• 제목/요약/키워드: Annealing Test

검색결과 279건 처리시간 0.024초

열간가공된 γ-TiAl 합금의 미세조직 제어 및 기계적 특성 평가 (Microstructure Control and Tensile Property Measurements of Hot-deformed γ-TiAl alloy)

  • 박성현;김재권;김성웅;김승언;박노진;오명훈
    • 열처리공학회지
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    • 제32권6호
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    • pp.256-262
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    • 2019
  • The microstructural features and texture development by both hot rolling and hot forging in ${\gamma}-TiAl$ alloy were investigated. In addition, additional heat treatment after hot forging was conducted to recognize change of the microstructure and texture evolution. The obtained microstructural features through dynamic recrystallization after hot deformed ${\gamma}-TiAl$ were quite different because two kinds of formation process were occurred depending on deformation condition. However, analyzed texture tends to be random orientation due to intermediate annealing up to ${\alpha}+{\beta}$ region during the hot deformation process. After additional heat treatment, microstructure transformed into fully lamellar microstructure and randomly oriented texture was also observed due to the same reason as before. Tensile test at room temperature demonstrated that anisotropy of mechanical properties were not appeared and transgranular fracture was occurred between interface of ${\alpha}_2/{\gamma}$. As a result, it could be suggested that microstructural features influenced much more than texture development on mechanical properties at room temperature.

A simple damper optimization algorithm for both target added damping ratio and interstorey drift ratio

  • Aydin, Ersin
    • Earthquakes and Structures
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    • 제5권1호
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    • pp.83-109
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    • 2013
  • A simple damper optimization method is proposed to find optimal damper allocation for shear buildings under both target added damping ratio and interstorey drift ratio (IDR). The damping coefficients of added dampers are considered as design variables. The cost, which is defined as the sum of damping coefficient of added dampers, is minimized under a target added damping ratio and the upper and the lower constraint of the design variables. In the first stage of proposed algorithm, Simulated Annealing, Nelder Mead and Differential Evolution numerical algorithms are used to solve the proposed optimization problem. The candidate optimal design obtained in the first stage is tested in terms of the IDRs using linear time history analyses for a design earthquake in the second stage. If all IDRs are below the allowable level, iteration of the algorithm is stopped; otherwise, the iteration continues increasing the target damping ratio. By this way, a structural response IDR is also taken into consideration using a snap-back test. In this study, the effects of the selection of upper limit for added dampers, the storey mass distribution and the storey stiffness distribution are all investigated in terms of damper distributions, cost function, added damping ratio and IDRs for 6-storey shear building models. The results of the proposed method are compared with two existing methods in the literature. Optimal designs are also compared with uniform designs according to both IDRs and added damping ratios. The numerical results show that the proposed damper optimization method is easy to apply and is efficient to find optimal damper distribution for a target damping ratio and allowable IDR value.

가중평균 해석법을 이용한 래핑된 베어링강 어닐링재료의 깊이방향에 대한 잔류응력분포 측정 (Measurement of Residual Stress Distribution in the Depth Direction of Annealed Materials of Lapped Bearing Steel Using Weighted Averaging Analysis Method)

  • 한창석;이찬우
    • 한국재료학회지
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    • 제33권5호
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    • pp.205-213
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    • 2023
  • This paper reports the results of an experimental examination using X-rays to test annealing materials for lapped bearing steel (STB2), to confirm the validity of the weighted averaging analysis method. The distribution behavior for the α𝜓-sin2𝜓 diagram and the presence or absence of differences in the peak method, half-value breadth method, and centroid method were investigated. When lapping the annealed bearing steel (STB2) material, a residual stress state with a non-directional steep gradient appeared in the surface layer, and it was found that the weighted averaging analysis method was effective. If there is a steep stress gradient, the sin2𝜓 diagram is curved and the diffraction intensity distribution curve becomes asymmetric, resulting in a difference between the peak method, half-value breadth method, and centroid method. This phenomenon was evident when the stress gradient was more than 2~3 kg/mm2/㎛. In this case, if the position of the diffraction line is determined using the centroid method and the weighted averaging analysis method is applied, the stress value on the surface and the stress gradient under the surface can be obtained more accurately. When the stress gradient becomes a problem, since the curvature of the sin2𝜓 diagram appears clearly in the region of sin2𝜓 > 0.5, it is necessary to increase the inclination angle 𝜓 as much as possible. In the case of a lapping layer, a more accurate value can be obtained by considering 𝜎3 in the weighted averaging analysis method. In an isotropic biaxial residual stress state, the presence or absence of 𝜎3 can be determined as the presence or absence of strain for sin2𝜓≈0.4.

다차원 배낭 문제를 위한 정수계획법 기반 지역 탐색 기법 (Integer Programming-based Local Search Techniques for the Multidimensional Knapsack Problem)

  • 황준하
    • 한국컴퓨터정보학회논문지
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    • 제17권6호
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    • pp.13-27
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    • 2012
  • 정수계획법 기반 지역 탐색은 단순 언덕오르기 탐색을 기반으로 하는 지역 탐색의 일종으로서 기존의 지역 탐색과는 달리 이웃해 생성 시 정수계획법을 활용한다. 기존 연구 [1]에 의하면 정수계획법 기반 지역 탐색은 경영과학 및 인공지능 분야에서 많은 관심을 받아 온 다차원 배낭 문제를 해결하는 데 매우 효과적인 것으로 알려져 있다. 그러나 해당 연구에서는 OR-Library에 있는 다차원 배낭 문제들 중 규모가 가장 큰 문제들만을 대상으로 하여 정수계획법 기반 지역 탐색의 우수성을 검증하였다는 단점이 있다. 본 논문에서는 그 외의 문제들을 대상으로 정수계획법 기반 지역 탐색을 적용함으로써 보다 객관적으로 정수계획법 기반 지역 탐색의 우수성을 검증한다. 아울러 본 논문에서는 기존의 정수계획법 기반 지역 탐색이 단순 언덕오르기 탐색과 정수계획법을 결합한 것과는 달리 언덕오르기 탐색, 타부 탐색, 시뮬레이티드 어닐링과 같은 다른 지역 탐색 기법과 정수계획법을 결합하는 방안을 제시한다. 실험 결과, 정수계획법 기반 지역 탐색은 중소 규모의 다차원 배낭 문제들에 있어서도 기존의 가장 좋은 휴리스틱 탐색 기법에 비해 유사하거나 더 우수한 성능을 발휘함을 확인하였다.

R.F. 스퍼터링법에 의한 상변화형 광디스크의 $(ZnS)_{1-x}-(SiO_2)_x$ 보호막 제조시 기판 바이어스전압의 영향 (The Effects of Substrate Bias Voltage on the Formation of $(ZnS)_{1-x}-(SiO_2)_x$ Protective Films in Phase Change Optical Disk by R.F. Sputtering Method.)

  • 이태윤;김도훈
    • 한국재료학회지
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    • 제8권10호
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    • pp.961-968
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    • 1998
  • 상변화형 광디스크의 보호막으로 사용되는 $ZnS-SiO_2$ 유전체막을 RF magnetron 스퍼트링방법에 의하여 제조하는 경우에 기판 바이어스전압의 영향을 조사하기 위하여, 알곤가스 분위기에서 ZnS(80mol%)-$SiO_2$(20mol%)타겟을 사용하여 Si Wafer와 Corning flass 위에 박막을 증착시켰다. 본 실험에서는 여러 실험 변수를 효과적으로 조절하면서 실험의 양을 줄이고 도시의 산포를 동시에 만족시키는 최적조건으로 타겟 RF 출력 200W, 기판 RF 출력 20W, 아르곤 압력 5mTorr과 증착시간 20분을 얻을 수 있었으며, 신뢰구간 95%에서 확인실험을 수행하였다. 증착된 박막의 열적 저항성을 측정하기 위해 $300^{\circ}C$$600^{\circ}C$에서 열처리시험을 수행하였고, Spectroscopic Ellipsometry 측정을 통한 광학적 데이터를 바탕으로 Bruggeman EMA(Effective Medium Approximation)방법을 이용하여 기공(void)분률을 측정하였다. 본 연구결과에 의하면 특성치 굴절률에 대하여 기판 바이어스인자와 증착시간 사이에는 서로 교호작용이 강하게 존재함을 확인할 수 있었다. TEM분석과 XRD 분석 결과에 의하면 기판 바이어스를 가한 최적조건에서 증착된 미세조직은 기존의 바이어스를 가하지 않을 조건에서 증착시킨 박막보다 미세한 구조를 가지며, 또한 과도한 바이어스전압은 결정구조의 조대화를 야기시켰다. 그리고 적절한 바이어스전압은 박막의 밀도를 증가시키며, 기공분률을 약 3.7%정도 감소시킴을 확인할 수 있었다.

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폴리머 기반 3차원 뉴런 프로브의 잔류 스트레스 제거 및 생체 외 신호 측정 (Removal of Residual Stress and In-vitro Recording Test in Polymer-based 3D Neural Probe)

  • 남민우;임천배;이기근
    • 마이크로전자및패키징학회지
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    • 제16권2호
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    • pp.33-42
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    • 2009
  • 뇌로부터 뉴런의 움직임을 탐지할 수 있는 폴리머 계열 기반의 유연한 뉴런 프로브가 개발되었다. 삽입 강도 증가를 위해서 5 ${\mu}m$ 두께의 생체 적합성이 우수한 금을 상하층 폴리머 사이에 전기도금 하였다. 개발된 뉴런 프로브는 실제 뇌 조직과 비슷한 강도를 지닌 젤에 조금의 균열도 없이 삽입되었다. 또한 기계적 잔류 스트레스 및 이로 인해 발생하는 뉴런 프로브의 휘어짐을 최소화하기 위하여 두 가지의 새로운 방법이 적용되었다; (1) 제작 완료 후 후열처리 과정을 통하여 잔류 스트레스를 최소화하는 방법 (2) 상하층을 서로 다른 물질로 제작하여 상호 간의 잔류 스트레스를 보상하는 방법. 위 두 가지의 방법을 적용한 후에는 제작된 직후 뉴런 프로브의 끝부분에서 보여졌던 휘어짐이 뚜렷하게 제거되었다. 전기적 특성 측정 결과 뉴런 프로브는 뇌로부터 뉴런의 신호를 기록하기에 적절한 임피던스 값을 가지고 있음을 보였으며 측정된 임피던스 값은 72시간 후에도 변함이 없었다. 또한 생체 외 신호 측정 실험 결과 제작된 프로브는 잔류 스트레스의 완전한 제거뿐만 아니라 우수한 신호 기록 능력을 보였다. 일주일 후에도 측정 결과에는 변함이 없었으며, 이는 제작된 전극이 생체 내에서 뉴런 파이어링(firing)으로부터 장기간의 안정적인 신호 기록의 가능성을 보인다고 할 수 있다.

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Comparative study on the performance of butt fusion-welding processes for nuclear safety class large-diameter thick-walled PE pipes

  • Zhenchao Wang;Bin Wang;Aimin Xiang;Di Jiao;Fa Yu;Qiuju Zhang;Xiaoying Zhao
    • Nuclear Engineering and Technology
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    • 제56권10호
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    • pp.4184-4194
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    • 2024
  • New technologies in polymer synthesis and pipe extrusion equipment have led to the commercialization of high-performance, large-diameter, thick-wall high density polyethylene (HDPE) pipes. They have been used in the field of seawater transport and cooling to replace metal pipes, due to their advantages of high corrosion resistance and extensibility. Connection of HDPE pipe is important as it determines the safety of the entire piping system. Butt fusion welding is commonly used for HDPE pipe connection but may cause the formation of weak points in the welded joints, interfering the reliability of the pipeline system in the application of nuclear power plants. At present, there is a lack of research on evaluating the performance of welded joint for large-diameter thick-wall HDPE pipes made by butt fusion-welding. The purpose of this study is to investigate the influence of three different butt fusion-welding processes, i.e., single low pressure (SLP), single high pressure (SHP) and dual low pressure (DLP), by evaluating the performance of their welded joints, including characterizing tensile strength, extensibility, crystallinity and hardness. In specific, a thick-wall HDPE pipe with OD of 812.8 mm and wall thickness of 74 mm which is certified for nuclear safety class was used for study. Representative specimen from the outer, middle and inner part across the wall of the main pipe body and welded joints were taken for testing. Different test methods and specimens were designed to assess the feasibility of evaluating the welding performance from different welding process. The results showed that the mechanical properties of different locations of the welded joints were different, and the tensile strength and fracture energy of the middle part of the joint were lower than that of the inner and outer parts, which could be caused by the difference in the crystallinity and thickness of the melting zone influenced by welding processes, as can be seen from the analysis of DSC test and morphology observation. Hardness testing was conducted on the section of the welded joints, and it revealed that the micromechanical properties of the welded joints in the region of the heat-affected zone were enhanced significantly, which may be due to the annealing effect caused by welding process. In summary, The DLP process resulted in the best extensibility of the welded joints among three processes, suggesting that the joining pressure from welding process plays an important role in affecting the extensibility of the welded joints.

Stellite bearings for liquid Zn-/Al-Systems with advanced chemical and physical properties by Mechanical Alloying and Standard-PM-Route

  • Zoz, H.;Benz, H.U.;Huettebraeucker, K.;Furken, L.;Ren, H.;Reichardt, R.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2000년도 춘계학술강연 및 발표대회 강연 및 발표논문 초록집
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    • pp.9-10
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    • 2000
  • An important business-field of world-wide steel-industry is the coating of thin metal-sheets with zinc, zinc-aluminum and aluminum based materials. These products mostly go into automotive industry. in particular for the car-body. into building and construction industry as well as household appliances. Due to mass-production, the processing is done in large continuously operating plants where the mostly cold-rolled metal-strip as the substrate is handled in coils up to 40 tons unwind before and rolled up again after passing the processing plant which includes cleaning, annealing, hot-dip galvanizing / aluminizing and chemical treatment. In the liquid Zn, Zn-AI, AI-Zn and AI-Si bathes a combined action of corrosion and wear under high temperature and high stress onto the transfer components (rolls) accounts for major economic losses. Most critical here are the bearing systems of these rolls operating in the liquid system. Rolls in liquid system can not be avoided as they are needed to transfer the steel-strip into and out of the crucible. Since several years, ceramic roller bearings are tested here [1.2], however, in particular due to uncontrollable Slag-impurities within the hot bath [3], slide bearings are still expected to be of a higher potential [4]. The today's state of the art is the application of slide bearings based on Stellite\ulcorneragainst Stellite which is in general a 50-60 wt% Co-matrix with incorporated Cr- and W-carbides and other composites. Indeed Stellite is used as the bearing-material as of it's chemical properties (does not go into solution), the physical properties in particular with poor lubricating properties are not satisfying at all. To increase the Sliding behavior in the bearing system, about 0.15-0.2 wt% of lead has been added into the hot-bath in the past. Due to environmental regulations. this had to be reduced dramatically_ This together with the heavily increasing production rates expressed by increased velocity of the substrate-steel-band up to 200 m/min and increased tractate power up to 10 tons in modern plants. leads to life times of the bearings of a few up to several days only. To improve this situation. the Mechanical Alloying (MA) TeChnique [5.6.7.8] is used to prOduce advanced Stellite-based bearing materials. A lubricating phase is introduced into Stellite-powder-material by MA, the composite-powder-particles are coated by High Energy Milling (HEM) in order to produce bearing-bushes of approximately 12 kg by Sintering, Liquid Phase Sintering (LPS) and Hot Isostatic Pressing (HIP). The chemical and physical behavior of samples as well as the bearing systems in the hot galvanizing / aluminizing plant are discussed. DependenCies like lubricant material and composite, LPS-binder and composite, particle shape and PM-route with respect to achievable density. (temperature--) shock-reSistibility and corrosive-wear behavior will be described. The materials are characterized by particle size analysis (laser diffraction), scanning electron microscopy and X-ray diffraction. corrosive-wear behavior is determined using a special cylinder-in-bush apparatus (CIBA) as well as field-test in real production condition. Part I of this work describes the initial testing phase where different sample materials are produced, characterized, consolidated and tested in the CIBA under a common AI-Zn-system. The results are discussed and the material-system for the large components to be produced for the field test in real production condition is decided. Outlook: Part II of this work will describe the field test in a hot-dip-galvanizing/aluminizing plant of the mechanically alloyed bearing bushes under aluminum-rich liquid metal. Alter testing, the bushes will be characterized and obtained results with respect to wear. expected lifetime, surface roughness and infiltration will be discussed. Part III of this project will describe a second initial testing phase where the won results of part 1+11 will be transferred to the AI-Si system. Part IV of this project will describe the field test in a hot-dip-aluminizing plant of the mechanically alloyed bearing bushes under aluminum liquid metal. After testing. the bushes will be characterized and obtained results with respect to wear. expected lifetime, surface roughness and infiltration will be discussed.

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Interface Control to get Higher Efficiency in a-Si:H Solar Cell

  • Han, Seung-Hee;Kim, En-Kyeom;Park, Won-Woong;Moon, Sun-Woo;Kim, Kyung-Hun;Kim, Sung-Min
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
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    • pp.193-193
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    • 2012
  • In thin film silicon solar cells, p-i-n structure is adopted instead of p/n junction structure as in wafer-based Si solar cells. PECVD is the most widely used thin film deposition process for a-Si:H or ${\mu}c$-Si:H solar cells. Single-chamber PECVD system for a-Si:H solar cell manufacturing has the advantage of lower initial investment and maintenance cost for the equipment. However, in single-chamber PECVD system, doped and intrinsic layers are deposited in one plasma chamber, which inevitably impedes sharp dopant profiles at the interfaces due to the contamination from previous deposition process. The cross-contamination between layers is a serious drawback of single-chamber PECVD system. In this study, a new plasma process to solve the cross-contamination problem in a single-chamber PECVD system was suggested. In order to remove the deposited B inside of the plasma chamber during p-layer deposition, a high RF power was applied right after p-layer deposition with SiH4 gas off, which is then followed by i-layer, n-layer, and Ag top-electrode deposition without vacuum break. In addition to the p-i interface control, various interface control techniques such as FTO-glass pre-annealing in O2 environment to further reduce sheet resistance of FTO-glass, thin layer of TiO2 deposition to prevent H2 plasma reduction of FTO layer, and hydrogen plasma treatment prior to n-layer deposition, etc. were developed. The best initial solar cell efficiency using single-chamber PECVD system of 10.5% for test cell area of 0.2 $cm^2$ could be achieved by adopting various interface control methods.

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다단 치차장치 설계 시스템 개발에 관한 연구(제 2보: 일반화된 신설계 알고리즘의 개발) (Development of a Design System for Multi-Stage Gear Drives (2nd Report: Development of a Generalized New Design Algorithm))

  • 정태형;배인호;박경진
    • 한국정밀공학회지
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    • 제17권10호
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    • pp.192-199
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    • 2000
  • The design of multi-stage gear drives is a time-consuming process because it includes more complicated problems, which are not considered in the design of single-stage gear drives. The designer has no determine the number of reduction stages and the gear ratios of each reduction stage. In addition, the design problems include not only dimensional design but also configuration design of gear drive elements. There is no definite rule or principle for these types of design problems. Thus the design practices largely depend on the sense and the experiences of the designer, and consequently result in undesirable design solution. A new and generalized design algorithm has been proposed to support the designer at the preliminary phase of the design of multi-stage gear drives. The proposed design algorithm automates the design process by integrating the dimensional design and the configuration design process. The algorithm consists of four steps. In the first step, the user determines the number of reduction stages. In the second step, gear ratios of every stage are chosen using the random search method. The values of the basic design parameters of a gear are chose in the third step by using the generate and test method. Then the values of the dimensions, such as pitch diameter, outer diameter and face width, are calculated for the configuration design in the next step. The strength and durability of each gear is guaranteed by the bending strength and the pitting resistance rating practices by using AGMA rating formulas. In the final step, the configuration design is carried out using simulated annealing algorithm. The positions of gears and shafts are determined to minimize the geometrical volume (size) of a gearbox while avoiding interferences between them. These steps are carried out iteratively until a desirable solution is acquired. The proposed design algorithm is applied to the preliminary design of four-stage gear drives in order to validate the availability. The design solution has considerably good results in both aspects of the dimensional and the configuration design.

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