• Journal of Pharmaceutical Investigation
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• v.18 no.4
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• pp.175-180
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• 1988

The role and effect of aluminum tristearate in microencapsulation were investigated based on the dispersion system of ethambutol hydrochloride in acetone-liquid paraffin. Eudragit RS was used as a wall-forming material. Eudragit RS microcapsules prepared using aluminum tristearate were uniform, free-flowing particles. The phase diagram of ethambutol hydrochloride-Eudragit RS-aluminum tristearate indicated that spherical microcapsules ranging from 250 to 1400 ${\mu}m$ in diameter could be prepared only in a very limited region. Instrumental analysis using an energy dispersive-type X-ray microanalyser and a scanning electron microscope showed that aluminum tristearate was localized near the surface of microcapsules. From these results, it was presumed that aluminum tristearate reduced the phase tension between Eudragit microcapsules and liquid paraffin. The dissolution rates of ethambutol hydrochloride from Eudragit RS microcapsules were consideraly lower than those from ethambutol hydrochloride powders and decreased as the amount of aluminum tristearate decreased.

• Transactions of Materials Processing
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• v.27 no.2
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• pp.87-92
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• 2018

Auto industries have tried to employ lightweight alloys to improve the fuel efficiency of manufactured vehicles, as the environmental concern becomes an important issue. Even though the aluminum alloy is one of the most appropriate lightweight alloys for auto parts, the low formability of an aluminum alloy has been an obstacle to its application. In order to resolve the low formability problem, a recent study (Lee et al., 2017 [1]) showed that the infrared (IR) local heat treatment can improve the formability with a reduction of heating energy. However, the aforementioned study was limited to only a linear line heating. Since many of the available auto parts as applicable to vehicle manufacturing have a curved line shape, the heating experiments for a curved line should be studied. The possibility of building IR lamps having complex shapes is an advantage of the IR lamp, since it can control the heating shape. This work conducted the IR local heat treatment for the curved line. The experimental results show that the IR local heat treatment can improve the formability of the aluminum alloy for curved line. Additionally, it is shown that the IR local heat treatment also reduces the heating energy when it is compared with the furnace heating which heats a blank as a whole. A numerical simulation with a stress-based forming limit diagram also supports the experimental results.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2002.05a
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• pp.44-47
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• 2002

In order to make a doubly curved sheet metal effectively, a sheet metal forming process has been developed by adopting the flexibility of the incremental forming process and the principle of bending deformation which causes slight deformation to thickness. The developed process is an unconstrained forcing process with no holder. For this study, the experimental equipment is set up with the roll set which consists of two pairs of support rolls and one center roll. In the experiments using aluminum sheets and FEM simulation, it is found that the curvature of the formed sheet metal is determined by controlling the distance between supporting rolls in pairs and the forming depth of the center roll. The FEM simulation of the forming process using the roll set along the one path shows the distributions of the curvatures in two directions along the path, and gives information about the characteristics of the proposed forming process.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.26 no.4
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• pp.410-417
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• 2017

Hydro-forming is being employed increasingly to realize lightweight vehicular parts. The bumper beam produced by this process weighs 30% less than the conventional products with equal stiffness. However, hydro-forming involves complex parameters to obtain the target geometry and low residual stress. Parametric studies are conducted using finite element analysis to obtain optimized process conditions. Through these numerical approaches, the internal and holding pressures and feeder forward stroke along the extruded direction are optimized to achieve low residual stress and to minimize springback. The numerical results are verified by experimental observations made by employing a three-dimensional laser scanner. The numerical and experimental results are compared in terms of the springback. Both results show similar tendencies.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.292-294
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• 2006

The aluminum Subframe for automobile chassis part was developed using hybrid process, i.e. extruforming, press stamping and MIG welding. To achieve a 30 % weight reduction compared with convensional steel subframe keeping satisfactory performance, the design of cross-section of extruforming part was introduced, then forming simulation was performed and the final design was determined. In addition, we tried to estibilish optimun aluminum welding conditions for good penetration depth and few pore defect, finally the prototype of aluminum subframe was assembled using MIG welding method. Furthermore, we will adapt this technology to mass production and apply to the other chassis parts.

• Proceedings of the IEEK Conference
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• 2001.10a
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• pp.173-178
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• 2001

The materials processing factors such as remelting and casting, heat treatment and microstructure, sheet rolling and can body forming in the aluminum can-to-can recycling procedure have been investigated. Aluminum used beverage can(UBC) was remelted together with virgin aluminum. The ceramic filter was used during casting to remove large impurities. As-cast microstructure was composed of large intermetallic compound (mainly $\beta$ -phase) distributed in the aluminum matrix. By heat treatment, $\beta$ -phase was transformed to $\alpha$ -phase which was also formed from $Mg_2$Si particles. The heat treated ingots were hot-rolled at 48$0^{\circ}C$ and cold-rolled to thin sheets. Can making from this thin sheets was successful and earing was measured after can making. There was a critical cold reduction rate for minimum earing. Some cracks were initiated from the impurity particles which was not removed during filtering.

• YAKHAK HOEJI
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• v.21 no.2
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• pp.101-109
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• 1977

The effect of humidity on the aging process of hydrous aluminum oxide prepared by the reaction of aluminum chloride and sodium bicarbonate solution at pH 7.8, which was then kept in various atmosphere under relative humidity at 37.deg. was observed by the measurements of acid consuming capacity, X-ray diffraction and IR absorption. The humidity was one of the important factors influencing the aging process of hydrous aluminum oxide during storage. The higer the humidity, the more was accelerated age, crystalize and loss in acid reactivity. Depending on the humidity, the aging product was different, especially, in the case of up to the relative humidity of 72%, it forming bayerite. On the other hand, the hydrous aluminum oxide aged below the relative humidity of 50% was still amorphous even after 120 days storage. When hydrous aluminum oxide was aged under higher humidity, definite IR absorption bands develop as the hydroxys become part of an ordered structure, and it showed their characteristic absorption band around 1630 and 1060 cm$^{-1}$.

• The Korean Journal of Ceramics
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• v.3 no.4
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• pp.269-273
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• 1997

Chemical composition of cement powder influences the setting time and early compressive strength development. The setting time increases as the amounts of zinc oxide and magnesium oxide are increased. For one day compressive strength development, a cement powder with a composition 90% ZnO, 8% MgO and 2% silica resulted in the highest strength (greater than 1, 090 kg/$\textrm{cm}^2$). Cement-forming liquids also need to be buffered, with both aluminum and zinc ions, for a good consistency and a higher strength of the zinc phosphate cement. These liquids control the setting reactions.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1996.03a
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• pp.172-184
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• 1996

Superplastic forming of thin sheet into complex shape is an important manufacturing process especially in aerospace industry. The main interest in modeling the superplastic forming process is to predict the forming pressure cycle to maintain optimum strain rate and the resulting thickness distribution. Many researchers have attemped to model superplastic forming using the various techniques including finite element method. But in most of their researches have disregarded the strain hardening effect which which occurs in several superplastic materials. In this study ABAQUS finite element code was used for prediction of process variables for axisymmetric cup forming of Supral 100 and 7075Al alloys considereing strain hardening. The performance of numerical results were compared with the experimental results.

• Transactions of Materials Processing
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• v.23 no.2
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• pp.116-121
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• 2014

Low pressure die casting and flow forming have been successfully used to produce sound road wheels from magnesium alloy AM80. In the current study, high speed compression testing was initially conducted to simulate the flow forming of a Mg wheel. Subsequently the flow forming was simulated with "Forge$^{TM}$", an FEM software package. On the basis of flow forming simulations, the flow forming of the Mg wheel was performed under different conditions. For the flow forming experiments, the preform castings were made by low pressure die casting from AM80, a commercial magnesium alloy. In flow forming of the magnesium preform wheel, the flow forming of the Mg wheel was successfully accomplished when the feed rate was less than half that for the forming of an aluminum road wheel. The reduction in feed rate was 52%. Finally, a comparison with the flow forming simulations was made.