress staining technique was compared with Empress 2 layering technique. 5. The SEM image of fracture surface of Empress 2 crown showed a very dense microstructure of the lithium disilicate crystals and the SEM image of fracture surface of Targis-Vectris crown showed indentations of Vectris and some fibers tom off from Vectris.

• 전기화학회지
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• 제11권4호
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• pp.268-272
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• 2008

본 연구에서는 $LiFePO_4$의 입자크기를 조절함으로써 우수한 전극특성을 나타낼 수 있도록 최적의 입자크기($50{\sim}100\;nm$)를 가지는 $LiFePO_4$ 양극 활물질을 전기방사법을 이용하여 합성하였다. XRD 분석결과 FeP, $Fe_2P$ 등의 불순물이 존재하지 않는 Pnma의 공간군을 가지는 잘 발달된 사방정 구조의 $LiFePO_4$가 합성됨을 확인하였으며, SEM 분석을 통하여 시료의 입자형태 및 크기를 관찰하였다. $0.1\;mA/cm^2$의 전류밀도와 $2.8{\sim}4.0\;V$의 전위영역에서 충 방전 테스트 수행시 135 mAh/g의 초기 방전용량을 나타내었으며, 50 싸이클 후에도 99.9% 이상의 용량 보존율을 보이는 우수한 싸이클 특성을 나타내었다.

• Journal of Pharmaceutical Investigation
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• 제38권1호
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• pp.31-38
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• 2008

The objective of this work is to study transdermal delivery of levodopa using iontophoresis and evaluate various factors which affect the transdermal transport. Levodopa is unstable in aqueous solution, and, in order to establish a stable condition for levodopa for the duration of experiment, we investigated the stability of levodopa in aqueous solutions of different pHs with/without the addition of dextrose or the application of current. Using stable aqueous solution, we have studied the effect of pH, polarity and penetration enhancer (ethanol) on transdermal flux and compared the results. We also investigated the iontophoretic flux from hydroxypropyl cellulose (HPC) hydrogel. In vitro flux study was performed at $33^{\circ}C$, using side-by-side diffusion cell. Full thickness hairless mouse skin and rat skin were used for this work. Current densities applied were 0.4 or $0.6mA/cm^2$ and current was off after 6 hour application. Stability study showed that levodopa solution with a pH 2.5 or 4.5 maintained the initial concentration of levodopa for 24 hours with the addition of 5% dextrose. However, at pH 9.5, levodopa was unstable and 30 to 40% of levodopa degraded within 24 hours, even with the addition of 5% dextrose. Hydrogel swollen with dextrose added levodopa solution maintained about 97% of the initial concentration of levodopa for 13 days, when stored in $4^{\circ}C$. The application of current did not affect the stability of levodopa in hydrogel. Flux study from levodopa solution with pH 2.5 showed that cathodal delivery of levodopa was higher than passive or anodal delivery. When the pH of the donor solution was 4.5, anodal delivery of levodopa was higher than passive or cathodal delivery. These results seem to indicate that electroosmosis plays more dominant role than electrorepulsion in the flux of levodopa at pH 2.5, and the reverse situation applies for pH 4.5. The passive flux was unexpectedly high for the ionized levodopa. Similar to the results from aqueous solution, cumulative amount of levodopa transported trom HPC hydrogel by cathodal delivery was significantly higher than passive or anodal delivery. The treatment of 70% ethanol cotton ball by scrubbing increased passive, anodal and cathodal flux, with the largest increase for anodal flux. These results indicate that iontophoretic delivery of zwitterion such as levodopa is much complicated than that can be expected from small ionic molecules with single charge. The results also indicate that the balance between electroosmosis and electrorepulsion plays a very important role in the transport through skin.

• 한국운동역학회지
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• 제19권1호
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• pp.149-157
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• 2009

본 연구의 목적은 한국의 대표적인 배드민턴화(A Type)와 외국 배드민턴 브랜드제품(B Type)의 생체역학적인 변인들을 비교함으로서 한국제품의 착화감과 기능을 향상시켜 세계적인 수준의 배드민턴화 개발에 일조하는데 목적을 두었다. 분석변인들로는 동작 간 신발 안에서 발의 상대적인 움직임, 지면반력과 압력분포, 아웃솔의 마찰력등을 분석하였다. 또한 17명의 피험자를 통한 주관적인 착화감과 기능에 관련된 주관적인 실험이 실시되었다. A Type 배드민턴화의 경우 높은 뒤꿈치의 위치와 밋밋한 뒷굽의 형태로 신발 안에서 뒤꿈치를 잘 잡아주지 못하는 것으로 나타났다. 따라서 A Type 배드민턴화가 약 40%이상 발이 신발 안에서의 미끄러짐 현상이 일어났으며 충격력의 형태나 최대 압력분포도 높게 나타났다. Type A 신발의 경우 Type B와 같이 자연스러운 굴곡이 발의 볼쪽에서 일어나지 않고 전족부근에서 일어났다. 요약을 하면, 두 신발 간에 몇몇 차이점들이 발견되었고 A Type 배드민턴화의 기능을 향상하기 위해서 보완가능 요인들이 제시되었다.

• 한국재료학회지
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• 제21권7호
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• pp.384-390
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• 2011

Ti-6Al-4V ELI (Extra Low Interstitial) alloy has been widely used as an alternative to bone due to its excellent biocompatibility. However, it still has many problems, including a high elastic modulus and toxicity. Therefore, nontoxic biomaterials with a low elastic modulus should be developed. However, the fabrication of a uniform coating is challenging. Moreover, the coating layer on Ti and Ti alloy substrates can be peeled off after implantation. To overcome these problems, it is necessary to produce bulk Ti and Ti alloy with hydroxyapatite (HA) composites. In this study, Ti, Nb, and Zr powders, which are biocompatible elements, were milled in a mixing machine (24h) and by planetary mechanical ball milling (1h, 4h, and 6h), respectively. Ti-35%Nb-7%Zr and Ti-35%Nb-7%Zr-10%HA composites were fabricated by spark plasma sintering (SPS) at $1000^{\circ}C$ under 70MPa using mixed and milled powders. The effects of HA addition and milling time on the biocompatibility and physical and mechanical properties of the Ti-35%Nb-7%Zr-(10%HA) alloys have been investigated. $Ti_2O$, CaO, $CaTiO_3$, and $Ti_xP_y$ phases were formed by chemical reaction during sintering. Vickers hardness of the sintered composites increases with increased milling time and by the addition of HA. The biocompatibilty of the HA added Ti-Nb-Zr alloys was improved, but the sintering ability was decreased.