• Title/Summary/Keyword: Analytical Techniques

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Yogurt Flavor Compounds and Analytical Techniques (Yogurt의 향미성분과 분석기술)

  • Chang, Eun-Jung;Kwak, Hae-Soo
    • Journal of Dairy Science and Biotechnology
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    • v.18 no.1
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    • pp.61-72
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    • 2000
  • Consumers primarily consider flavor when they take yogurt. Recent researches on yogurt flavor productron its analytical technique have been extensively developed. These studies have provided a better understanding on the role of starter culture microorganisms on flavor formation and degradation. Yogurt volatile flavor compounds produced by the lactic cultures include acetaldehyde, diacetyl, ethanol and organic acid. Among them, acetaldehyde is recognized as a principal flavor component. since yogurt contains a delicate and low intense flavor, mild sample isolation techniques and sensitive identification means might be used. This paper attempts to discuss recent findings in yogurt flavor and to describe the application of yogurt flavor separation techniques. The section on practical aspects of culture selection based on flavor compound production and flavor analysis is also included.

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Dynamic Nonlinear Analysis Model for Reinforced Concrete Elements considering Strain Rate Effects under Repeated Loads (변형율속도를 고려한 반복하중을 받는 철근콘크리트 부재의 동적 비선형 해석모델)

  • 심종성;문일환
    • Proceedings of the Korea Concrete Institute Conference
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    • 1990.04a
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    • pp.78-83
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    • 1990
  • The current analytical techniques for R/C elements under severe dynamic repeated loads, like earthquake or impact, has two major problems; one is that the effects of strain rate are not considered and the other one is the current model was developed based on flexural behavior only. Thus, this study develops a computer software that can idealize the flexural and shear behavior of R/C elements using several parameters and also can consider the effects of strain rate. The analytical results using the developed analytical technique were compared with several experimental results and were generally satisfied.

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Analytical modelling and behavior of RC beam-column joints (RC 보-기둥 접합부의 해석 모델링과 거동)

  • 우성우;이한선
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.11a
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    • pp.388-391
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    • 2003
  • In this study, the experimental results were simulated by using a nonlinear analysis programs IDARC 2D and RUAUMOKO 2D. These programs use a global Takeda-like model. The objectives of this study is to verify the correlation between the experimental and analytical responses of reinforced concrete (RC) frame and to provide the calibration to the available static inelastic analysis techniques. The evaluation of the accuracy of analytical simulation by IDARC 2D and RUAUMOKO 2D leads to the conclusion that the global behaviors can be, in general, simulated with limited accuracy in the linear analysis as detailing.

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A Study on the Techniques of Simulation Test in Automotive Braking System (자동차 제동장치의 시뮬레이션 시험 기법에 관한 연구)

  • 민규식;김형섭
    • Journal of the Korean Society of Safety
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    • v.8 no.2
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    • pp.23-29
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    • 1993
  • In this study, the method of deciding simulation test conditions is developed by computer program compared to actual vehicle test as accurately as possible. These results of analytical test conditions are conformed by simulation test using the brake dynamometer by comparison with test results of actual vehicle. Results of simulation test by these analytical results show good agreement with the vehicle test results. The analytical simulation test conditions provide the input data to brake dynamometer which follows : - each test inertia corresponding to braking deceleration - test condition of input control : brake line pressure - test condition of output control : braking torque

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Complete Assignment of the $^H1$ and $^{13}C$ NMR Spectra of a Sucrose Ester from Euphorbia Lathyris L.

  • Jung, Min-Hwan;Kim, Hyun-Sik;Sangdoo Ahn;Kim, Cheong-Taek;Jin, Mu-Hyun;Yim, Yong-Hyeon;Kim, Young-Kook;Jong hoa Ok
    • Journal of the Korean Magnetic Resonance Society
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    • v.4 no.2
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    • pp.125-132
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    • 2000
  • The detailed $^1$H and $^{13}$ C NMR assignments of a novel sucrose isovaleryl ester isolated from the seed of Euphorbia Lathyris L., were achieved by one-and two-dimensional techniques. The new sucrose ester was characterized as an $\alpha$-D-glucopyranoside, 3,4,6-tris-O-(3-methyl-1-oxobutyl)-$\beta$-D-fructofuranosyl, 2,6-bis(3-methylbutanoate); sucrose 4,7,8,11,12-pentaisovalerate by MS and NMR experiments.

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Determination of trace bromate in various water samples by direct-injection ion chromatography and UV/Visible detection using post-column reaction with triiodide

  • Kim, Jungrae;Sul, Hyewon;Song, Jung-Min;Kim, Geon-Yoon;Kang, Chang-Hee
    • Analytical Science and Technology
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    • v.33 no.1
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    • pp.42-48
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    • 2020
  • Bromate is a disinfection by-product generated mainly from the oxidation of bromide during the ozonation and disinfection process in order to remove pathogenic microorganism of drinking water, and classified as a possible human carcinogen by International Agency for Research of Cancer (IARC) and World Health Organization (WHO). For the purpose of determining the trace level concentration of bromate, several sensitive techniques are applied mostly based on suppressed conductivity detection and UV/Visible detection after postcolumn reaction (PCR). In this study, the suppressed conductivity detection method and the PCR-UV/Visible detection method through the triiodide reaction were compared to analyze the trace bromate in water samples and estimated for the availability of these analytical methods. In addtion, the state-of-the-art techniques was applied for the determination of trace level bromate in various water matrices, i.e., soft drinking water, hard drinking water, mineral water, swimming pool water, and raw water. In comparison of two analytical methods, it was found that the conductivity detection had the suitable advantage to simultaneously analyze bromate and inorganic anions, however, the bromate might not be precisely quantified due to the matrix effect especially by chloride ion. On the other hand, the trace bromate was analyzed effectively by the method of PCR-UV/Visible detection through triiodide reaction to satisfactorily minimize the matrix interference of chloride ion in various water samples, showing the good linearity and reproducibility. Furthermore, the method detection limit (MDL) and recovery were 0.161 ㎍/L and 101.0-108.1 %, respectively, with a better availability compared to conductivity detection.

Direct Analysis in Real Time Mass Spectrometry: a Powerful Tool for Fast Analysis

  • Li, Xianjiang;Wang, Xin;Li, Linnan;Bai, Yu;Liu, Huwei
    • Mass Spectrometry Letters
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    • v.6 no.1
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    • pp.1-6
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    • 2015
  • Direct analysis in real time mass spectrometry (DART-MS) is one of the variants of ambient mass spectrometry. The ionization process of DART-MS is in open environment and only takes few seconds, so it is suitable for fast analysis. Actually, since its introduction in 2005, more and more attentions have been drawn to its various applications due to its excellent properties, e.g., fast analysis, and no or less sample preparation, high salt tolerance and so on. This review summarized the promising features of DART-MS, including its ionization mechanism, equipment modification, wide applications, coupling techniques and extraction strategies before analysis.

Nanometrology and its perspectives in environmental research

  • Kim, Hyun-A;Seo, Jung-Kwan;Kim, Taksoo;Lee, Byung-Tae
    • Environmental Analysis Health and Toxicology
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    • v.29
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    • pp.16.1-16.9
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    • 2014
  • Objectives Rapid increase in engineered nanoparticles (ENPs) in many goods has raised significant concern about their environmental safety. Proper methodologies are therefore needed to conduct toxicity and exposure assessment of nanoparticles in the environment. This study reviews several analytical techniques for nanoparticles and summarizes their principles, advantages and disadvantages, reviews the state of the art, and offers the perspectives of nanometrology in relation to ENP studies. Methods Nanometrology is divided into five techniques with regard to the instrumental principle: microscopy, light scattering, spectroscopy, separation, and single particle inductively coupled plasma-mass spectrometry. Results Each analytical method has its own drawbacks, such as detection limit, ability to quantify or qualify ENPs, and matrix effects. More than two different analytical methods should be used to better characterize ENPs. Conclusions In characterizing ENPs, the researchers should understand the nanometrology and its demerits, as well as its merits, to properly interpret their experimental results. Challenges lie in the nanometrology and pretreatment of ENPs from various matrices; in the extraction without dissolution or aggregation, and concentration of ENPs to satisfy the instrumental detection limit.