• Title/Summary/Keyword: Analytical Techniques

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Analysis on Static Characteristics of Slotless Type Permanent Magnet Electrical Machines Using the Electromagnetic Transfer Relations (전자기 전달관계를 이용한 슬롯리스형 영구자석 전기기기의 정특성 해석)

  • Jang, Seok-Myeong;Choi, Jang-Young;Lee, Sung-Ho;Cho, Han-Wook
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.55 no.3
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    • pp.138-145
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    • 2006
  • It is well known that the accurate calculation of the field distribution is essential for the design of electrical machines. The analytical techniques for electromagnetic field can quickly and exactly determine airgap magnetic field distribution in electrical machines. Many analytical techniques have been investigated to predict the magnetic field distribution in PM machines equipped with permanent magnets. Using the analytical technique by transfer relations, D. L. Trumper and K. R. Davey already presented the design and analysis of linear permanent-magnet machines and induction machines, respectively. Using the transfer relations (Melcher's general methodology) to describe electromagnetic phenomena, this paper deals with the analysis on the magnetic field distribution due to PM and winding current, the induced voltage and the static torque characteristics in surface-mounted slotless type permanent magnet machine. The validity of the analysis results is confirmed by finite element (FE) analysis.

Mass Spectrometry-Based Analytical Methods of Amatoxins in Biological Fluids to Monitor Amatoxin-Induced Mushroom Poisoning

  • Choi, Jin-Sung;Lee, Hye Suk
    • Mass Spectrometry Letters
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    • v.13 no.4
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    • pp.95-105
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    • 2022
  • Amatoxin-induced mushroom poisoning starts with nonspecific symptoms of toxicity but hepatic damage may follow, resulting in the rapid development of liver insufficiency and, ultimately, coma and death. Accurate detection of amatoxins, such as α-, β-, and γ-amanitin, within the first few hours after presentation is necessary to improve the therapeutic outcomes of patients. Therefore, analytical methods for the identification and quantification of α-, β-, and γ-amanitin in biological samples are necessary for clinical and forensic toxicology. This study presents a literature review of the analytical techniques available for amatoxin detection in biological matrices, and established an inventory of liquid chromatography (LC) techniques with mass spectrometry (MS), ultraviolet (UV) detection, and electrochemical detection (ECD). LC-MS methods using quadrupole tandem mass spectrometry, time-of-flight mass spectrometry, and orbitrap MS are powerful analytical techniques for the identification and determination of amatoxins in plasma, urine, serum, and tissue samples, with high sensitivity, specificity, and reproducibility compared to LC with UV and ECD, enzyme-linked immunoassay, and capillary electrophoresis methods.

A Study on the Analyzing International Cooperation Using Bibliometrics : Focused on LED (계량서지분석을 통한 국가간 협력도 분석에 관한 연구 : LED분야를 중심으로)

  • Lee, Woo-Hyoung;Yeo, Woon-Dong;Park, Jun-Cheul
    • The Journal of Information Systems
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    • v.20 no.3
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    • pp.111-127
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    • 2011
  • This study is intended for international cooperation in the field of LED were analyzed. The results, LED wide coverage areas, and a promising future is expected to grow fast enough to occupancy for a major national technology is a competitive situation. Chip Scale Package, including our country, such as LED manufacturing technology that might be competitive in parts, but new technologies such as renal substrate R&D and technology development still active preemption is not the situation. Renal substrate, particularly, large-diameter sapphire, large size/large LED manufacturers, such as a promising area for future research and development support will be needed. To do this, previous research in this area and the U.S., Japan cooperation in such studies also will need to expand. Bibliometrics way through this study, analytical techniques and analytical tools used in the integrated analysis of the usefulness and necessity of the system development were found.

Analytical Techniques Using ICP-MS for Clinical and Biological Analysis

  • Ko, Jungaa;Lim, H. B.
    • Mass Spectrometry Letters
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    • v.6 no.4
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    • pp.85-90
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    • 2015
  • This article reviews recent analytical techniques using inductively coupled plasma-mass spectrometry (ICP-MS) immunoassay for clinical and bio analysis. We classified the techniques into two categories, direct and indirect analysis, which depend upon a guideline of whether tagging materials are used or not. Direct analysis is well known, and generally used in conjunction with various other techniques, such as laser ablation, chromatographic separations, etc. Recently, indirect analysis using tagging elements has intensively been discussed because of its importance in future applications to bio and clinical analysis, including environmental and food industries. The method has shown advantages of multiplex detection, excellent sensitivity, and short analysis time owing to signal amplification and magnetic separation. Now, it expands the application field from small biomolecules to large cells.

Structural Equation Modeling Using R: Mediation/Moderation Effect Analysis and Multiple-Group Analysis (R을 이용한 구조방정식모델링: 매개효과분석/조절효과분석 및 다중집단분석)

  • Kwahk, Kee-Young
    • Knowledge Management Research
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    • v.20 no.2
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    • pp.1-24
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    • 2019
  • This tutorial introduces procedures and methods for performing structural equation modeling using R. To do this, we present advanced analysis methods based on structural equation model such as mediation effect analysis, moderation effect analysis, moderated mediation effect analysis, and multiple-group analysis with R program code using R lavaan package that supports structural equation modeling. R is flexible and scalable, unlike traditional commercial statistical packages. Therefore, new analytical techniques are likely to be implemented ahead of any other statistical package. From this point of view, R will be a very appropriate choice for applying new analytical techniques or advanced techniques that researchers need. Considering that various studies in the social sciences are applying structural equations modeling techniques and increasing interest in open source R, this tutorial is expected to be useful for researchers who are looking for alternatives to existing commercial statistical packages.

Recent Reseach in Simulation Optimization

  • 이영해
    • Proceedings of the Korea Society for Simulation Conference
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    • 1994.10a
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    • pp.1-2
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    • 1994
  • With the prevalence of computers in modern organizations, simulation is receiving more atention as an effectvie decision -making tool. Simualtion is a computer-based numerical technique which uses mathmatical and logical models to approximate the behaviror of a real-world system. However, iptimization of synamic stochastic systems often defy analytical and algorithmic soluions. Although a simulation approach is often free fo the liminting assumption s of mathematical modeling, cost and time consiceration s make simulation the henayst's last resort. Therefore, whenever possible, analytical and algorithmica solutions are favored over simulation. This paper discussed the issues and procedrues for using simulation as a tool for optimization of stochastic complex systems that are dmodeled by computer simulation . Its emphasis is mostly on issues that are speicific to simulation optimization instead of consentrating on the general optimizationand mathematical programming techniques . A simulation optimization problem is an optimization problem where the objective function. constraints, or both are response that can only be evauated by computer simulation. As such, these functions are only implicit functions of decision parameters of the system, and often stochastic in nature as well. Most of optimization techniqes can be classified as single or multiple-resoneses techniques . The optimization of single response functins has been researched extensively and consists of many techniques. In the single response category, these strategies are gradient based search techniques, stochastic approximate techniques, response surface techniques, and heuristic search techniques. In the multiple response categroy, there are basically five distinct strategies for treating the responses and finding the optimum solution. These strategies are graphica techniqes, direct search techniques, constrained optimization techniques, unconstrained optimization techniques, and goal programming techniques. The choice of theprocedreu to employ in simulation optimization depends on the analyst and the problem to be solved. For many practival and industrial optimization problems where some or all of the system components are stochastic, the objective functions cannot be represented analytically. Therefore, modeling by computersimulation is one of the most effective means of studying such complex systems. In this paper, after discussion of simulation optmization techniques, the applications of above techniques will be presented in the modeling process of many flexible manufacturing systems.

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Design Techniques for Reducing Cogging Torque in Permanent Magnet Flux Switching Machine

  • Wang, Daohan;Wang, Xiuhe;Jung, Sang-Yong
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.361-364
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    • 2013
  • Permanent magnet flux switching motor (PMFSM) is a novel double salient machine which employs PMs instead of field winding for excitation. PMFSM contains only one set of armature winding, thereby features simple control strategy, low cost power inverter and substantial high efficiency. Due to the unique double salient structure and operation principle, the generated cogging torque in PMFSM is critical and quite different compared to the traditional PM machines. This paper presents and investigates various design techniques for reducing cogging torque in PMFSM. Firstly, an analytical model is proposed to study the influence of different methods on cogging torque. Then the optimal design parameters for minimizing cogging torque are determined by the analytical model, which significantly reduces the computational efforts. At last, the cogging torque with different design approaches are simulated by FEA along with the average output electromagnetic torque, which validates the analysis above.

Evaluation of Analytical Method for Determination of Potassium in Tobacco Leaf (담배 엽 중 칼륨 분석법의 평가)

  • Cho Sung-Eel;Kim Mi-Ju;Kim Sang-Un;Kim Yong-Ha;Min Young-Keun
    • Journal of the Korean Society of Tobacco Science
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    • v.28 no.1
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    • pp.51-57
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    • 2006
  • This study was carried out to improve and evaluate the analytical method for determination of potassium in tobacco leaf by various pre-treatment techniques. The time requirment of various pre-treatments was about 10 hour for dry ashing and 6 hour for microwave digestion and 3 hour for sonication. The results of recover in both pre-treatment techniques, microwave digestion and sonication, is greater than 85 % stably with reproducibility(RSD %) on replicates of less than 3 %. However the mean values for microwave digestion were lower than certified standard value of NlST SRM. Compared to the other pre-treatment techniques, analytical results for sonication technique strictly improved the accuracy and precision. In conclusion, the use of the simple sonication technique seems to be efficient for the determination of potassium in tobacco leaf in consideration for both the accuracy and reproducibility.

NEAR INFRARED TRANSFLECTANCE SPECTROSCOPY (NIRS) IN PHYTOCHEMISTRY

  • Huck, C.W.;W.Guggenbichler;Bonn, G.K.
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.3114-3114
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    • 2001
  • During the last years phytochemistry and phytopharmaceutical applications have developed rapidly and so there exists a high demand for faster and more efficient analysis techniques. Therefore we have established a near infrared transflectance spectroscopy (NIRS) method that allows a qualitative and quantitative determination of new polyphenolic pharmacological active leading compounds within a few seconds. As the NIR spectrometer has to be calibrated the compound of interest has at first to be characterized by using one or other a combination of chromatographic or electrophoretic separation techniques such as thin layer chromatography (TLC), high performance liquid chromatography (HPLC), capillary electrophoresis (CE), gas chromatography (GC) and capillary electrochromatography (CEC). Both structural elucidation and quantitative analysis of the phenolic compound is possible by direct coupling of the mentioned separation methods with a mass spectrometer (GC-MS, LC-MS/MS, CE-MS, CEC-MS) and a NMR spectrometer (LC-NMR). Furthermore the compound has to be isolated (NPLC, MPLC, prep. TLC, prep. HPLC) and its structure elucidated by spectroscopic techniques (UV, IR, HR-MS, NMR) and chemical synthesis. After that HPLC can be used to provide the reference data for the calibration step of the near infrared spectrometer. The NIRS calibration step is time consuming, which is compensated by short analysis times. After validation of the established NIRS method it is possible to determine the polyphenolic compound within seconds which allows to raise the efficiency in quality control and to reduce costs especially in the phytopharmaceutical industry.

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Study on the Application of RAMS for Rolling Stock (철도차량 RAMS 적용에 관한 연구)

  • Oh, Ji-Eun;Kang, Chan-Yong;Kim, Chul-Ho
    • Proceedings of the KSR Conference
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    • 2004.06a
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    • pp.206-212
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    • 2004
  • This paper is application of System Assurance(SA) for the rolling stock. As railway systems become more complex, design teams are increasingly under pressure to deliver, design solutions, which integrate both technical and Systems Assurance(SA). Systems Assurance is the application of management methods and analysis techniques to ensure that a design meets Reliability, Availability, Maintainability and Safety (RAMS) criteria. It should be clearly understood that the intent of System Assurance is not just to provide analytical techniques as a metric on performance, but more importantly it should provide a management tool with which to co-ordinate and assure the whole design. System Assurance encompasses the ongoing requirement to consider safety, and RAM through each stage of a Project, from feasibility study through to commissioning and operation. If System Assurance is undertaken properly at feasibility study at the design stages of a Project, the benefits of such analyses can be significant in identifying potential problems early enough for action to be taken before manufacture or installation. At commissioning, RAMS demonstration activities are undertaken to validate the predictive and analytical techniques undertaken during the design.

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