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COMPARATIVE STUDIES OF THE ADHESIVE QUALITIES OF POLYCARBOXYLATE CEMENTS (카복실레이트계 시멘트의 접착력에 관한 비교 연구)

  • Lee, Han-Moo
    • The Journal of Korean Academy of Prosthodontics
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    • v.17 no.1
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    • pp.23-34
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    • 1979
  • In this study, the adhesive strength of three commercial polycarboxylate cements to ten types of dental casting alloys, such as gold, palladium, silver, indium, copper, nickel, chromium, and human enamel and dentine were measured and compared with that of a conventional zinc phosphate cement. The $8.0mm{\times}3.0mm$ cylindrical alloy specimens were made by casting. The enamel specimens were prepared from the labial surface of human upper incisor, and the dentine specimens were prepared from the occulusal surface of the human molar respectively. Sound extracted human teeth, which had been kept in a fresh condition since, extraction, were mounted in a wax box with a cold-curing acrylic resin to expose the flattened area. The mounted teeth were then placed in a Specimen Cutter (Technicut) and were cut down under a water spray, and then the flat area on the all specimens were ground by hand with 400 and 600 grit wet silicone carbide paper. Two such specimens were then cemented together face-to-face with freshly mixed cement, and moderate finger pressure was applied to squeeze the cement to a thin and uniform film. All cemented specimens were then kept in a thermostatic humidor cabinet regulated at $23{\pm}2^{\circ}C.$ and more than 95 per cent relative humidity and tested after 24 hours and 1 week. Link chain was attached to each alloy specimen to reduce the rigidity of the jig assembly, and then all the specimens were mounted in the grips of the Instron Universal Testing Machine, and a tensile load was delivered to the adhering surface at a cross head speed of 0.20 mm/min. The loads to which the specimens were subjected were recorded on a chart moving at 0.50 mm/min. The adhesive strength was determined by measuring the load when the specimen separated from the cement block and by dividing the load by the area. The test was performed in a room at $23{\pm}2^{\circ}C.$ and $50{\pm}10$ per cent relative humidity. A minimum of five specimens were tested each material and those which deviated more than 15 per cent from the mean were discarded and new specimens prepared. From the experiments, the following results were obtained. 1) It was found that the adhesive strength of the polycarboxylate cement to all alloys tested was considerably greater than that of the zinc phosphate cement. 2) The adhesive strength of the polycarboxylate cements was superior to the non precious alloys, such as the copper, indium, nickel and chromium alloys, but it was inferior to the precious gold, silver and palladium alloys. 3) Surface treatment of the alloy was found to be an important factor in achieving adhesion. It appears that a polycarboxylate cement will adhere better to a smooth surface than to a rough one. This contrasts with zinc phosphate cements, where a rough helps mechanical interlocking. 4) The adhesion of the polycarboxylate cement with enamel was found superior to its adhesion with dentine.

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A study on the application of waste concrete powder as a material for construction (건설용 재료로써 폐콘크리트 미분말의 활용성 연구)

  • Kim, Yong-Jic;Choi, Yun-Wang;Kim, Sang-Chel;Kim, Young-Jin
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.4
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    • pp.88-94
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    • 2012
  • This study is conducted to utilize waste concrete powder made as a by-product manufacturing high quality recycled aggregate. The blaine fineness of the used waste concrete powder was 928 and $1,360cm^2/g$. As the main characteristic of waste concrete powder, it showed an angular type similar to cement, but hydrated products were attached on the surface of particles. In addition, the size of the particles of waste concrete powder was larger than OPC and in terms of chemical components it had higher $SiO_2$ contents. The viscosity of the paste that mixed waste concrete power decreased by 62% at the most, compared to the paste that only used OPC, and the final set time was delayed about two hours. As composition rates of waste concrete powder increased, the flow value decreased by 30% at the most according to the comparison with mortar that only used OPC, and sorptivity coefficients increased by 70%. The compressive strength of mortar decreased by 73% at the most as composition rates of waste concrete powder increased. According to the test results, it is desirable to use waste concrete powder by combining OPC appropriately(below 15%).

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A COMPARATIVE STUDY ON THE PROPERTIES OF FILLER-ADDED METHACRYLATE POLYMERS (필러를 배합한 메타크릴레이트 중합체의 물성에 관한 비교 연구)

  • Park Dong-Won;Choi Boo-Byong;Kwon Kung-Rock
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.5
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    • pp.606-616
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    • 2003
  • Purpose : The purpose of this study was to research the properties of some chemically cured methacrylate polymers such as MMA, HEMA, TEG-DMA, bis-GMA, GMA. Material and Method : 5 kinds of methacrylates were selected and added 2% tertiary amine and benzoyl peroxide to make a chemically curable polymer 25 micron crushed silicas which are treated with silane were selected as filler, they were added into methacrylate monomer until the consistency did not changed by the load of 500gram. All of the experimental resins were 5 kinds, and a serial test was done with 3 kinds of items including the filler contents, the tensile strength, and the bond strength. The number of specimen were 10 for each group. Filler contents were obtained by reducing the specimens to ashes at $600^{\circ}C$ for 1 hour. The specimens with the dimension of 6mm in diameter and 3mm thick were immersed in $37{\pm}1^{\circ}C$ distilled water for 24 hours before test, and tensile strength were measured with cross-head speed 1mm/min. Shear bond strength were mea sured on the specimens attached to bovine enamel etched with 37% phosphoric acid for 1 minute. Results : 1. Maximum filler incorporation was the highest as 75.5% on MMA, and the least as 53.4% on bis- GMA(p<0.0001). 2. The tensile stregth were MMA 141.3, GMA 154.3, TEG-DMA 157.4, bis-GMA 161.4 MPa, and HEMA showed the highest value, 226.9MPa(p = 0.0004). 3. The bond strength were GMA 10.1, TEG-DMA 11.7, HEMA 12.2, bis-GMA 13.3 MPa, and MMA showed the highest value, 15.3MPa, however statistical significances were not (p =0.3838), 4. TEG-DMA and HEMA were not different on the aspect of maximum filler contents and shear bond strength(p>0.05). Conclusion : HEMA can be used as an another diluent substituting TEG-DMA with the increased strength and with the constant bond strength and the constant filler contents.

Design of GPS Receiving Antenna Installed in a Missile's Warhead (미사일 탑재형 GPS 안테나 설계)

  • Lee Jong-Min;Woo Jong-Myung
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.17 no.9 s.112
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    • pp.900-912
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    • 2006
  • A GPS receiving antenna installed in the missile's warhead is designed and fabricated at a center frequency 1.575 GHz. The circular shaped antenna is installed in the middle of the warhead where the antenna's patch and the ground plane are connected with a hollow cylindrical shaped short pin. Using the dual feeding and phase difference method, an omni-directional radiation pattern which direction is normal to the missile's axis(H-plane) is obtained. The optimized diameters of the circular patch and the cylindrical ring typed shorting pin of the GPS receiving antenna which use the FR4.material(dielectric constant $\varepsilon_r=4.6$) are 59.5 mm and 14 mm, respectively. The cylindrical body with diameter 100 mm and height 500 mm is attached to the lower part of the warhead in order to complete the missile figure. The radiation patterns are measured by changing the angle and phase between the dual feeding points. When the phase difference of dual feeding is $100^{\circ}$ and the angle between the dual feeding points is $100^{\circ}$, the nearly omni-directional radiation pattern in the H-plane is obtained. In this case, the antenna gain is -5.55 dBd and the relative level difference between the maximum and the minimum radiation intensity is 3.98 dB.

Design of a Broadband Printing RFID Tag Antenna with Low Performance Degradation Due to Nearby Dielectric Material (근접 유전체에 의한 성능 열화가 적은 광대역 프린팅 태그 안테나 설계)

  • Ji, Sung-Hwan;Han, Won-Keun;Park, Ik-Mo;Choo, Ho-Sung
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.20 no.8
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    • pp.694-700
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    • 2009
  • In this paper, we propose a RFID tag antenna with low performance degradation due to nearby dielectric materials. The proposed antenna is designed to be appropriate for ink printing fabrication. The antenna is designed to operate in UHF band of $860{\sim}960$ MHz. The antenna uses a T-matching network in the middle of the main body and two parasitic patches in vicinity for complex conjugate matching with a commercial tag chip. In addition, the two parasitic patches induce currents at different dielectric constants of nearby dielectric materials. This can minimize the performance degradation due to nearby dielectric materials. The measured results show the half power matching bandwidth from 844 MHT to 1,268 MHz. It exhibits the reading distance of about 3.5 m in free space when the tag antenna is used with the commercial reader antenna (transmitting power of 20 dBm and the reader antenna gain of 6 dBi). When the tag is attached on dielectric materials of wood and FR4, the resulting reading distances are 2.61 m and 2.51 m, respectively.

Morphological Changes Associated with the Antibacterial Action of Silver Ions against Bovine Mastitis Pathogens (은 이온의 항균효과에 대한 소 유방염 원인균의 형태학적 변화)

  • Kang, Seog-Jin;Seol, Jae-Won;Hur, Tai-Young;Jung, Young-Hun;Choe, Chang-Yong;Park, Sang-Youel
    • Journal of Veterinary Clinics
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    • v.28 no.6
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    • pp.576-580
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    • 2011
  • Silver has potent antibacterial activity against a variety of bacteria while maintaining low toxicity in mammalian cells. This study was conducted to investigate the possible mechanism underlying the bactericidal effects of silver ions against bovine mastitis pathogens using electron microscopy. We used two different bacterial strains, Escherichia coli and Staphylococcus aureus, which are primarily responsible for the majority of bovine mastitis cases. Interaction between the bacteria and silver ions (50 ${\mu}g/mL$, 2 hours) were studied using energy-filtering transmission electron microscopy (EFTEM). EFTEM images showed that E. coli and S. aureus cells treated with the silver ions had distorted plasma membranes, silver ions attached to the outer membranes, scattered electron-light material, and leakage of cell contents from disrupted cell membranes.

Skeletal Muscle Ventricle Mechanics (골격근 심실의 역학)

  • 오중환
    • Journal of Chest Surgery
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    • v.32 no.5
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    • pp.428-432
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    • 1999
  • Background: It has been shown that low-grade electrical stimulus can transform fatigue resistant muscles which then can be used to protect the heart. The bulky and cumbersome power sources of the artificial heart or implantable ventricular assist devices are still in need of solution; however, on the other hand, the implantable ventricular assist devices using the resistant muscles as the power source have the advantages of using its own muscle contractions. The purpose of this study was to determine the possibility of a clinical application of the skeletal muscle ventricle. Material and Method: Latissimus dorsi muscles (LDM) of 8 canines were used for skeletal muscle ventricle. A latex chamber was wrapped one and a half times with LDM. The chamber was attached to a pressure transducer via Tygon tube. An electrode stimulator was placed around the thoracodorsal nerve and LDM was stimulated in cyclic bursts of 0.31 sec on time and 6.0 sec off time using 3.0 volt Itrel stimulator. The preload volume was added to the system in 25cc increments. Ejection volumes, pressures, and peak power outputs were measured. Result: Ejection volume was 76.3cc with 0cc of preload. Ejection volumes were less than 70ml with increments of preload over 75cc Pressures were more than 107 mmHg when the preloads were less than 75cc and less than 100 mmHg when the preloads were more than 100cc. Peak power output of 16.6 W/kg was observed at 50cc preload. Conclusion: Depending on the changes of preload, the volumes ejected from skeletal muscle ventricle and pressures from the skeletal muscle contraction surpassed those of the normal heart. These data suggest that there are clinical applications for skeletal muscle ventricular assist system.

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A Study on external and internal morphology and pattern analysis in 4 kinds of Mok-Hyaeng Radix (4종류 목향류(木香類)의 외부(外部) 및 내부형태(內部形態)와 이화학패턴연구)

  • Kim, Hong-Jun;Kang, Kyoung-Sik;Choi, Go-Ya;Kim, Ho-Kyung;Jeong, Seung-Il;Ju, Young-Sung
    • Korean Journal of Oriental Medicine
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    • v.12 no.3 s.18
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    • pp.117-130
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    • 2006
  • The purpose of this study was to introduce the differential standard of Mok-Hyaeng Radix species. We established the classificatory standard according to the external and internal morphology and the pattern in 4 kinds of Mok-Hyaeng Radix. The results follow: 1. On the external morphology, Radix of Vladimiria souliei had a sticky material in the head of roots and it was yellowish white in the cut surface. It attached to teeth during chewing. Radix of Aucklandia lappa (=Saussurea lappa) was dark grayish brown and was grayish brown in the cut surface. It had special odor and was not attache to teeth chewing it. On the other hand, Radix of Inula helenium was dark brown. In the cut surface, cortical layer was different from wood layer. Radix of Aristolochia contorta was yellowish brown. In the cut surface, it was not smooth and cortical layer was different from wood layer. 2. On the internal morphology, Radix of Vladimiria souliei had many fascicular fibers and scattered large oil chambers in the bast ray, xylem ray, and parenchyma. On Radix of Aucklandia lappa (=Saussurea lappa), it was difficult to find out the trace when the cork layer was exfoliated. The cambium formed circle and the large oil chambers were scattered in the phloem and xylem. On the other hand, external cortical layer of Radix of Inula helenium was detached and cambium was formed to indistinct circle and large oil chambers were scattered in the phloem and xylem. On Radix of Arustolochia contorta, the large oil chambers were scattered in the surface later, bast part was relatively broad and cambium formed circle. 3. On the TLC pattern, Radix of Aristolochia contorta, Inula helenium, Aucklandia lappa, and Vladimiria souliei were chromogenic to violet and purple according to sulfuric acid colour pattern, especially faint on Aristolochia contorta. 4. On the pattern analysis of HPLC, we compared the content and the pattern of constunolide and dehydrocostus lactone, Radix of Aucklandia lappa was similar to Radix of Vladimiria souliei and Radix of Aristolochia contorta was similar to Radix of Inula helenium. On the total HPLC component pattern, constunolide and dehydrocostus lactone were similar in all four types, but it showed the Rf 5-6 peak was only in Radix of Aristolochia contorta, not in Radix of Inula helenium, Aucklandia lappa, and Vladimiria souliei. It is considered the results of this study will be furnished the basis to succeeding studies and it is needed to extensive comparative study for the same genus-degree of relatedness.

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Delamination Detection of Retrofitted Concrete Using Horn Antenna (Horn Antenna를 이용한 콘크리트 보강재의 박리탐사 실험)

  • Rhim, Hong-Chul;Cho, Young-Sik
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.409-416
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    • 2007
  • In accordance with the increased usage of reinforcing materials such as carbon fibers and glass fibers, delamination detection between concrete and the reinforcing material is needed as such delaminations may be a major cause for strength reduction or failure of a structure. In this work, 15 GHz center frequency with 10 GHz band width horn antenna was used to detect delamination between concrete and carbon fibers or glass fibers. The specimens measured $600\;(length)\;{\times}\;600\;(width)\;{\times}\;100\;(thickness)\;mm$, and glass fibers and carbon fibers with a thickness of 1.5 mm were attached on the specimens' surfaces using epoxy. In addition, artificial delaminations of size $50\;(length)\;{\times}\;50\;(width)\;mm$ were placed in the middle of the specimen with thickness of 2, 4, 6 mm respectively together with a 2 mm delamination projecting upwards from the surface of the concrete. Therefore a total of 8 specimens were used, 4 specimens for glass fiber reinforced concrete and 4 for carbon fiber reinforced concrete, containing delaminations as described above. The experiment results were derived by using the difference of area under the curved graph. According to experimental results artifical delaminations were identified in both fiber reinforced and carbon reinforced specimens and these results could contribute to further development of delamination detection technology.

Microflora of Manufacturing Process and Final Products of Saengshik (시판생식의 제조공정 및 최종제품의 미생물분포)

  • Chang, Tae-Eun;Moon, Sung-Yang;Lee, Kun-Wook;Park, Jang-Mi;Han, Jeong-Su;Song, Ok-Ja;Shin, Il-Shik
    • Korean Journal of Food Science and Technology
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    • v.36 no.3
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    • pp.501-506
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    • 2004
  • Microflora and contamination process of Saengshik products were investigated to ensure microbial safety of Saengshik. Food-borne pathogenic bacteria, such as Staphylococcus aureus, Bacillus cereus, and Clostridium perfringens detected mainly from grains were not removed by washing with tap water and freeze-drying. Contaminations of food-borne pathogenic bacteria occurred through raw material powder processed at other factories and during actual product manufacturing process, because detection rates of final products were higher than those of raw materials. Concentration of food-borne pathogenic bacteria increased with advancing of process after first pulverization. Dusts of powder and powder attached to machine were good media for air-borne microorganisms and caused to increase of food-borne pathogenic bacteria during process. Improvement of manufacturing process and sanitary control of machines arc necessary to ensure microbial safety of Saengshik.