• Title/Summary/Keyword: B-1212

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The Precipitation of Second Phases by Annealing Heat Treatment in the $(Bi,Pb)_2$${Sr_2}{Ca_2}{Cu_3}{O_{10}}$ Superconductor System (BSCCO계 초전도체에서 서냉 열처리에 의한 2차상 석출)

  • 이상희;김철진;유재무
    • Journal of the Korean Ceramic Society
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    • v.37 no.12
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    • pp.1212-1220
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    • 2000
  • Bi-2223 초전도체계에서 석출물을 flux-pinning center로 이용할 수 있는지 가능성을 타진하기 위하여 $Bi_{1.8}$P $b_{0.4}$S $r_{2}$C $a_{2.2}$C $u_3$ $O_{8}$ 조성을 가진 Bi-2223/Ag 선재를 반응온도, 산소분압, 시간 등을 변화시키면서 열처리를 행하였다. 열처리 후 석출물들은 XRD, SEM, TEM, EDS로 분석하였다. Bi-2223 모상내의 (Ca, Sr)$_2$(Pb,Bi) $O_4$, B $i_{0.5}$ P $b_3$S $r_2$C $a_2$Cu $O_{12+}$$\delta$/ (3221)와 같은 2차상들의 크기와 분포는 2223 입자들의 연결성을 파괴하지 않고 열처리 조건에 의해서 조절할 수 있었다. 서냉 열처리가 된 시편은 임계전류밀도( $J_{c}$)값이 증가하였는데, 이는 2223 입자내 나노미터 크기로 형성된 석출물들이 flux-pinning sites로 작용한 것으로 추정된다.다.

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Quickest Spectrum Sensing Approaches for Wideband Cognitive Radio Based On STFT and CS

  • Zhao, Qi;Qiu, Wei;Zhang, Boxue;Wang, Bingqian
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.13 no.3
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    • pp.1199-1212
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    • 2019
  • This paper proposes two wideband spectrum sensing approaches: (i) method A, the cumulative sum (CUSUM) algorithm with short-time Fourier transform, taking advantage of the time-frequency analysis for wideband spectrum. (ii)method B, the quickest spectrum sensing with short-time Fourier transform and compressed sensing, shortening the time of perception and improving the speed of spectrum access or exit. Moreover, method B can take advantage of the sparsity of wideband signals, sampling in the sub-Nyquist rate, and it is more suitable for wideband spectrum sensing. Simulation results show that method A significantly outperforms the single serial CUSUM detection for small SNRs, while method B is substantially better than the block detection based spectrum sensing in small probability of the false alarm.

A Numerical Study of Heat and Mass Transfer Phenomena for Thermal Protection Material (열보호재료의 열 및 물질전달 현상에 관한 수치해석적 연구)

  • Kim, Jung-Hoon;Kwon, Chang-Oh;Seo, Jeong-Il;Bai, Cheol-Ho;Song, Dong-Joo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.23 no.9
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    • pp.1201-1212
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    • 1999
  • A numerical analysis is performed to predict the thermal response and ablation rate for charring or non-charring material which is designed to be used as thermal protection system (TPS). The numerical program composed of in-depth energy balance equation and the aerotherm chemical equilibrium (ACE) program. The ACE program calculates various thermochemical state from ablation products. The developed numerical program is verified by comparing the reported results from literature. The sensitivity tests for input parameters are performed. The thermal behavior of ablating material is mainly affected by density of ablating material, convective heat transfer coefficient and recovery enthalpy of flow field.

Repeated Batch Production of Epothilone B by Immobilized Sorangium cellulosum

  • Park, Sang-Woo;Park, Su-Jeong;Han, Se-Jong;Lee, Jin-Won;Kim, Dong-Shik;Kim, Ji-Heung;Kim, Byung-Woo;Lee, Jee-Won;Sim, Sang-Jun
    • Journal of Microbiology and Biotechnology
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    • v.17 no.7
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    • pp.1208-1212
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    • 2007
  • Production of extracellular epothilone B, one of the potent anticancer agents, by free and immobilized Sorangium cellulosum was studied using the repeated batch culture process. The concentration of alginate used in immobilization was directly related to the mass transfer rate of nutrients, mechanical stability, and the epothilone B production yield. With the optimized 3% (w/v) calcium alginate carrier, a prolonged repeated batch culture was investigated for the 5 repeated batches for 24 days. The maximum productivity of epothilone B obtained from the alginate-immobilized cells was 5.03 mg/l/day, which is 3 times higher than that of free cells (1.68 mg/l/day).

Synthesis of New 2-Thiouracil-5-Sulphonamide Derivatives with Antibacterial and Antifungal Activity

  • Fathalla O. A.;Awad S. M.;Mohamed M. S.
    • Archives of Pharmacal Research
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    • v.28 no.11
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    • pp.1205-1212
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    • 2005
  • 2-Thiouracil-5-sulphonic acid N-(4-acetylphenyl) Amide (1) was reacted with a series of aromatic aldehydes giving chalcones 2 (Claisen-Schemidt reaction), some of these chalcones were reacted with urea and thiourea giving pyrimidine-2-one and pyrimidine-2 thione derivatives respectively of the type 3a,b and 4a,b. In addition many chalcones were reacted with hydroxylamine hydrochloride giving isoxazoline derivatives 5a,b. They could also reacted with phenylhydrazine to give pyrazoline derivatives 5a,b, chalcones also were reacted withethylcyano acetate and/or malononitryl in pyridine giving pyran derivatives 7a,c and 8a,c. In another pathway chalcones were epoxidised by $H_{2}O_{2}$ giving epoxides 9a,c which in turn were reacted with phenylhydrazine giving 4-hydroxypyrazoline derivatives 10a,c. In another reaction chalcones were reacted with ethylcyanoacetate in presence of amm.acetate giving pyridone derivatives 11a,d which could be prepared also in exellent yield from compound 1 by its reaction with certain aromatic aldehydes and ethylcyanoacetate in presence of ammonium acetate. Finally, compound 1 was reacted with semicarbazide giving semicarbazone intermediate 12 which in turn was reacted with thionyl chloride giving thiadiazole derivative 13. The biological effects of some of the new synthesized compounds were also investigated.

Bacillus subtilis as a Tool for Screening Soil Metagenomic Libraries for Antimicrobial Activities

  • Biver, Sophie;Steels, Sebastien;Portetelle, Daniel;Vandenbol, Micheline
    • Journal of Microbiology and Biotechnology
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    • v.23 no.6
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    • pp.850-855
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    • 2013
  • Finding new antimicrobial activities by functional metagenomics has been shown to depend on the heterologous host used to express the foreign DNA. Therefore, efforts are devoted to developing new tools for constructing metagenomic libraries in shuttle vectors replicatable in phylogenetically distinct hosts. Here we evaluated the use of the Escherichia coli-Bacillus subtilis shuttle vector pHT01 to construct a forest-soil metagenomic library. This library was screened in both hosts for antimicrobial activities against four opportunistic bacteria: Proteus vulgaris, Bacillus cereus, Staphylococcus epidermidis, and Micrococcus luteus. A new antibacterial activity against B. cereus was found upon screening in B. subtilis. The new antimicrobial agent, sensitive to proteinase K, was not active when the corresponding DNA fragment was expressed in E. coli. Our results validate the use of pHT01 as a shuttle vector and B. subtilis as a host to isolate new activities by functional metagenomics.

Structural and Microwave Dielectric Properties of the $Ba_5B_4O_{15}$ (B=Ta, Nb) Ceramics with Sintering Temperature (소결온도에 따른 $Ba_5B_4O_{15}$ (B=Ta, Nb)세라믹스의 구조 및 마이크로파 유전특성)

  • Lee, Sung-Jun;Kim, Jae-Sik;Ryu, Ki-Won;Lee, Young-Hie
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.57 no.7
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    • pp.1208-1212
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    • 2008
  • In this study, both structural and microwave dielectric properties of the $Ba_5B_4O_{15}$ (B=Ta, Nb) cation-deficient perovskite ceramics with sintering temperature were investigated. All samples of the $Ba_5B_4O_{15}$ (B=Ta, Nb) ceramics were prepared by the conventional mixed oxide method and sintered at $1325^{\circ}C{\sim}1575^{\circ}C$. The bulk density and dielectric constant of the $Ba_5Ta_4O_{15}$ ceramics were increased continuously with increasing of sintering temperature. The quality factor of the $Ba_5Ta_4O_{15}$ ceramics was increased in as the sintering temperature increases from $1375^{\circ}C{\sim}1475^{\circ}C$ but decreased at the temperatures above $1475^{\circ}C$. And the bulk density, dielectric constant and quality factor of the $Ba_5Nb_4O_{15}$ ceramics were increased in as the sintering temperature increases from $1325^{\circ}CP{\sim}1400^{\circ}C$ but decreased at the temperatures above $1400^{\circ}C$. In the case of the $Ba_5Ta_4O_{15}$ sintered at $1475^{\circ}C$ and $Ba_5Nb_4O_{15}$ ceramics sintered at $1400^{\circ}C$, the dielectric constant, quality factor, and temperature coefficient of the resonant frequency (TCRF) were 25.15, 53,105 GHz, -3.06 $ppm/^{\circ}C$ and 39.55, 28,052 GHz, +5.7 ppm/$^{\circ}C$, respectively.

${\alpha}-Amylase$ production of Bacillus natto IAM 1212 in the wheat bran medium (밀기울배지를 이용한 Bacillus natto ${\alpha}-Amylase$ 생산)

  • 김광;박인호;선우양일
    • KSBB Journal
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    • v.6 no.2
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    • pp.143-146
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    • 1991
  • The liquifying $\alpha-amylase$ production from B. subtilis, A. oryzae and B. natto using wheat and rice bran as low cost culture medium was investigated. Among 3 strains, B. natto showed heights productivity of $\alpha-amylase$ in the outer wheat bran medium. And the optimum culture condition is pH 6.8 and $37^{\circ}C$ for the production of $\alpha-amylase$. The $\alpha-amylase$ activity of the crude enzyme and the purified enzyme are 256 unit/ml and 10,700 unit/ml, respectivitly. The $\alpha-amylase$ from B. natto cultrtured in outer wheat bran medium was purified into nearly a pure state(98.7%). And the molecular weight of the purified $\alpha-amylase$ was 34,000.

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ASIC Design for Speed Sensor less Control of Indution Motor (유도전동기의 센서리스 속도제어 ASIC 설계)

  • Kim, S.J.;Lee, B.C.;Shin, Y.J.;Lee, I.H.;Kwon, Y.A.
    • Proceedings of the KIEE Conference
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    • 2001.07b
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    • pp.1212-1214
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    • 2001
  • In this paper ASIC design technique using VHDL is applied to MRAS based speed sensorless control of induction motor. ASIC for MRAS based speed sensorless control is designed through the description of speed estimator using FSM, stator voltage controller, flux angle detector, coordinate transformation, and inverter switching signal output. Finally the above system has been implemented on the FPGA (VERTEX XCV400HQ240). Simulation and experiment have been performed to verify the performance of the designed ASIC.

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