• Title/Summary/Keyword: Autoclave curing

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A Study on Improving the Non-Combustible Properties of High-Density Fiber Cement Composites (고밀도 섬유 시멘트 복합체 불연특성 개선에 관한 연구)

  • Song, Tae-Hyeob;Jang, Kyong-Pil
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.9 no.4
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    • pp.521-528
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    • 2021
  • The high-density fiber composite manufacturing method by the extrusion molding method has the characteristic that continuous production is possible, and the product is molded through a mold forming a specific cross-section. OPC is used as a defect material, an appropriate amount of SiO2 is supplied for CaO reaction activity, and high density and high strength are expressed through steam and autoclave curing. However, due to the use of organic reinforcing fibers, the flame duration exceeds the regulations during the non-combustible performance test, making it difficult to secure performance. In this study, the product was produced by mixing alkali-resistant organic fiber and fly ash having voids as a binder by replacing the existing polypropylene fiber. appeared to be possible.

Carbonation Behavior of Lightweight Foamed Concrete Using Coal Fly Ash

  • Lee, Jae Hoon;Lee, Ki Gang
    • Journal of the Korean Ceramic Society
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    • v.53 no.3
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    • pp.354-361
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    • 2016
  • The purpose of this study was to prepare lightweight foamed concrete by mixing coal fly ash of circulating fluidized bed combustion(CFBC) with cement, and to develop uses for recycling by analyzing carbonation behavior resulting from a change in conditions for pressurized carbonation. For concrete, CFBC coal fly ash was mixed with Portland cement to the water-binder ratio of 0.5, and aging was applied at room temperature after 3 days of curing at $20^{\circ}C$, RH 60%. For carbonation, temperature was fixed at $60^{\circ}C$ and time at 1 h in the use of autoclave. Pressures were controlled to be $5kgf/cm^2$ and the supercritical condition of $80kgf/cm^2$, and gas compositions were employed as $CO_2$ 100% and $CO_2$ 15%+N2 85%. In the characteristics of produced lightweight concrete, the characteristics of lightweight foamed concrete resulting from carbonation reaction were affirmed through rate of weight change, carbonation depth test, air permeability, and processing analysis for the day 28 specimen. Based on these results, it is concluded that the present approach could provide a viable method for mass production of eco-friendly lightweight foamed concrete from CFBC coal fly ash stabilized by carbonation.

Dynamic Property Evaluation of Four-Harness Satin Woven Glass/epoxy Composites for a Composite Bogie Frame (복합소재 대차프레임용 4매 주자직 유리섬유/에폭시 복합소재의 진동특성평가)

  • Kim, Il Kyeom;Kim, Jung Seok;Seo, Sung Il;Lee, Woo Geun
    • Journal of the Korean Society for Railway
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    • v.16 no.1
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    • pp.1-6
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    • 2013
  • In this study, the natural frequency and damping ratio of a four-harness satin woven glass/epoxy composite material are evaluated by means of modal tests and a finite element analysis. To achieve this goal, glass/epoxy beam specimens with different lengths and thicknesses were manufactured via autoclave curing. In the test, the maximum damping ratio was found to occur at the lowest test frequency. As the test frequency increased, the damping ratio decreased exponentially to a critical value. After that value, the damping ratio increased gradually to the maximum test frequency.

Prediction of Deformation of Carbon-fiber Reinforced Polymer Matrix Composite for Tool Materials and Surface Conditions (성형툴의 상태에 따른 탄소섬유강화 복합재 구조물의 변형 예측)

  • Sung, Su-Hwan;Kim, Wie-Dae
    • Composites Research
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    • v.27 no.6
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    • pp.231-235
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    • 2014
  • Autoclave processing has a good quality of product, but manufacturing cost is expansive. After curing of composite, the unwanted deformation and distortion increase the manufacturing cost by redesign of tool parts. Therefore, manufacturing cost down is a big issue in processing level. For the reduction of tool costs, it is important to investigate the effects of tool materials and tool surface conditions. In this paper, we organized user subroutine in ABAQUS to consider the thermal effects of part and tool, and the results are compared with commercial code, COMPRO. And this paper suggests reference point for the selection of tool materials to reduce manufacturing costs.

The Static Collapse Characteristics of CFRP Single and Double Hat Shaped Section Members according to the Interface Number for Lightweight (경량화용 CFRP 단일 모자형 부재와 CFRP 이중 모자형 부재의 계면수 변화에 따른 정적압궤특성)

  • Hwang, Woo-Chae;Cha, Cheon-Seok;Yang, In-Young
    • Journal of the Korean Society of Safety
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    • v.27 no.6
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    • pp.20-25
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    • 2012
  • Currently, the most important purpose in designing automobile is environment-friendly and safety performance aspect. CFRP(Carbon Fiber Reinforced Plastics) of the advanced composite materials as structure materials for vehicles, has a wide application in lightweight structural materials of air planes, ships and automobiles because of high strength and stiffness. In this study, experimental investigations are carried out for CFRP single and double hat shaped section member in order to study the effect of various stacking condition. They were cured by heating to the appropriate curing temperature($130^{\circ}C$) by means of a heater at the vacuum bag of the autoclave. The stacking conditions were selected to investigate the effect of the interface numbers. The CFRP single and double hat shaped section members which manufactured from unidirectional prepreg sheets were made of 8ply. The static collapse tests performed and the collapse mode and energy absorption capability were analyzed according to interface number.

Expansion behavior of low-strength steel slag mortar during high-temperature catalysis

  • Kuo, Wen-Ten;Shu, Chun-Ya
    • Computers and Concrete
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    • v.16 no.2
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    • pp.261-274
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    • 2015
  • This study established the standard recommended values and expansion fracture threshold values for the content of steel slag in controlled low-strength materials (CLSM) to ensure the appropriate use of steel slag aggregates and the prevention of abnormal expansion. The steel slags used in this study included basic oxygen furnace (BOF) slag and desulfurization slag (DS), which replaced 5-50% of natural river sand by weight in cement mixtures. The steel slag mortars were tested by high-temperature ($100^{\circ}C$) curing for 96 h and autoclave expansion. The results showed that the effects of the steel slag content varied based on the free lime (f-CaO) content. No more than 30% of the natural river sand should be replaced with steel slag to avoid fracture failure. The expansion fracture threshold value was 0.10%, above which there was a risk of potential failure. Based on the scanning electron microscopy (SEM) analysis, the high-temperature catalysis resulted in the immediate extrusion of peripheral hydration products from the calcium hydroxide crystals, leading to a local stress concentration and, eventually, deformation and cracking.

Thermal Deformation of Carbon Fiber Reinforced Composite by Cure Shrinkage (탄소섬유강화 복합재료 성형시 화학수축에 의한 변형연구)

  • Choi, Eun-Seong;Kim, Wie-Dae
    • Composites Research
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    • v.31 no.6
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    • pp.404-411
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    • 2018
  • As the autoclave process progresses in a given cure cycle, residual stress in the composite product is induced by cure shrinkage of the resin. As a result, It generates the thermal deformation such as spring-in and warpage, and the inaccuracy of the final product increases. It is important to predict thermal deformation in aerospace parts which require precise fabrication. The research has been done on predicting and grasping curing process of composite material. In this study, the cure mechanism of composite materials according to the process is predicted through finite element analysis, and the effect of cure shrinkage on thermal deformation generated by the process is analyzed.

A Study on the Estimation of Corrosion Protection Performance of Concrete Containing Ground Granulated Blast-Furnace Slag for Massive Coastal Structures (매시브한 해양구조물 적용을 위한 고로슬래그 혼입 콘크리트의 방청성능 평가에 관한 연구)

  • Yoo, Jae-Kang;Kim, Dong-Suk;Park, Sang-Joon;Won, Chul;Lee, Sang-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2002.11a
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    • pp.87-91
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    • 2002
  • This paper investigates the corrosion inhibition and the reduction of hydration heat properties of Ground Granulated Blast-Furnace Slag (GGBFS) added concrete. Since the massive civil structure is vulnerable to the thermal crack by hydration. adiabatic temperature rising tests were performed for water-binder ratios from 43.2% to 47.3%, while replacing 15% to 50% of cement with GGBFS of equal weight. Then, the corrosion protection performance was evaluated using cylindrical specimens embedded with steel reinforcement according to the combination of 3 W/B ratios and 2 levels of chloride ion quantity. The corrosion area of the embedded steel ban was determined using the high pressure steam curing method specified in KS F 2561. The test results showed that the replacement of GGBFS was effective in reducing the hydration heat. The corrosion area of the embedded steel ban decreased as the replacement of GGBFS increased. However, the corrosion area of the steel bar was proportional to the autoclave cycle and the chloride ion quantity. Among the tested specimens, compressive strength, reduction of hydration heat, and corrosion inhibition performance were excellent when 50% of cement was replaced with GGBFS of equal weight.

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The Synthesis and Mechanical Property of Calcium Silicate Hydrates Using the Amorphous Silicates (비정질 규산원료를 이용한 칼슘실리케이트 수화물 합성과 역학적 특성)

  • 엄태선;최연묵;최상흘
    • Journal of the Korean Ceramic Society
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    • v.34 no.1
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    • pp.45-55
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    • 1997
  • Various kinds of amorphous silicates were used as raw materials to synthesize building materials based on calcium silicate hydrates. Relationships between the reactivities of silicates and castabilities of the building materials were investigated. In addition, effects of the reactivities of silicates on the mechanical properties of casted specimens were studied by analyzing microstructures and hydrates produced. As the reactivity of silicate increase, the press castability increases and the crystal size of hydrate and pore size also increase. For the mechanical properties, the flexural strength increases with decreasing crystal size and densifing microstructure. The compressive strength is greatly dependent on the den-sification of microstructure rather than crystal size of hydrate. Based on the results, diatomous ma-terials are desirable due to high reactivity and formation of densified microstructure. Slag and fly ash may be partially used as raw materials with amorphous silicates to manufacture building materials based on calcium silicate hydrates.

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Synthesis of Iodine Substituted Polycarbosilane by High Temperature and Pressure Reaction Process and Properties Characterization (고온, 고압에서의 요오드 치환 Polycarbosilane의 합성 및 특성)

  • Byen, Ji Cheol;Sharbidre, Rakesh Sadanand;Kim, Yoon Ho;Park, Seung Min;Ko, Myeong Seok;Min, Hyo Jin;Lee, Na young;Ryu, Jae-Kyung;Kim, Taik-Nam
    • Korean Journal of Materials Research
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    • v.30 no.9
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    • pp.489-494
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    • 2020
  • SiC is a material with excellent strength, heat resistance, and corrosion resistance. It is generally used as a material for SiC invertors, semiconductor susceptors, edge rings, MOCVD susceptors, and mechanical bearings. Recently, SiC single crystals for LED are expected to be a new market application. In addition, SiC is also used as a heating element applied directly to electrical energy. Research in this study has focused on the manufacture of heating elements that can raise the temperature in a short time by irradiating SiC-I2 with microwaves with polarization difference, instead of applying electric energy directly to increase the convenience and efficiency. In this experiment, Polydimethylsilane (PDMS) with 1,2 wt% of iodine is synthesized under high temperature and pressure using an autoclave. The synthesized Polycarbosilane (PCS) is heat treated in an argon gas atmosphere after curing process. The experimental results obtain resonance peaks using FT-IR and UV-Visible, and the crystal structure is measured by XRD. Also, the heat-generating characteristics are determined in the frequency band of 2.45 GHz after heat treatment in an air atmosphere furnace.