• Journal of the Korean institute of surface engineering
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• v.39 no.5
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• pp.235-239
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• 2006

The aluminum nitride(AlN) layer on Al7075 substrate has been formed through nitrogen ion implantation process. The implantation process was performed under the conditions : 100 keV energy, total ion dose up to $2{\times}10^{18}\;ions/cm^2$. XRD analysis showed that aluminum nitride layers were formed by nitrogen implantation. The formation of Aluminum nitride enhanced surface hardness up to 265HK(0.02 N) from 150HK(0.02 N) for the unimplanted specimen. Micro-Knoop hardness test showed that wear resistance was improved about 2 times for nitrogen implanted specimens above $5\;{\times}\;10^{17}\;ions/cm^2$. The friction coefficient was measured by Ball-on-disc type wear tester and was decreased to 1/3 with increasing total nitrogen ion dose up to $1\;{\times}\;10^{18}ions/cm^2$. The enhancement of mechanical properties was observed to be closely associated with AlN formation. AES analysis showed that the maximum concentration of nitrogen increased as ion dose increased until $5\;{\times}\;10^{17}\;ions/cm^2$.

• Journal of the Korean Society for Precision Engineering
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• v.17 no.7
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• pp.141-146
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• 2000

A flexible tool is developed for automatic finishing of curved surfaces without any complicated control technique on three-axes machining center. The tool is made of thermosetting polyurethane elastomer on the surface of which aluminum oxide abrasives are mounted. Performance and durability of the tool are examined by finishing ball-end milled surfaces of high-alloyed tool steel. It is demonstrated that the tool removes cusp successfully without changing overall surface shape in relatively short time.

• Journal of the Korean Society for Precision Engineering
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• v.20 no.5
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• pp.156-163
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• 2003

In order to investigate the possibility of punching process of brittle material by ball impact, the effects of sealing materials about impact damage of soda-lime glass by small spheres were evaluated experimentally. The using of sealing materials in the development of perfect cone crack was more effective than no using of sealing materials. At the sealing materials condition, in the case of 5mm-thick specimen, Copper and PMMA sealing were more effective in producing a perfect cone formation than the other sealing materials. And in the case of 8mm-thick specimen, Aluminum sealing was most effective in producing a perfect cone formation. The impact velocity range over which perfect cones were formed was influenced by both the thickness of specimen and sealing materials. By a proper selection of sealing materials, the application fur industrial technology for hole (or nozzle) punching process of brittle materials is expected.

• Journal of the Korean Society of Industry Convergence
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• v.16 no.3
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• pp.85-93
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• 2013

The MCT has been most extensively used in the machining. In particular, the ball endmill has been mainly adopted for finishing on the free- form surface. The advancement of CAD/CAM software has made it possible to develop various cutting pattern methods and to create diverse tool routes. Therefore, the current research made an attempt to find the optimal cutting pattern among the seven cutting patterns (i.e., Follow Periphery, Zig, Zig Zag, Concentric Zig, Concentric Zig Zag, Radial Zig, Radial Zig Zag) when aluminium 6000 series were machined by the ball endmill. The optimal pattern was found by comparing different shapes and surface roughness produced by the seven patterns. The current research found that each cutting pattern produced its own unique geometric features on the machined surface. It was found that the Radial Zig cutting pattern produced the lowest roughness on the flat surfaces. The Radial Zig Zag cutting pattern was found to produce the most accurate free-form surface. Finally, the most efficient cutting pattern in terms of machining time turned out to be the Follow Periphery.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2002.11a
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• pp.47-50
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• 2002

ZnO nanowires were coated conformally with aluminum oxide ($Al_{2}O_{3}$) material by atomic layer deposition (ALD). The ZnO nanowires were first synthesized on a Si (100) substrate at $1380^{\circ}C$ from ball-milled ZnO powders by a thermal evaporation procedure with an argon carrier gas without any catalysts; the length and diameter of these ZnO nanowires are $20\sim30{\mu}m$ and $50{\sim}200$ nm, respectively. $Al_{2}O_{3}$ films were then deposited on these ZnO nanowires by ALD at a substrate temperature of $300^{\circ}C$ using trimethylaluminum (TMA) and distilled water ($H_{2}O$). Transmission electron microscopy (TEM) images of the deposited ZnO nanowires revealed that 40nm-thick $Al_{2}O_{3}$ cylindrical shells surround the ZnO nanowires.

• Journal of Powder Materials
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• v.27 no.3
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• pp.203-209
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• 2020

The automotive industry has focused on the development of metallic materials with high specific strength, which can meet both fuel economy and safety goals. Here, a new class of ultrafine-grained high-Mn steels containing nano-scale oxides is developed using powder metallurgy. First, high-energy mechanical milling is performed to dissolve alloying elements in Fe and reduce the grain size to the nanometer regime. Second, the ball-milled powder is consolidated using spark plasma sintering. During spark plasma sintering, nanoscale manganese oxides are generated in Fe-15Mn steels, while other nanoscale oxides (e.g., aluminum, silicon, titanium) are produced in Fe-15Mn-3Al-3Si and Fe-15Mn-3Ti steels. Finally, the phases and resulting hardness of a variety of high-Mn steels are compared. As a result, the sintered pallets exhibit superior hardness when elements with higher oxygen affinity are added; these elements attract oxygen from Mn and form nanoscale oxides that can greatly improve the strength of high-Mn steels.

• Journal of the Korean Society for Heat Treatment
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• v.3 no.2
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• pp.32-36
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• 1990

For the accurate measurements of hardness in a material, it is necessary to have a thorough understanding of the effects of test variables on the accuracy of hardness value. For the rebound hardness test, major test variables are the radius of hammer ball tip, type of backing materials, size and roughness of the specimen. In this study, effects of these variables on Equo-Tip hardness value were investigated. Hardness measurements were carried out using WC balls with various sizes of worn-ot zone. The sample materials chosen for the experiments were commercial standard hardness blocks and SM45C steel bars subjected to either normalization or quench and temper treatments. As backing materials, aluminum, steel and rubber plates were used in all the experiments. Experimental results show that for the accurate measurements of Equo-tip hardness, it is necessary to use the hammer ball with a worn-out zone parameter of less than 0.23, and the recommended minimum thickness and width of the specimen are 25mm and 70mm, respectively. Further for the surface preparation, the specimens need to be polished with an emery paper of No. 400 or finer, and for the backing matrials, it is recommended to use steels or rubbers.

• Journal of the Korean Ceramic Society
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• v.31 no.8
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• pp.893-901
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• 1994

In this study, AlN powder of fine particle size and of high purity was synthesized by the carbothermal reduction-nitridation of monodisperse, spherical Al(OH)3 which had been prepared by sol-gel method using Al(O-sec-C4H9)3 as the starting material. Depending on the mixing order and kinds of reducing agents, the optimum condition for the preparation of AlN was determined as follows. AlN single-phase was produced by the carbothermal reduction-nitridation of (1) Benzene-washed Al(OH)3 and the reducing agent, carbon, which was mixed in a ball mill: for 5 hours at 140$0^{\circ}C$ under NH3 atmosphere; (2) The mixture prepared by hydrolysis of alkoxide solution into which carbon had been dispersed beforehand: for 5 hours at 135$0^{\circ}C$ ; (3) Al(OH)3 Poly(furfuryl alcohol) composite powder: for 2.5 hours at 135$0^{\circ}C$; (4) The mixture of Al(OH)3 and polyacrylonitrile: for 5 hours at 140$0^{\circ}C$. Addition of CaF2 increased the nitridation rate when carbon or polyacrylonitrile was used as the reducing agent; but it had no effect on the nitridation rate when furfuryl alcohol was used as the reducing agent.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2002.05a
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• pp.852-855
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• 2002

In order to investigate the fracture behaviors(penetration modes) and resistance to penetration during ballistic impact of surface hardening treated Aluminum, Titanium alloy laminates, ballistic tests were conducted. In this paper, Anodized Al 5083-H131 alloy laminates and nitrified Ti (Gr.2) alloy laminates were used to achieve higher surface hardness. Surface hardness test were conducted using a Micro victor's hardness tester and thickness of surface hardening treated specimens was measured by video microscope. Resistance to penetration is determined by the protection ballistic limit($V_50$), a statistical velocity with 50% probability far complete penetration. Fracture behaviors and ballistic tolerance, described by penetration modes, are respectfully observed at and above ballistic limit velocities, as a result of $V_50$ test and Projectile Through Plates (PTP) test methods. PTP tests were conducted with $0^{\circ}$ obliquity at room temperature using 5.56mm ball projectile. $V_50$ tests with $0^{\circ}$ obliquity at room temperature were conducted with projectiles that were able to achieve near or complete penetration during PTP tests.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1997.10a
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• pp.183-190
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• 1997

The wear behaviors of $Al_2O_3-40%TiO_2$ deposited on casting aluminum alloy(ASTM A356) by plasma spray against SiC ball have been investigated experimentally. Friction and wear tests are carried out at room temperature. The friction coefficient of $Al_2O_3-40%TiO_2$ coating is lower than that of pure $Al_2O_3$ coating(APS). It is found that low friction correspond to low wear and high friction to high wear in the experimental result. The thickness of $Al_2O_3-40%TiO_2$ coatings indicated the existence of the optimal coating thickness. It is found that a voids and porosities of coating surface result in the crack generated. As the tensile stresses in coating increased with the increased friction coefficient. The columnar grain of coating will be fractured to achieve the critical stress. It is found that the cohesive of splats and the porosity of surface play a role in wear characteristics. It is suggested that the mismatch of thermal expansion of substrate and coating play an important role in wear performance. Tensile and compressire under thermo-mechanical stress may be occurred by the mismatch between thermal expansion of substrate and coating. This crack propagation above interface is observed in SEM.