• 생약학회지
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• 제41권1호
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• pp.67-72
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• 2010

In the recent version of the Korea Pharmacopoeia(KP) and the Korean Herbal Pharmacopoeia(KHP), there are 563 items(181 in KP, 381 in KHP) of herbal medicines including finished drugs. Also, approximately 507 items including herbal extracts and herbal medicinal products was published in the 3th edition of Korea Pharmaceutical Codex (KPC). These items help the persons working in the pharmaceutical manufacturing field to register the drug and in research fields to develop the new drug considering as a standard specifications. This study was carried out to establish standard analytical methods for 'Compound Hawthorn Berry 60% Ethanol Extract, Ginkgo Biloba Leaf Extract and Garlic Oil Capsules' in the 3th edition of Korea Pharmaceutical Codex. Ginkgo flavonoid and terpene lactone were employed as reference compounds for analytical method. Analytical methods established in this study could be applied to a reasonable and unified quality control of G. biloba leaf extract and hawthorn berry extract.

• 분석과학
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• 제15권3호
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• pp.300-316
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• 2002

수질 및 토양 시료 중의 PBBs의 분석방법 확립을 위해 표준물질이 준비된 PBBs 22종을 대상으로 추출 및 정제 등의 전처리 회수율 및 검출한계를 환경시료로부터 얻었다. PBBs의 시료 추출법으로 액/액, 속실렛, 초음파 추출법을 적용하였고, 실리카겔, 플로리실 정제컬럼의 적용성 검토 후 GC/MS로 분석하였다. 수질 시료의 경우 검출한계는 브롬화된 정도에 따라 약간의 차이를 보였고 5~10 ng/L이었으며, n-hexane, dichloromethane 및 toluene 등의 단일 용매의 평균회수율은 96~107%, n-hexane:acetone (1:1) 및 (9:1)의 혼합용매의 평균 회수율은 60~80%로 나타났다. 또한, 토양 시료의 경우 검출한계는 0.5~3.5 ng/g이었으며, 선정 용매의 평균 회수율은 속실렛 추출이 67~97% 및 초음파 추출이 64~76%로 나타났다.

• 분석과학
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• 제20권2호
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• pp.91-108
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• 2007

토양 중 PCBs 분석방법을 검토하기 위해 우리나라 토양오염공정시험방법 및 선진국의 분석방법을 비교 검토하고 결과를 근거로, 추출 및 전처리방법, 칼럼정제방법, 분석용 칼럼 조건, 기기분석 조건 및 정량방법을 검토하였다. 또한 검토된 방법에 따라 토양 중 PCBs 세부분석지침(안)을 제시하고, 제시된 세부분석지침(안)에 의해 PCBs 제품으로 오염시킨 토양 5건 시료와 토지이용도별 및 오염원별 23건의 시료를 전처리하여 분석하였다. 기체크로마토그래피/전자포획검출법(GC/ECD)에 의한 토지이용도별 및 오염원별 PCBs 분석결과는 모든 시료에서 피크패턴(GC/ECD)을 확인 할 수 없었으나, 기체크로마토그래피/질량분석법(GC/MS)에 의한 개별이성체 정량결과는 $0.002{\sim}0.487{\mu}g/kg$ 범위로 검출되었다.

• 대한화학회지
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• 제38권11호
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• pp.800-807
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• 1994

직독식 원자방출분광기로 철강 재료중의 구성원소를 매트릭스 보정법으로 신속히 분석하는 방법에 대하여 연구하였다. 선형과 비선형법으로 매트릭스 보정계수를 구하였으며 이때 구한 매트릭스 계수는 서로 차이가 있지만 이들의 계수를 이용하여 구한 분석결과는 비교적 잘 일치하였다.

• Journal of Astronomy and Space Sciences
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• 제15권2호
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• pp.485-497
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• 1998

본 논문에서는 다목적 실용위성 관제시스템의 성능지표의 하나인 가용 도를 산출하기 위한 H/W 및 S/W 시스템 가용도의 수학적 모델 링을 제시하고, 직렬연결 시스템과 별렬 연결 시스템 그리고 이중화 시스템에 대한 가용도 산출 방법을 제시하였다. 또한 가용도 향상을 위한 이중화 방법에서 효율적인 스위치 선택방법을 기술하였으며, 다목적 실용위성 1호 관제시스템의 가용 도를 산출하였다. 가용도 분석 결과 비 이중화 시가용 도는 0.995216, 이중화 시가용도는 0.9955165, 관제시스템 실시간 운용 가용 도는 0.9963991로 분석되었다.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2010년도 춘계학술대회 논문집
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• pp.41-44
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• 2010

Hazardous air pollutants such as benzo[a]pyrene (BaP), benzene, formaldehyde have been concerned about the adverse health effect of long-term exposure. Contour map is useful for finding high-concentration region, emission source, and distributions of HAPs in the ambient air. To make a contour map, we have developed simple analytical method for selected HAPs; polycyclic aromatic hydrocarbons such as BaP, benzene and its derivatives such as toluene and xylene, and aldehydes and ketones. We have applied these methods to investigate air pollution by HAPs in some cities in Japan. The results show that these methods reveal actual emission sources if the PRTR emission report was not submitted.

• Selected Papers of The Society of Naval Architects of Korea
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• 제2권1호
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• pp.1-17
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• 1994

For a planar curve-sided panel with constant or linear density distributions of source or doublet in the singularity methods, Cantaloube and Rehbach show that the surface integral can be transformed into contour integral by using Stokes'formulas. As an extension of their formulations, this paper deals with a planar polygonal panel for which we derive the closed-forms of the potentials and the velocities induced by the singularity distributions. Test calculations show that the analytical evaluation of the closed-forms is superior to numerical integration (suggested by Cantaloube and Rehbach) of the contour integral. The compact and explicit expressions may produce accurate values of matrix elements of simultaneous linear equations in the singularity methods with much reduced computer time.

• 한국환경과학회:학술대회논문집
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• 한국환경과학회 2003년도 International Symposium on Clean Environment
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• pp.135-138
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• 2003

Based on solid phase extraction, gas chromatography and mass spectrometry procedure for determining phenol and its derivatives in natural water was presented. In solid phase extraction, three types of techniques using solid phase adsorption material were treated with acid and salt, and converted second portion of acetyl derivatives. Under the these condition, extraction efficiency and detection ability dependent on extraction methods were discussed. Obtained results using optimized solid phase extraction techniques showed more convenience, simplifier and lower cost than the conventional analytical methods with holding wide dynamic range and lower detection limits.

• 한국생산제조학회지
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• 제26권2호
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• pp.199-204
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• 2017

In this study, analytical methods for designing a torque arm pin and elastomeric bushings of a conventional-type three-point-suspension gearbox of a wind turbine are investigated. The design loads for the torque arm were derived by considering the effects of the transmitted torque and self-weight of the gearbox. Based on the design loads, design methods for the torque arm pin and elastomeric bushings were introduced in the terms of material and size selection. Finally, a small-scale conventional-type gearbox was designed by applying the derived design methods. This study is an elementary and analytical study for the design of the torque arm pin and elastomeric bushings. It is necessary to verify and supplement the results further through extensive experimentation.

• Food Science and Biotechnology
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• 제18권6호
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• pp.1515-1518
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• 2009

The objective of this study was to compare 3 extraction methods including, solid phase extraction (SPE), acetonitrile extraction, and methanol extraction, for their usefulness as extraction methods to determine capsaicinoids. The determination of capsaicinoids in the extracts was carried out on a reverse-phased high performance liquid chromatography (HPLC) using a fluorescence detector. Three extraction methods, i.e., SPE, acetonitrile extraction, and methanol extraction were compared for the quantification of capsaicinoids using raw peppers and pepper powder. The highest analytical values were observed using methanol extraction and the lowest values using SPE. Also, the analytical method validation parameters such as accuracy, precision, limit of detection, limit of quantitation, and specificity were calculated to ensure the method's validity. This method provides a fast and accurate approach for the determination of capsaicinoids in peppers.