• Journal of Korean Society of Steel Construction
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• v.19 no.1
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• pp.43-52
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• 2007

There is a growing range of applications for concrete-filled steel tube (CFT) member because of its superior performance. But a CFT member may be uneconomical or has weight problems because it is fully filled with concrete. In this study, a new type of member, called internally confined hollow (ICH) CFT member, was developed to solve the high cost and weight problems of the CFT member. To determine stress-strain model of the concrete in an ICH CFT column, possible failure modes of an ICH CFT column were suggested and confining pressure was derived from equilibriums for each failure mode. From the derived equations, a computer program was coded and parametric studies were performed for some examples. Analytical results showed that internally confined concrete has enhanced strength and ductility compared with those of unconfined or biaxially confined concrete.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2011.10a
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• pp.325-330
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• 2011

RCP(Reactor coolant pump) must be designed to preserve it's functions on normal or abnormal environments and seismic event same as operating basis earthquake(OBE) and safe shutdown earthquake(SSE). Generally, there are static and dynamic analytical method which can be applied by a floor response spectrum or time history analysis for the seismic qualification. Initially, It was accomplished a detailed structural FE-model for finite element analysis on the bases of 3-dimensional solid model which was made by the RCP drawing. As the result of dynamic characteristic using the detailed FE-model, it's shown about 12Hz natural frequency of 1st bending mode shape and maximum displacement has 11mm with the structural bending by single-point response spectrum(SPRS) method at all elevation. But maximum displacement has 7.6mm by multi-point response spectrum(MPRS) method which was applied to the three floor response spectrum at each elevation. Therefore, On a large heighten structures as RCP, The application by SPRS method causes to be more conservative results. Finally, A simpled equivalent beam model which was developed by use of iteration of detailed FE-model is shown the result more similar with those of natural frequencies and SPRS analysis. And maximum equivalent stress and displacement of the simpled beam has verified with 180MPa and 7.1mm each at 15sec as results by SSE time history method.

• Natural Product Sciences
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• v.17 no.2
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• pp.147-159
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• 2011

A high-performance liquid chromatography-electrospray ionization-tandem mass spectrometric method was developed to determine simultaneously eight marker constituents of Forsythiae fructus, and subsequently applied it to classify its two botanical origins. The marker compounds of Forsythia suspensa were phillyrin, pinoresinol, phillygenin, lariciresinol and forsythiaside; those of F.viridissima were arctiin, arctigenin and matairesinol. Separation of the eight analytes was achieved on a phenyl-hexyl column (150${\times}$2.0 mm i.d., 3 ${\mu}M$) using gradient elution with the mobile phase: (A) 10% acetonitrile in 0.5% acetic acid, (B) 40% aqueous acetonitrile. A few fragment ions specific to the types of lignans, among the product ions generated by collisonally induced dissociation (CID) of molecular ion clusters, such as [M-H]$^-$ or [M+OAc]$^-$ were used not only for fingerprinting analysis but for the quantification of each epimer by using multiple-reaction monitoring mode. It was shown good linearity ($r^2{\geq}$ 0.9998) over the wide range of all analytes; intra- and inter-day precisions (RSD, %) were within 9.14% and the accuracy ranged from 84.3 to 115.1%. The analytical results of 40 drug samples, combined with multivariate statistical analyses - principal component analysis (PCA) and hierarchical cluster analysis (HCA) - clearly demonstrated the classification of the test samples according to their botanical origins. This method would provide a practical strategy for assessing the authenticity or quality of the herbal drug.

• Journal of Ginseng Research
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• v.40 no.3
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• pp.292-299
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• 2016

Background: We previously reported that two-phase partition chromatography between ginseng water extract and soybean oil efficiently eliminated pesticide residues. However, an undesirable odor and an unpalatable taste unique to soybean oil were two major disadvantages of the method. This study was carried out to find an alternative vegetable oil that is cost effective, labor effective, and efficient without leaving an undesirable taste and smell. Methods: We employed six vegetable oils that were available at a grocery store. A 1-mL sample of the corresponding oil containing a total of 32 pesticides, representing four categories, was mixed with 10% aqueous ginseng extract (20 mL) and equivalent vegetable oil (7 mL) in Falcon tubes. The final concentration of the pesticides in the mixture (28 mL) was adjusted to approximately 2 ppm. In addition, pesticides for spiking were clustered depending on the analytical equipment (GC/HPLC), detection mode (electron capture detector/nitrogen-phosphorus detector), or retention time used. Samples were harvested and subjected to quantitative analysis of the pesticides. Results: Soybean oil demonstrated the highest efficiency in partitioning pesticide residues in the ginseng extract to the oil phase. However, canola oil gave the best result in an organoleptic test due to the lack of undesirable odor and unpalatable taste. Furthermore, the qualitative and quantitative changes of ginsenosides evaluated by TLC and HPLC, respectively, revealed no notable change before or after canola oil treatment. Conclusion: We suggest that canola oil is an excellent vehicle with respect to its organoleptic property, cost-effectiveness and efficiency of eliminating pesticide residues in ginseng extract.

• The Journal of the Acoustical Society of Korea
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• v.21 no.5
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• pp.503-509
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• 2002

Cylindrical chamber silencers with an extended inlet and outlet are extensively used in many application fields to reduce the propagated noise in ducts. The basic attenuation effectiveness in the low frequency region can be explained by the reactive wave action inside the expansion chamber associated with the geometric configurations of the inlet and outlet locations, and the area expansion of the jacket. In this study. an acoustic analysis is carried out for a concentric extended pipe inserted into a simple expansion chamber. An algebraic equation is derived by using the eigenfunction expansion and orthogonality principle in which the acoustic pressures and particle velocities defined on each subdivided surface are expressed by the separable coordinates. By using the proposed analytical method, transmission losses are predicted for several configurations of the concentric extended systems and they agree very well with experimental results.

• Korean Journal of Food Science and Technology
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• v.28 no.3
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• pp.421-427
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• 1996

Ethyl carbamate is an animal carcinogen and a suspected human carcinogen found in fermented foods and beverages. For the determination of ethyl carbamate in typical Korean diet, an analytical method was established for the food as complex as Kimchi. Kimchi samples collected from various locations in the country were homogenized and extracted four times with ethyl acelate. Following concentration and reconstitution with water, the extract was loaded onto $C_{18}$ column. Fraction containing ethyl carbamate was eluted with methanol, while most of the red pigment of the sample was retained on the column. The eluent was further purified with alumina, followed by Florisil column. The final eluent was analyzed by gas chromatography mass spectrometry in the selected ion monitoring mode. None of the twenty Kimchi samples showed ethyl carbamate level higher than 4.6 ppb without correction for the recovery. The concentration of ethyl carbamate in Kimchi increased as pH decreased, suggesting fermentation dependent formation of ethyl carbamate.

• Korean Chemical Engineering Research
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• v.46 no.4
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• pp.660-664
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• 2008

In this work, analytical HPLC was utilized to obtain Tanshinone IIA (TIIA) from Salvia Miltiorrhiza Bunge (SMB). The optimum operating conditions were experimentally determined to analyze the TIIA in the pretreated extract. SMB was extracted with the various organic solvents of methanol, ethyl acetate, and ethanol, then the extract was analyzed to compare the amount of TIIA. From the results, the methanol showed the best extraction efficiency of TIIAd. The analysis by $C_{18}$ column was performed. The mobile phase was composed of methanol and water, and the isocratic elution mode was mainly applied. $2.154{\mu}g$ of TIIA/mg of SMB powder was extracted with methanol.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.15 no.3
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• pp.389-398
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• 2002

The mixed mode problem (I and II) of a peny-shaped interface cracks in remote tension loading on a bi-material cylinder is studied using finite element method. The energy release rates for the tip of the crack in the interface were calibrated for several different moduli combinations and crack ratios using the modified crack closure integral technique and J-integral method, with numerical results obtained from a commercial finite element program. Numerical results show that non-dimensional value of$\sqrt{G_{II}E^*}/\sqrt[p]{\pi a}$ increases as the crack size or moduli ratio increases. Meanwhile, non-dimensional value of$\sqrt{G_{I}E^*}/\sqrt[p]{\pi a}$ decreases as the moduli ratio increases, but above the moduli ratio of 3 its value decreases then increases again as the crack size increases. Reliability of the numerical analysis in this study was acquired with comparison to an analytical solution for the peny-shaped interface crack in an infinite medium.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.18 no.3
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• pp.311-320
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• 2005

In this paper an enhanced quadratic finite element for static and dynamic analysis of plate structures is presented. The performance of a proposed plate element is improved by the coupled use of non conforming displacement modes, the selective integration scheme, and the assumed shear strain fields. An efficient direct modification method is also applied to this element to solve the problem such as failure of the patch test due to the adoption of non conforming modes. The proposed quadratic finite element does not show any spurious mechanism and does not produce shear locking phenomena even with distorted meshes. It is shown that the results obtained by this element converged to analytical solutions very rapidly tough numerical tests for standard benchmark problems. It is also noted that this element is applicable to transient dynamic analysis of Mindlin plates.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.21 no.5
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• pp.483-491
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• 2008

The effectiveness of a new fiber-steel composite plate designed specifically to be used for strengthening of reinforced concrete members has been investigated. Twelve reinforced concrete beams were tested. Seven of the beams were strengthened with carbon fiber-steel composite plate(CSP), four of the beams were strengthened with glass fiber-steel composite plate(GSP), and one beam was used as a control specimen. The experimental results showed that new strengthening system controls the premature debonding and provides a more ductile failure mode than other conventional strengthening systems. The observed ductility ratios were $3.01\sim3.81$ and $3.55\sim4.95$ for strengthened beam with CSP and GSP, respectively. The maximum load was increased by 115% and 107% for strengthened beam with CSP and GSP, respectively, comparing with control beam. In addition, experimental and analytical results were well agreed.