• Title/Summary/Keyword: Alumina coating

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Preparation of Cu-Al$_2$O$_3$ Composite Powder in the Aqueous Solution by Ha Gas Reduction (수소환원법에 의한 수용액 중 Cu-Al$_2$O$_3$ 복합분말제조)

  • 이종현
    • Journal of Powder Materials
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    • v.4 no.2
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    • pp.106-112
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    • 1997
  • $Cu-Al_20_3 $ composite powders were prepared by hydrogen reduction of $Cu^{2+}$ from ammoniacal copper sulfate solution on alumina core using autoclave. The copper reduction rate and the properties of copper layer were investigated using Scanning Electron Microscope(SEM), X-ray diffractometer, size and chemical analyzers. The reduction rate of $Cu^{2+}$ showed the maximum value when the molar ratio of [$NH_3$]/[$Cu^{2+}$] was 2. In order to prevent the agglomeration of Cu powder and ethane reduction rate, $Fe^{2+}$ and anthraquinone which act as catalysis were added in the solution. Catalysis was effectively chanced with the addition of two elemerts at a time. Optimum conditions obtained in this study were hydrogen reduction temperature of 205$^{\cire}C$, stirring speed of 500 rpm and hydrogen partial pressure of 300 psi. Obtained $Cu-Al_20_3 $ composite Powders were found to have the uniform and continuous copper coating layer of nodule shape with 3~5 $\mu$m thickness.

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Electronic properties of PZT(20/80) thick film and PZT(80/20) thin film multilayer with variation of sintering temperature (다층 PZT(20/80)후막과 PZT(80/20)박막의 소결온도에 따른 전기적 특성)

  • Noh, Hyun-Ji;Lee, Sung-Gap;Park, Sang-Man;Bae, Seon-Gi
    • Proceedings of the KIEE Conference
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    • 2006.07d
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    • pp.2209-2210
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    • 2006
  • In this paper, PZT(20/80) thick films were fabricated by the screen-printing method. And the PZT(80/20) coating solution was synthesized by the sol-gel method. PZT(20/80) thick films were screen-printed on the alumina substrates. PZT(80/20) thin film was spin-coaled on the PZT(20/80) thick films to obtain densification. And the structural and electrical properties of PZT thick films were investigated with variation of sintering temperature. The PZT specimen sintered at $650^{\circ}C$ showed good relative dielectric constant of 219 and dielectric loss of 2.45%. Also the remanent polarization and the coercive field wore 16.48 ${\mu}C/cm^2$ and 35.48kV/cm, respectively.

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Electronic properties of PZT(20/80) thick film and PZT(80/20) thin film multilayer with variation of sintering temperature (다층 PZT(20/80)후막과 PZT(80/20)박막의 소결온도에 따른 전기적 특성)

  • Noh, Hyun-Ji;Lee, Sung-gap;Park, Sang-Man;Bae, Seon-Gi
    • Proceedings of the KIEE Conference
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    • 2006.07a
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    • pp.577-578
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    • 2006
  • In this paper, PZT(20/80) thick films were fabricated by the screen-printing method. And the PZT(80/20) coating solution was synthesized by the sol-gel method. PZT(20/80) thick films were screen-printed on the alumina substrates. PZT(80/20) thin film was spin-coated on the PZT(20/80) thick films to obtain densification. And the structural and electrical properties of PZT thick films were investigated with variation of sintering temperature. The PZT specimen sintered at 650f showed good relative dielectric constant of 219 and dielectric loss of 2.45%. Also the remanent polarization and the coercive field were 16.48${\mu}C/cm^2$ and 35.48kV/cm, respectively.

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Dense Ceramic-metal Composite Inorganic Membranes for Oxygen Separation (산소 분리를 위한 무공성 세라믹- 금속 복합 무기막)

  • 김진수
    • Proceedings of the Membrane Society of Korea Conference
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    • 2002.05a
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    • pp.35-41
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    • 2002
  • Dense oxygen ionic conducting materials can be used for oxygen separation membranes at high temperatures. However, they show relatively low permeation flux because of their large resistances. To reduce resistances and improve the oxygen permeation flux, thin dense yttria-stabilized-zirconia (YSZ)/Pd composite dual-phase membranes were fabricated by a new approach that combines the reservoir method and chemical vapor deposition (CVD). A thin porous YSZ layer was coated on a porous alumina support by dip-coating the YSZ suspension. A continuous Pd phase was formed inside pores of the YSZ layer by the reservoir method. The residual pores of the YSZ/Pd layer were plugged with yttria/zirconia by CVD to ensure the gas tightness of the membranes. The oxygen permeation fluxes through these composite membrane were 2.0$\times$10$^{-8}$ mol/cm$^2$.s and 4.8$\times$10$^{-8}$ mol/cm$^2$.s at 105$0^{\circ}C$ when air and oxygen were used as the permeate gases, respectively. These oxygen permeation values are about 1 order of magnitude higher than those of pure YSZ membranes prepared under similar conditions.

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Effects of Intermediate Layer in DLC Thin Film on Al2O3 for Improvement of High Temperature Strength

  • Ok, Chul-Ho
    • Transactions on Electrical and Electronic Materials
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    • v.8 no.3
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    • pp.125-130
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    • 2007
  • DLC coating on ceramics is very useful for manufacturing the materials with hardness and low friction. Adhesion of DLC thin film on ceramics, on the other hand, is usually very weak. Adhesion of DLC film depends on many parameters such as contamination and chemical bonding between thin film and substrate. In this study, adhesion of DLC film on ceramics was improved by the intermediate layer when the plasma immersion ion deposition (PIID) technique was applied. It is found that the chemical composition and the thickness of intermediate layer have significantly an effect on the adhesion of DLC thin film on $Al_2O_3$.

Low temperature UV-assisted rapid thermal processing of (Ba,Sr)$TiO_3$ thin films (저온에서 (Ba,Sr)$TiO_3$ 박막의 UV를 이용한 RTP에 관한 연구)

  • Cho, Kwang-Hwan;Kang, Chong-Yun;Yoon, Seok-Jin;Lee, Young-Pak
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.234-234
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    • 2008
  • Chemically homogeneous $Ba_{0.6}Sr_{0.4}TiO_3$ (BST) sols were synthesized using barium acetate, strontium acetate, and titanium isoproxide as starting materials. BST thin films of thickness 340 nm were deposited on Pt/$TiO_2/SiO_2$/Si and alumina substrates using spin coating method. The technique used for the processing of these films was Ultraviolet (UV) sol-gel photoannealing, using phto-sensitivity precursor solutions and UV-assisted rapid thermal processing(UV-RTP). The crystallization behaviour of the BST sols and thin films was studied by differential thermal analysis (DTA) and X-ray diffraction (XRD). Variation of permittivity and dielectric loss were measured in LCR-meter, model HP 4394A.

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Study on Relation between Surface Roughness and Heat Absorption Capability of Materials for Solar Collector (태양열 집열기용 소재의 표면 거칠기와 흡열성능의 관계 연구)

  • Chun, Tae-Kyu;Ahn, Young-Chull
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.12 no.5
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    • pp.76-85
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    • 2013
  • This study was carried out to investigate the relation between surface roughness and heat absorption capability of materials for solar collector. For this purpose, 3 kinds of materials (copper, aluminum, iron), 5 kinds of surface roughness (scrubber, alumina sand #80, #200, #400, glass bead) and 2 kinds of surface treatment (black chrome plating, copper black coating) were used for finding optimal conditions to apply solar collector. As the results, it was confirmed that the optimal relations between surface roughness and surface treatment as well as optimal materials were necessary. Further, heat absorption capability was showed good results in cases of copper materials, glass bead and black chrome plating.

Red Mud를 이용한 토양 및 슬러지내 중금속 제거 특성

  • 김이태;배우근;김우정;정원식
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2003.09a
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    • pp.73-77
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    • 2003
  • Red mud is a waste material formed during the production of alumina when the bauxite ore is subjected to caustic leaching. It is a brick-red colored highly alkaline (pH 10-12) sludge containing mostly oxides of iron, aluminum, titanium, and silica. Red mud, due to its high aluminum, iron, and calcium contents, has been suggested as a cheap adsorbent for removal of toxic metals (e.g., As, Cr, Pb, Cd) as well as for water or wastewater treatment. The basic advantage of red mud is its versatility in application. This study was conducted to evaluate the effect of red mud on stabilization and fixation of heavy metals (such as Pb, Cu, C $r^{6+}$, Cd, Zn) contained in the Al-coating sludge and soil. The results showed that the concentration of heavy metals leached from the treated sludge and soil was low, meeting the regulatory permit level.

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Development of Electromagnetic Wave Absorbers Using Sendust for a Portable Phone (Sendust를 이용한 휴대전화용 전파흡수체의 개발)

  • Choi, Jung-Hyun;Kim, Dong-Il;Song, Jae-Man;Jung, Jae-Hyun
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2005.06a
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    • pp.429-434
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    • 2005
  • In this paper, we investigated EM wave absorption property of EM wave absorbers prepared with sendust. The EM wave absorbers have good EM wave absorption properties in 1 GHz ${\sim}$ 3 GHz. On the other hand, the absorption band of the EM wave absorber coated with $Al(OH)_3$ larger than non-coated one. Pulverization effect of sendust on EM wave absorption properties was also investigated.

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An Experimental Study on the Corrosion Behavior in the Steel Meterial Embedded in Cement Mortar with Metal Spray Method (금속용사피막을 갖는 강재의 시멘트 모르타르 내 부식거동에 관한 실험적연구)

  • Park, Jang-Hyun;Kim, In-Soo;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.05a
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    • pp.105-106
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    • 2017
  • The metal spray method, one of the surface anti-corrosion methods to prevent the corrosion of the steel material, does little effects on the material, while it can be used on a wider surface. However, metal spraying is used only in a limited environment, and research on the case of using with concrete is lacking. The purpose of this study was to observe the corrosion behavior of steels with metal spray coatings in concrete using electrochemical methods And to evaluate the performance of the method according to the type of metal used in the metal spray. As a result, the Al metal spray coating showed the best performance, because Aluminum is oxidized in the cement mortar and forms alumina oxide film.

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