• Journal of the Earthquake Engineering Society of Korea
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• v.8 no.3
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• pp.1-12
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• 2004

Due to the 1989 Loma Prieta, 1995 Hyogoken Nambu earthquakes, etc, a number of bridge columns  were collapsed in flexure-shear failures as a consequence of the premature termination of the column longitudinal reinforcement. Nevertheless, previous researches for the performance of bridge columns were concentrated on the flexural failure mode. It is well understood that the seismic behaviour of RC bridge piers was dependent on the performance of the plastic hinge of RC bridge piers, the ductility of which was desirable to be computed on the basis of the curvature. Experimental investigation was made to evaluate the variation of the curvature of the plastic hinge  region for the seismic performance of earthquake-damaged RC columns in flexure-shear failure mode. Seven test specimens in the aspect ratio of 2.5 were made with test parameters: confinement ratios, lap splices, and retrofitting FRP materials. They were damaged under series of artificial earthquakes that could be compatible in Korean peninsula. Directly after the pseudo-dynamic test, damaged columns were retested under inelastic reversal cyclic loading under a constant axial load, $P=0.1f_{ck}A_g$. Residual seismic capacity of damaged specimens was evaluated by analzying the moment-curvature hysteresis and the curvature ductility. Test results show that the biggest curvature was developed around 15cm above the footing, which induced the column failure. It was observed that RC bridge specimens with lap-spliced longitudinal steels appeared to fail at low curvature ductility but significant improvement was made in the curvature ductility of RC specimens with FRP straps wrapped around the plastic hinge region. Based on the experimental variation of the curvature of RC specimens, new equivalent length of the plastic hinge region was proposed by considering the lateral confinement in this study. The analytical and experimental relationship between the displacement and the curvature ductility were compared based on this proposal, which gave excellent result.

• Journal of the Korea institute for structural maintenance and inspection
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• v.21 no.3
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• pp.130-137
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• 2017

The purpose of this study is to provide a reasonable analytical method for the reinforced concrete beams which shows failure mode of shear and flexure-shear by proposing a modified formulation to consider the effect of shear deformation on the beam-column fiber element based on the flexibility method and a new constitutive law of inelastic shear response history for the section. A total of 6 specimens of reinforced concrete beams which is designed to cause shear failure before yielding longitudinal reinforcement to investigate the influence of the main experimental variables on the shear behavior characteristics and the analysis was performed by using a non-linear finite element analysis program (RCAHEST) applying the newly modified constitutive equation by the authors. The failure mode and the overall behavior characteristics until fracture are predicted appropriately for all specimens and the results are expected to be useful enough for the 3 - D analysis to carry out reliable results of large-scale and complicated structures in the future.

• Journal of Food Hygiene and Safety
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• v.33 no.2
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• pp.118-123
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• 2018

The objective of this study was to develop a sensitive method for the identification and determination of nitrovin in fishery products by using a solid-phase extraction (SPE), as performed with a liquid chromatography-tandem mass spectrometry (LC-MS/MS). The samples were extracted with a mixture of acetonitrile and water, and were then defatted with acetonitrile saturated hexane, after which further clean-up was accomplished with SPE on the hydrophilic-lipophilic balance (HLB) cartridges. The analytes were subsequently ionized in the positive mode of an electrospray ionization (ESI), and where thereby detected in a process of multiple reaction monitoring (MRM). The linearity (expressed as correlation coefficients) of the matrix calibration curves was > 0.985. The limit of the quantification for the nitrovin was measured at 0.001 mg/kg. The accuracy (expressed as average recovery) was noted between 72.1 and 122%. The precision (expressed as coefficient variation) was noted from 2.9 to 16.9%. According to the CODEX CAC/GL-71 guideline accuracy, precision, linearity, and limit of detection were determined in three matrices (which were flatfish, eel and shrimp). The proposed method was suitable for analyzing the associated nitrovin residues. This application and result can also be a factor to contribute to the non-detection drugs management in fishery products.

• Journal of Korean Society of Steel Construction
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• v.16 no.3 s.70
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• pp.295-303
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• 2004

In this paper, an improved four-node Reissner-Mindlin plate-bending element with enhanced assumed strain field is presented for the analysis of isotropic and laminated composite plates. To avoid the shear locking and spurious zero energy modes, the transverse shear behavior is improved by the addition of a new enhanced shear strain based on the incompatible displacement mode approach and bubble function. The "standard" enhanced strain fields (Andelfinger and Ramm, 1993) are also employed to improve the in-plane behaviors of the plate elements. The four-node quadrilateral element derived using the first-order shear deformation theory is designated as "14EASP". Several applications are investigated to assess the features and the performances of the proposed element. The results are compared with other finite element solutions and analytical solutions. Numerical examples show that the element is stable, invariant, passes the patch test, and yields good results especially in highly distorted regimes.

• YAKHAK HOEJI
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• v.57 no.5
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• pp.330-336
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• 2013

"The Act on Medication Treatment of Sexual Impulse of Sex Offenders" known as chemical castration has been effective since July 2011 in Korea. According to the law, monitoring of male sex hormone in urine is enforced to request National Forensic Service more than once a month after injection of medicine designed to reduce sex impulse. We established a rapid and sensitive method for the monitoring of testosterone (T) and epitestosterone (E) in human urine by liquid chromatography with tandem mass spectrometry (LC-MS/MS). Three mL of urine was pretreated by solid-phase extraction for purification and performed enzymatic hydrolysis. The pretreated samples were extracted twice with 2 ml of ethyl acetate and n-hexane (2 : 3). The separation was applied on Thermo Hypersil GOLD C18 column ($1.9{\mu}m$, $100{\times}2.1mm$). A gradient elution of methanol and water of 0.1% formic acid were used as mobile phase and the retention time was less than 10 min. LC-MS/MS system coupled with an electrospray ionization source was performed in multiple reaction monitoring mode. The transitions of the analytes executed as following: m/z $289{\rightarrow}97$, 109 for T and E, m/z $292{\rightarrow}109$ for $T-d_3$ and $E-d_3$ as internal standards. The validation results of the method were satisfactory. The limits of detection were 0.05 ng/ml and the limits of quantification were 0.1 ng/ml. This method was successfully applied to real human urine sample. The developed method will be useful for monitoring T/E ratio in urine of sex offenders.

• Computational Structural Engineering
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• v.5 no.4
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• pp.93-102
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• 1992

The design of reactor internals requires the accurate vibration characteristics of each component for subsequent dynamic structural response analyses. For Korean standard nuclear power plant some modifications on the Control Element Assembly shroud from the reference design have been made, Since the shroud is complex in geometry having an array of vertical round tubes and webs in a square grid pattern, and being tied down by preloaded tie rods into position, it is planned to perform a vibration measurement program consisting of both experimental and analytical modal studies upon that component. The shroud modal testing was performed on the low frequency global survey to measure the first several modes. The analysis using the finite element model was also performed for the as-tested conditions. The natural frequencies and mode shapes from both test and analysis have been acquired and compared to be in good agreement. It is concluded that finite element model generated is good enough to be used in the design for the dynamic response analysis under various loading conditions.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2008.04a
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• pp.397-401
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• 2008

Knowledge of dynamic characteristics of structural elements often can make difference between success and failure in the design of structure due to resonance effect. In this paper an analytical model of a cantilever beam having midpoint load is considered for structural optimization. This involves creating the geometry which allows parametric study of all design variables. For that purpose optimization of cantilever beam is elaborated in order to find the optimum geometry which minimizes its volume eventually for minimum weight using ANSYS. But such geometry could be obtained by different combinations of width and height, so that it may have the same cross sectional area yet different dynamic behavior. So for optimum safe design, besides minimum volume it should have minimum vibration as well. In order to predict vibration different dynamic analyses are performed simultaneously to solve the eigenvalues problem assuming no damping initially through MATLAB simulations using state space form for modal analysis, which identifies the resonant frequencies and mode shapes belonging to the lowest three modes of vibration. And next by introducing damping effects tip displacement, bending stress and the vertical reaction force at the fixed end is evaluated under some dynamic load of varying frequency, and finally it is discussed how resonance can be avoided for particular design. Investigation of results clearly shows that only structural analysis is not enough to predict the optimum values of dimension for safe design. Potentially this technique will meet maintenance and cost goals of many organizations particularly for the application where dynamic loading is invertible and helps a lot ensuring that the proposed design will be safe for both static and dynamic conditions.

• International Journal of Naval Architecture and Ocean Engineering
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• v.10 no.3
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• pp.393-402
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• 2018

While interacting with a sloping structure, an ice floe may fracture in different patterns. For example, it can be local bending failure or global splitting failure depending on the contact properties, geometry and confinement of the ice floe. Modelling these different fracture patterns as a natural outcome of numerical simulations is rather challenging. This is mainly because the effects of crack propagation, crack branching, multi fracturing modes and eventual fragmentation within a solid material are still questions to be answered by the on-going research in the Computational Mechanic community. In order to simulate the fracturing of ice floes with arbitrary geometries and confinement; and also to simulate the fracturing events at such a large scale yet with sufficient efficiency, we propose a semi-analytical/empirical and semi-numerical approach; but with focus on the global splitting failure mode in this paper. The simulation method is validated against data we collected during the Oden Arctic Technology Research Cruise 2015 (OATRC2015). The data include: 1) camera images based on which we specify the exact geometry of ice floes before and after an impact and fracturing event; 2) IMU data based on which the global dynamic force encountered by the icebreaker is extracted for the impact event. It was found that this method presents reasonably accurate results and realistic fracturing patterns upon given ice floes.

• Journal of the Korean Society of Tobacco Science
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• v.30 no.1
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• pp.33-38
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• 2008

This study was carried out to determine the analytical methods for heterocyclic amines(HAs) of the tobacco smoke by LC/MS/MS. HAs have been found in pyrolysate of protein and cooked food including protein, were known the Sugimura compound. HAs content of the smoke were known to exist very low ppb level. Especially, some of HAs are mutagenic and carcinogenic compounds. In according to IARC, the toxicity of N-heterocyclic amines classified IARC class 2A or 2B group. Precursors of these compounds are glutamic acid, protein and free amino acids including tryptophan, therefore, the precursors have been proved in cooked food continuously. This study was investigate multiple analysis methods for HAs and HAs contents of some commercial products. In this study, we used the linear type smoking machine for HAs analysis. At the ISO conditions, mainstream smoke was collected on cambridge filter pad, and then cambridge filter pad was extracted by 0.1% acetic acid. The extracted solution were passed cation exchange SPE cartridge to remove matrix, samples were analyzed using LC/MS/MS on MRM mode. From the result that optimized this methods, the correlation coefficient(R) of the individual compounds were good linearity over 0.999, recovery rate over 96% and the limit of detection were good values between 0.06 to 0.37 ng/mL, In addition, HAs content of some commercial products were in range of 0.02 to 43.8 ng/cig.

• Magazine of the Korea Concrete Institute
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• v.11 no.2
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• pp.177-186
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• 1999

The purpose of this study is to analyze the interface debonding of RC beams strengthened by carbon fiber sheet(CFS). The behavior of damaged RC beams strengthened with CFS is analytically investigated next using linear elastic fracture mechanics(LEFM) approach and the finite element method. The study includes an investigation of the separation mode by interface fracture of the strengthening materials due to the interfacial shear and normal stresses. The numerical method is presented to obtain the value of interfacial fracture parameter such as the strain energy release rate. Based on the results of this study, it is found that the critical case occurs when the interfacial cracks occur within a short region of the flexural crack. The CFS strengthening has not an adequate factor of safety against interfacial debonding of CFS. Furthermore, for the thicknesses of the adhesive studied[1mm~3mm], it is no noticeable effect on the strain energy release rate.