• Analytical Science and Technology
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• v.32 no.3
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• pp.88-95
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• 2019

This study was conducted to establish the analytical method for the determination of cyanide in blood, urine, lung and skin tissues in rats. In order to detect or quantify the sodium cyanide in above biological matrixes, it was derivatized to Pentafluorobenzyl cyanide (PFB-CN) using pentafluorobenzyl bromide (PFB-Br) and then reaction substance was analyzed using gas chromatography mass spectrometer (GC/MS)-SIM (selected ion monitoring) mode. The analytical method for cyanide determination was validated with respect to parameters such as selectivity, system suitability, linearity, accuracy and precision. No interference peak was observed for the determination of cyanide in blank samples, zero samples and lower limit of quantification (LLOQ) samples. The lowest limit detection (LOD) for cyanide was $10{\mu}M$. The linear dynamic range was from 10 to $200{\mu}M$ for cyanide with correlation coefficients higher than 0.99. For quality control samples at four different concentrations including LLOQ that were analyzed in quintuplicate, on six separate occasions, the accuracy and precision range from -14.1 % to 14.5% and 2.7 % to 18.3 %, respectively. The GC/MS-based method of analysis established in this study could be applied to the toxicokinetic study of cyanide on biological matrix substrates such as blood, urine, lung and skin tissues.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1995.10a
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• pp.859-863
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• 1995

Presented in the paper are a review of sorting and buffering system(SBS), the design procedure of a SBS and an analytical model for the initial alternative generation. SBS is an automated material handling system in which incoming items of different part types are automatically sorted and buffered so that the processing machines can process the part in lots. SBSs play a key role in modern manufacturing systems ans are widely found in mass fabrication lines, packaging and palletizing, and disribution centers.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2010.05a
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• pp.151-152
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• 2010

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1996.04a
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• pp.378-382
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• 1996

This paper presents a 'mixed' method for performing the sensitivity analysis for multibody dynamics. The mixed method uses both the analytical derivation and the numerical evaluation, in which premitive derivations rely on the analytical process and their associated individual terms are evaluated by the numerical precess. Therefore, this method can eliminate difficulty in dervation of the direct differentiation. Furthermore, by using the joint coordinate formulation for the equations of motion, compulational efficiencyand numerical accuracy are achieved.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2010.05a
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• pp.487-488
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• 2010

• Journal of the Korean Society for Precision Engineering
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• v.16 no.9
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• pp.104-109
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• 1999

The flywheel energy storage system using superconducting magnetic bearings is a device to store electrical energy as rotatioal kinetic energy by motor and to convert it to electrical energy by generator when it is necessary. The rotordynamic analysis should be performed with an adequate analytical model and equations of motion to identify the stable driving condition and the dynamic behavior. The critical speed and the unbalance response of superconducting magnetic bearings-flywheel system are studied in this paper. The analytical results show that the system has one forward whirling mode and two backward whirling models below 500rpm. The maximum displacement 0.75mm is detected at the first forward mode (385rpm)through unbalance response analysis. The analytical results are compared with the experimental result by the spin-down test. The experimental result shows that the maximum displacement is 0.7mm at 370rpm.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1996.04a
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• pp.568-573
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• 1996

In this paper, A design strategy of the Surface Mounting Device for accurate and better performance is studied. Analytical Modeling. Sensitivity analysis and optimization are being conducted. The ANSYS software and experimental method are used for verification of the analytical equations withboundary conditons. Through the sensitivity analysis, the most dominant design parameters can be detected. The optimum design parameters for performing given performing given perfomances are selected by using the optimization algorithm. The design tool based on the design strategy for the analysis, modeling and optimization will be useful for a re-design and better perofrmance of the SMD.

• Journal of the Korean Society for Precision Engineering
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• v.14 no.2
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• pp.120-128
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• 1997

In this paper, A design strategy of the Surface Mounting Device for accurate and better performance is studied. Analytical modeling, sensitivity analysis, and optimization are being conducted. The ANSYS software and experimental method are used for the verification of the analytical equations with boundary conditions. Through the sensitivity analysis, the most dominant design parameter can be detected. The optimum design parameters for improving the given performances are selected by using the optimiza- tion algorithm. The design tool based on the design strategy for the analysis, modeling, and optimization will be useful for are-design and better improving of the SMD.

• Environmental Analysis Health and Toxicology
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• v.17 no.2
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• pp.95-107
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• 2002

This study was designed to investigate the characteristics of atmospheric concentrations of toxic volatile organic compounds (VOCs) in Korea. Target compounds included 1,3-butadiene, aromatics such as BTEX, and a number of carbonyl compounds. In this paper, as the first part of the study, the performance of sampling and analytical methods was evaluated for the measurement of selected VOCs and carbonyl compounds in the ambient air. VOCs were determined by the adsorbent tube sampling and automatic thermal desorption coupled with GC/MSD analysis, while carbonyls by the DNPH-silica cartridge sampling with HPLC analysis. The methodology was investigated with a wide range of performance criteria such as repeatability, linearity. lower detection limits, collection efficiency, thermal conditioning, breakthrough volume and calibration methods using internal standards. In addition, the sampling and analytical methods established in this study were applied to real field samples duplicately collected in various ambient environments. Precisions for the duplicate samples appeared to be comparable with the performance criteria recommended by USEPA TO-17. The overall precision of the sampling and analytical methods was estimated to be within 20 ∼ 30% for major aromatic VOCs such as BTEX, whereas the precision for major carbonyl compounds such as formaldehyde and acetaldehyde was within 10 ∼ 20% for field samples. This study demonstrated that the adsorbent sampling and thermal desorption method can be reliably applied for the measurement of BTEX in ppb levels frequently occurred in common indoor and ambient environments.

• Journal of the Korean Society for Precision Engineering
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• v.28 no.5
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• pp.623-631
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• 2011

Metallic sandwich panels based on a truss core structure have been developed for a wide range of potential applications with their lightweight and multi-functionality. Structural performance of sandwich panels can be predicted from the studies on mechanical behavior of a unit cell of truss core structures. Analytical investigations on the unit cell provide approximated guidelines for the design of overall core structures for a specific application in short time. In this study, the effects of geometrical parameters on mechanical behavior of a pyramidal shape of unit cell were investigated with analytical models. The unit cell with truss member angle of 45 degree was considered as reference model and other models were designed to have the same weight and projected area but different truss member angle. All truss members were assumed to be connected with pin joint in analytical models. Under the assumptions, the equivalent strength and stiffness of the unit cell under compressive and shear loads were predicted and compared. And finally, the optimum core member angle to have maximum mechanical property could be calculated and verified with FE analysis results.