• Title/Summary/Keyword: Average Grain Diameter

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Fabrication of Injection Molded Fe-50%Ni Sintered Bodies (사출성형된 Fe-50%Ni 소결체의 제조)

  • Kim Ki-Hyun;Yoon Hyeong-Chul;Choi Chul-Jin;Lee Byong-Taek
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.472-476
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    • 2004
  • The Fe-Ni compact bodies were fabricated using Fe-Ni mixed powders with 50 nm in diameter by injection molding process. The relationship between microstructure and material properties was characterized with respect to the volume ratio of powder/binder and sintering temperature with SEM and TEM. In the compact body having the volume percent ratio of 45(Fe-Ni) : 55(binder), which was sintered at $900^{\circ}C$ the values of relative density and hardness were low about 97.7% and 277.1 Hv, respectively. Using the composition of 50(Fe Ni) : 50(binder) and sintered at $900^{\circ}C$, the values of relative density and hardness were 98.5%, 294.4 Hv, respec-tively. The grain size of sintered bodies strongly depended on the sintering temperature. In both samples sintered at $600^{\circ}C$ and $900^{\circ}C$, the average grain sizes were about 150 nm and 500 nm in diameter, respectively.

THE EFFECT OF SUBSTRATE TEMPERATURE ON GRAIN STRUCTURES AND MAGNETIC PROPERTIES OF Pd(Pt/Co/Pt) MODULATED MULTILAYERS

  • Xiao, Ying;Xu, Jun-Hao;Wittborn, Jesper;Yu, Seong-Cho;Rao, K.V.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.716-719
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    • 1995
  • Pd/(Pt/Co/Pt) modulated multilayer films have been deposited on various substrates with Pd/Pt buffer layers. Films grown at different temperatures have very distinct magnetic properties and surface microstructures. Atomic force(AFM) and scanning tunneling (STM) microscopies studies of these films reveal that films deposited at room temperature have small grain structures with an average grain size of about $140\;{\AA}$. However, much larger grains of about $1200\;{\AA}$ in size are observed in the films grown on buffer layers which were deposited at $500^{\circ}C$. These large grains are found to actually consist of smaller grains of about $170{\AA}$ in diameter. SQUID magnetic and Kerr hysteresis loop measurements indicate that multilayer films with large grains exhibit high magnetic coercivities of around 5 kOe. A subgrain growth model is proposed to understand the observed grain structures in the multilayers.

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Effects by Variation of Raw Materials on Physical Properties of Ni-Zn Ferrite (원료 변화에 따른 Ni-Zn Ferrite의 물리적 특성에 미치는 영향)

  • Koh, Jae-Gui
    • Korean Journal of Materials Research
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    • v.16 no.9
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    • pp.578-583
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    • 2006
  • We studied the physical properties of Ni-Zn ferrites by adding different chemicals such as $SO_4$, Cl, and $NO_3$. Specimens were prepared by the coprecipitation method and sintered at temperatures $950^{\circ}C,\;1,150^{\circ}C,\;and\;1,350^{\circ}C$, respectively. X-ray diffractions showed a spinel structure and the optical microscopy revealed grain size of 0.3 to 0.6 ${\mu}m$. The optimum sintering temperature to obtain fine, sintered microstructure depended on the additive : Cl and $NO_3\;at\;950^{\circ}C\;and\;SO_4\;at\;1,150^{\circ}C$. According to particle size analysis, higher magnetic permeability and magnetization value were observed with Cl and $NO_3\;than\;SO_4$. As sintering temperature was raised from $950^{\circ}C$ to $1,350^{\circ}C$, the average grain diameter, initial permeability and the magnetic moment also increased.

X-X: Single-Crystalline Si TFTs Fabricated with ${\mu}-Czochralski$ (grain-filter) process

  • Ishihara, R.;Dijk, B.D.van;Wilt, P.Ch. van der;Metselaar, J.W.;Beenakker, C.I.M.
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.159-162
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    • 2002
  • This paper reviews an advanced excimer-laser crystallization technique enabling precise location-control of the individual grains. With the developed ${\mu}$-Czochralski (grain-filter) process, the large grains having a diameter of 6 ${\mu}m$ can be set precisely at predetermined positions. We will also discuss the performance of the single-crystalline Si TFTs that are formed within the location-controlled Si grains. The field-effect mobility for electrons is 430 $cm^2/Vs$ on average, which is well comparable to that of TFTs made with silicon-on-insulator wafers.

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Grain Size Analysis by Hot-Cooling Cycle Thermal Stress at Y-TZP Ceramics using Full Width at Half Maximum(FWHM) of X-ray Diffraction (X-ray 회절의 반치전폭(FWHM)을 이용한 Y-TZP세라믹스에서 반복 열응력에 의한 입계크기 분석)

  • Choi, Jinsam;Park, Kyu Yeol;Kong, Young-Min
    • Korean Journal of Materials Research
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    • v.29 no.4
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    • pp.264-270
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    • 2019
  • As a case study on aspect ratio behavior, Kaolin, zeolite, $TiO_2$, pozzolan and diatomaceous earth minerals are investigated using wet milling with 0.3 pai media. The grinding process using small media of 0.3 pai is suitable for current work processing applications. Primary particles with average particle size distribution D50, ${\sim}6{\mu}m$ are shifted to submicron size, D50 ${\sim}0.6{\mu}m$, after grinding. Grinding of particles is characterized by various size parameters such as sphericity as geometric shape, equivalent diameter, and average particle size distribution. Herein, we systematically provide an overview of factors affecting the primary particle size reduction. Energy consumption for grinding is determined using classical grinding laws, including Rittinger's and Kick's laws. Submicron size is obtained at maximum frictional shear stress. Alterations in properties of wettability, heat resistance, thermal conductivity, and adhesion increase with increasing particle surface area. In the comparison of the aspect ratio of the submicron powder, the air heat conductivity and the total heat release amount increase 68 % and 2 times, respectively.

Development of a Vacuum Nozzle Seeder for Large Seeds in Cucurbitaceae

  • Kim D. E.;Chang Y. S.;Kim J. K.;Kim H. H.;Lee D. H.
    • Agricultural and Biosystems Engineering
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    • v.5 no.2
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    • pp.55-59
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    • 2004
  • This study aimed to develop a seeder for sowing large seeds such as those of fruit vegetables used as rootstocks in grafting. It investigated how the nozzle diameter and the nozzle's vacuum pressure affected the seeding performance. This study found that a nozzle diameter of 1.5 mm was capable of sowing most of the seed sizes used in this study. The highest seeding rates for 'Chambak', 'Tuktozwa', and 'Hukjong' were $97.6\%$, $98.8\%$, and $97.6\%$, respectively. Lineup status after sowing was good. The working performance was 75.6 sheets/hr. An average seeding rate of 1 grain was $97.8\%$.

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Microstructures and Mechanical Properties of Pressureless and Spark Plasma Sintered ZrO2(3 mol%Y2O3) Bodies

  • Shin, Na-Young;Han, Jae-Kil;Lee, Hae-Hyoung;Lee, Byong-Taek
    • Journal of the Korean Ceramic Society
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    • v.42 no.2 s.273
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    • pp.140-144
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    • 2005
  • The microstructures and mechanical properties of Tetragonal Zirconia Polycrystals (TZP) sintered bodies, which made by pressureless and spark plasma sintering techniques, were investigated using XRD, SEM, and TEM techniques. In the spark plasma sintered samples, the TZP grains were equiaxed type including many sub-grain boundaries regardless of sintering conditions. The biaxial strength of TZP having an average of 80 nm grains in diameter was high in value with 1025 MPa, but fracture toughness showed a low value due to the absence of a fracture toughening mechanism such as transformation toughening. In the Pressureless Sintered (PLSed) samples, the grain size of TZP was strongly dependent on the sintering temperature; i.e., it gradually increased as the sintering temperature increased. The value of fracture toughness increased as the grain size increased by the stress-induced phase transformation and Borne crack deflection.

Effect of Grain Boundary Composition on Microstructure and Mechanical Properties of Silicon Carbide (입계상 조성이 탄화규소의 미세구조와 기계적 특성에 미치는 영향)

  • 김재연;김영욱;이준근
    • Journal of the Korean Ceramic Society
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    • v.35 no.9
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    • pp.911-916
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    • 1998
  • By using {{{{ { { {Y }_{3 }Al }_{5 }O }_{12 } }} (YAG) and SiO2 as sintering additives the effect of the composition of sintering ad-ditives on microstructure and mechanical properties of the hog-pressed and subsequently annealed SiC ma-terials were investigated. Microstructures of sintered and annealed materials were strongly dependent onthe composition of sintering additives. The average diameter and volume fraction of elongated grains in an-nealed materials increased with the SiO2/YAg ratio while the fracture toughness increased with the SiO2/YAg ratio. The average MPa.{{{{ { m}^{1/2 } }} respectively. Typical strength and fracture toughness of an annealed material with SiO2/YAg ra-tionof 0.67 were 371 MPa and 5.6 MPa.{{{{ { m}^{1/2 } }} respectively.

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Growth Characteristics of Castor Bean (Ricinus communis L.) Collections (피마자 수집종의 생육특성)

  • Kim, In-Jae;Nam, Sang-Young;Kim, Min-Ja;Rho, Chang-Woo;Lee, Jung-Gwan;Yun, Tae;Song, Hang-Lin;Kim, Hong-Sig
    • Korean Journal of Plant Resources
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    • v.22 no.1
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    • pp.1-4
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    • 2009
  • This study was carried out to evaluate ecological growth characteristics of forty castor bean collections for biodiesel utilization. The emergence date and it's rate of collections was 15-16 days and 82.5%, respectively. It took 63-68 days from emergence to flowering. Stem length was ranged from 173 to 251 cm with an average 211.8 cm. The average stem diameter was 24.2 cm, and showed the high occurrence as 52.5% at the 20.4-24.9 cm. The node number was widely distributed as 13-22 and the average node number was 18.9. The seed numbers were widely distributed as 7-33ea, and the average liter weight of seed was 502.9 g of which minimum weight was 432.3 g and maximum weight was 572.5 g, and the gap between maximum and minimum was 140.2 g. It showed high difference. The 100 grain weight was distributed as 20.3 g-38.3 g which showed high differences between small grain and large grain collections. The seed numbers per plant were varied as 72 at the minimum and 1,011 at the maximum number, and average seed number was 465.2. The total yields of seed per plant were varied as 20 g-266.2 g, and the average yields were 128.1 g.

Characteristics of Seed-germination and Fruit for Sageretia thea in Jeju Region (제주지역 상동나무의 열매와 종자발아 특성)

  • Song, Sang Churl;Song, Chang Khil;Kim, Ju Sung
    • Korean Journal of Medicinal Crop Science
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    • v.23 no.1
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    • pp.8-12
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    • 2015
  • Characteristic of seed for Sageretia thea fruits collected from the habitat of harvest season in Jeju and their germination ratio in different temperatures were considered. The average weight was 0.2 g, average diameter was 7.2 mm, average length was 6.5 mm, and size distribution range was 5.1 ~ 10.0 mm. The number of seeds per fruit was 1.8, and 1000 grain weight was 7.77 g with diameter of 3.7 mm and thickness of 1.7 mm in size. The fruit maturation was investigated to be from April 27 to June 1, when the best maturation period was about a week, May 11 to May 18. Also, the fruits grown on May 4 to May 11 were seen to have the bigger in transverse size and weight with a tendency of the earlier maturation date has the greater the number of seeds. S. thea seeds pretreated for 24 hours at $50^{\circ}C$ were not germinated, while most of those pretreated for 24 hours at $4^{\circ}C$ were successfully germinated at any degree of temperature (except at a temperature of $10^{\circ}C$). Particularly, the highest germination rate of 55% was made at $15^{\circ}C$, and plumule and radicle were best grown within the temperature range of $25^{\circ}C$.