• Title/Summary/Keyword: Atomic emission

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Data-Driven Modelling of Damage Prediction of Granite Using Acoustic Emission Parameters in Nuclear Waste Repository

  • Lee, Hang-Lo;Kim, Jin-Seop;Hong, Chang-Ho;Jeong, Ho-Young;Cho, Dong-Keun
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.19 no.1
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    • pp.75-85
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    • 2021
  • Evaluating the quantitative damage to rocks through acoustic emission (AE) has become a research focus. Most studies mainly used one or two AE parameters to evaluate the degree of damage, but several AE parameters have been rarely used. In this study, several data-driven models were employed to reflect the combined features of AE parameters. Through uniaxial compression tests, we obtained mechanical and AE-signal data for five granite specimens. The maximum amplitude, hits, counts, rise time, absolute energy, and initiation frequency expressed as the cumulative value were selected as input parameters. The result showed that gradient boosting (GB) was the best model among the support vector regression methods. When GB was applied to the testing data, the root-mean-square error and R between the predicted and actual values were 0.96 and 0.077, respectively. A parameter analysis was performed to capture the parameter significance. The result showed that cumulative absolute energy was the main parameter for damage prediction. Thus, AE has practical applicability in predicting rock damage without conducting mechanical tests. Based on the results, this study will be useful for monitoring the near-field rock mass of nuclear waste repository.

Predicting Damage in a Concrete Structure Using Acoustic Emission and Electrical Resistivity for a Low and Intermediate Level Nuclear Waste Repository

  • Hong, Chang-Ho;Kim, Jin-Seop;Lee, Hang-Lo;Cho, Dong-Keun
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.19 no.2
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    • pp.197-204
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    • 2021
  • In this study, the well-known non-destructive acoustic emission (AE) and electrical resistivity methods were employed to predict quantitative damage in the silo structure of the Wolsong Low and Intermediate Level Radioactive Waste Disposal Center (WLDC), Gyeongju, South Korea. Brazilian tensile test was conducted with a fully saturated specimen with a composition identical to that of the WLDC silo concrete. Bi-axial strain gauges, AE sensors, and electrodes were attached to the surface of the specimen to monitor changes. Both the AE hit and electrical resistance values helped in the anticipation of imminent specimen failure, which was further confirmed using a strain gauge. The quantitative damage (or damage variable) was defined according to the AE hits and electrical resistance and analyzed with stress ratio variations. Approximately 75% of the damage occurred when the stress ratio exceeded 0.5. Quantitative damage from AE hits and electrical resistance showed a good correlation (R = 0.988, RMSE = 0.044). This implies that AE and electrical resistivity can be complementarily used for damage assessment of the structure. In future, damage to dry and heated specimens will be examined using AE hits and electrical resistance, and the results will be compared with those from this study.

Comparison of Different Techniques for Measurement of Cold Work in Mild Steel

  • Badgujar, B.P.;Jha, S.K.;Goswami, G.L.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.23 no.6
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    • pp.616-621
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    • 2003
  • There are various Non-Destructive Evaluation (NDE) techniques used for measurement of residual stresses in material, such as magnetic methods, X-ray diffraction, Ultrasonic velocity measurement etc. The capabilities, applications and limitations of these techniques for evaluation of cold work/plastic deformation were studied and compared. Mild steel plates were subjected to different degree of cold deformation and were analyzed by Magneto-mechanical Acoustic Emission (MAE), Barkhausen Noise (BN) and magnetic properties (hysteresis loop parameters analysis). Further, these specimens were analyzed by X-ray diffraction and ultrasonic velocity measurements. The microhardness measurement and microstructure studies of these cold worked plates were also carried out. The results of all these studies and comparison of different techniques are discussed in this paper.

Preconcentration of Cd by Continuous Hydroxide Precipitation-Dissolution in Atomic Emission Spectrometry

  • 연평흠;허걸;박용남
    • Bulletin of the Korean Chemical Society
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    • v.19 no.7
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    • pp.766-770
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    • 1998
  • On-line preconcentration by direct precipitation with hydroxide has been developed and applied for the analysis of Cd in Inductively Coupled Plasma Atomic Emission Spectrometry. Cadmium is continuously precipitated with hydroxide and dissolved by nitric acid in on-line mode. Currently, the enrichment factor is more than 90 times for 20.0 mL of sample and could be further increased very easily. For a large sample throughput, 1.0 mL of sample loop is used and the enrichment factor is 4.5 with the sampling speed of 15/hr. The method has been applied to the analysis of NIST reference sample and has yielded good results with the certified value.

Comparison of analytical methods for quantifying total chromium in soil using Atomic Absorption Spectrometer (AAS) and Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) (토양 시료 중 Atomic Absorption Spectrometry (AAS) 및 Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES)를 이용한 총 크롬 분석방법 비교)

  • Lee, Hong-gil;Kim, Ji-in;Byun, Yoonjoo;Kim, Hyunkoo;Yoon, Jeong Ki
    • Journal of Soil and Groundwater Environment
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    • v.22 no.6
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    • pp.22-28
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    • 2017
  • The accuracy of analytical results in response to the use of different additives ($NH_4Cl$, KCl, $LaCl_3$) and oxidant gases was evaluated and compared by using Atomic Absorption Spectrometry (AAS). Identification of spectroscopic interferences and possible improvements in Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) analysis were also discussed. The average accuracies of total chromium using Certified Reference Materials (CRMs) were found to be 72.1~94.2% in air/acetylene flame condition by AAS, and they were improved to 100.5~110.5% when the oxidants was changed to nitrous oxide rather than adding the additives. The field samples showed similar trends to CRMs, but chromium concentrations were highly variable depending on analytical conditions. The average accuracies using CRMs were estimated to be 89.3~166.1% by ICP-AES, and improved to below 121.7% after eliminating iron interference. Field samples with low chromium and high iron concentration were measured to be > 30% lower in total chromium concentrations by ICP-AES than AAS in nitrous oxide/acetylene flame. Total chromium concentrations in soil could be analyzed with better accuracy under nitrous oxide/acetylene flame by AAS because it was more effective to increase the temperature of the flame than to eliminate the chemical interference for maximizing atomization of chromium. When using ICP-AES, interference substances, total chromium levels, and analytical conditions should be also considered.

Characterization and Preparation of the Hydrogel has Excellent Release Effect of the Active Ingredients Using a Radiation Cross-linking Technology (방사선 가교 기술을 이용한 유효성분 방출력이 우수한 하이드로겔 제조 및 특성 분석)

  • Hwang, Seung-Hyun;Ahn, Sung-Jun;Park, Jong-Seok;Jeong, Sung In;Gwon, Hui-Jeong;Lee, Dong Yun;Lim, Youn-Mook
    • Journal of Radiation Industry
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    • v.9 no.4
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    • pp.199-207
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    • 2015
  • Typical radiation cross-linked hydrogels has the characteristic that high water content, but low emission efficiency of active ingredients. Therefore, the hydrogel was prepared by the addition to collagen, which is closely related to the formation of skin wrinkles in biocompatibility and highly water-soluble carboxymethyl cellulose sodium salt (CMC) in order to preparation of hydrogels has excellent emission efficiency of active ingredients. Hydrogels were prepared by dissolving CMC and collagen each of 0.5%, 10% concentration in deionized water. Then, prepared hydrogels are performed by gamma-radiation at 1, 3, 5 kGy irradiation dose. The results showed that the gel fraction of after irradiated 3 kGy hydrogel was higher than before irradiated gelation as long as the 55.3%. The swelling rate of irradiated 3 kGy hydrogel was lower than the non-irradiated sample. The compressive strength of 3 kGy irradiated hydrogel was the highest. The visco-elastic did not show any significant differences, even after irradiation. The CMC hydrogel in this study suggested a potential use as a material for the mask pack for improved emission efficiency of the active ingredient and anti-wrinkles.

Dynamics of an atomic wave packet in a standing wave quantized field

  • Tak, Jo-Yeong;Won, An-Gyeong
    • Proceedings of the Optical Society of Korea Conference
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    • 2001.02a
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    • pp.252-253
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    • 2001
  • The purpose of this work is to investigate the dynamics of an atomic wave packet whose center-of-mass motion is quantized in a resonant standing wave cavity field. The mechanical aspect of the matter-field interaction has been extensively studied In the theme of atomic beam deflection, diffraction, or reflection by a standing-wave field. The effect caused in the behavior of spontaneous emission by the atomic center-of-mass motion, classical and quantized, in a standing wave cavity mode has been studied, and recently the one-atom laser with quantized atomic center-of-mass motion has been investigated. (omitted)

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