• Korean Journal of Materials Research
• /
• v.9 no.2
• /
• pp.132-138
• /
• 1999

In order to investigate the toughening characteristic by microcrack formation in ceramic composites, $Al_2$O$_3$/(0~20)vol% YAG composites containing equiaxed second grains were fabricated using$ Al_2$$O_3$ during hot-pressing. AE(acoustic emission) measurements have been coupled with fracture toughness experiments of SENB method, to evaluate the microcrack formation and the improvement in fracture toughness of ceramic composites. Formation of microcrack was detected by Ae. The generation of AE events increased with increasing of load when load was applied at specimen. The AE events are generated mainly around at maximum load. Specially, the detected AE evetns of composites are many as compared with monolithic $Al_2$$O_3$. Fracture toughness of composites was improved than that of monolithic alumina. $Al_2$O$_3$/YAG composites exhibit main toughening effects by microcracking, results from mutual coalesence of microcracks being generated under applied load. However, there are few toughening mechanism like microcracking in monolithic alumina.

• Journal of the Korean Ceramic Society
• /
• v.43 no.9 s.292
• /
• pp.515-518
• /
• 2006

The microstructure of $ZrO_2$ toughened $Al_2O_3$ ceramics was carefully controlled so as to obtain dense and fine-grained ceramics, thereby improving the properties and reliability of the ceramics for capillary applications in semiconductor bonding technology. $Al_2O_3-ZrO_2(Y_2O_3)$ composite was produced via Ceramic Injection Molding (CIM) technology, followed by Sinter-HIP process. Room temperature strength, hardness, Young's modulus, thermal expansion coefficient and toughness were determined, as well as surface strengthening induced by the fine grained homogenous microstructure and the thermal treatment. The changes in alumina/zirconia grain size, sintering condition and HIP treatment were found to be correlated.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.32 no.6
• /
• pp.483-489
• /
• 2019

For machine learning techniques, a large amount of high-quality material property data should be accumulated. In this study, several data for an alumina tape casting process were produced with the variables of slurry viscosity, gap size, and coating speed. The alumina tapes were manufactured in the range of 1,000~6,000 cps for slurry viscosity, $300{\sim}1,000{\mu}m$ for gap size, and 0.5~2.0 m/min for coating speed. As a result, the lower the viscosity, coating speed, and gap size, the more pore-free tapes could be manufactured. The viscosity of the slurry limited the minimum thickness of the tape. Green sheets with high packing density were manufactured from the slurry of 100~6,000 cps slurry viscosity, coating speed of 0.5 m/min, and a $300{\sim}500{\mu}m$ gap size.

• Journal of the Microelectronics and Packaging Society
• /
• v.26 no.4
• /
• pp.89-94
• /
• 2019

Glass base sealant is required as a ceramic-ceramic joining material between α-alumina insulation cap and β-alumina electrolyte tube in the development of NaS battery cell package for electrical energy storage system. The fabrication of glass frit by thermal quenching method, phase analysis, particle size analysis, coefficient of thermal expansion and surface roughness according to the glass compositions were analyzed for the fabrication of glass sealing paste for ceramic-ceramic joining. Also, a new evaluation method of the adhesion strength of glass sealant at the small area in ceramic-ceramic joining component was proposed using conventional Dage bond tester that was used to measure the adhesion of solder ball joint.

• Journal of the Korean Ceramic Society
• /
• v.37 no.5
• /
• pp.403-409
• /
• 2000

The permeation characteristics and reclamation efficiency of waste lubricating oil were studied as a function of the types of ceramic composite membranes and the membrane separation process variables. The oil permeability of the TiO2 composite membrane(pore size 0.015 $\mu\textrm{m}$) was directly proportional to the crossflow velocity(0.22∼0.9 m/s) and temperature(150$^{\circ}C$∼200$^{\circ}C$). In the batch concentration process, as the concentration factor increased, both the permeability and the ash content of the permeate decreased. The average ash contents of the total permeate through the A6 alumina membrane(average pore size 0.8$\mu\textrm{m}$), Z1/A6 and Z1/A4(pore size 0.23$\mu\textrm{m}$)/A7(pore size 6$\mu\textrm{m}$) zirconia composite membrances(average pore size 0.07$\mu\textrm{m}$) were about 0.063 wt%, 0.045wt% and 0.08wt% in the region of 1∼2 concentration factor, respectively. The ash content of the mixed permeate through the A6 alumina and zirconia composite membrane was about 0.06 wt% and it can be also reduced to 0.06 wt% in the Z1/A6 membrane and below 0.003 wt% in the TiO2/Z1/A6 membrane. It was concluded that the treated oil obtained from the multi-step membrane separation process could be used as reclaimed lubricating oil as well as reclained fuel oil.

• The Journal of Korean Academy of Prosthodontics
• /
• v.45 no.2
• /
• pp.159-168
• /
• 2007

Statement of problem: Literature showed different results on the durability of bonded ceramic restoration. Purpose: The purpose of this article is to review the effect of surface treatment of ceramics in resin-ceramic bond to get predictable results. Material and method: PubMed data base was utilized to search the articles which were written in English and published in 1986 and 2006. Some electronic published articles which are forthcoming to publish in paper were also included for this review. This review article focused on the effect of acid etching and silane application on the silica based ceramics. The durability of resin-ceramic bonding, the methodology for bond strength test and resin bonding to alumina or zirconia based ceramics were compared in brief at the end of the review. Results and Conclusion: the effect of silane application can be influenced by the contaminations of saliva or solutions. Micromechanical retention by acid etching as well as silane application plays an important role in initial and durable bond strength between resin and ceramic. The use of phosphate modified resin cement following tribochemical silica coating and silane application produced best bond strength for alumina or zirconia based ceramics.

• Journal of Korean Society of Water and Wastewater
• /
• v.22 no.3
• /
• pp.329-336
• /
• 2008

The pilot study was conducted to evaluate the applicability of air flotation(AF) processes combined with biological nutrient removal(BNR) for the retrofitting of conventional wastewater treatment facilities. The BNR system was operated in pre-denitrification and intermittent aeration; developed ceramic membrane diffusers were installed to separate the solid-liquid of activated sludge at the bottom of a flotation tank. Before performing a pilot scale study, the size distribution of microbubbles generated by silica or alumina-based ceramic membrane diffusers was tested to identify the ability of solid-liquid separation. According to the experimental results, the separation and thickening efficiency of the alumina-based ceramic membrane diffuser was higher than the silica-based ceramic membrane diffuser. In a $100m^3/d$ pilot plant, thickened and return sludge concentration was measured to be higher than 15,000mg SS/L, therefore, the MLSS in the bioreactor was maintained at over 3,000mg SS/L. The effluent quality of the AF-BNR process was 4.2mg/L, 3.7mg/L, 10.6mg/L and 1.6mg/L for $BOD_5$, SS, T-N and T-P, respectively. Lastly, it was revealed that the unit treatment cost by flotation process is lower than about $1won/m^3$ compared to a gravity sedimentation process.

• Journal of the Korean Ceramic Society
• /
• v.19 no.2
• /
• pp.115-120
• /
• 1982

The main objective of this work was to study the efTect of pressed density of pellets prepared from an oxide powder on their fired density and to prove experimentally the parabolic relationship proposed by FORD. A-I6 and A-J7 alumina powders. which showed quite dlfrerent powder characteristics but were essentially very reactive powders, were employed, and a series of pelIets weIe pressed in a 1l.2mm diameter hardened steel die with a hydraulic press and a mechanically operated press in order to obtain a wide range of pressed demity. Density ranges from 35 to 65 % theoretical for A-16, and 46 to 66 % theoretical far A-17 were obtained and the highest pressed density achieved using lubricant was 67.8 % theoretical. CompactlOn mechanisms for A-16 and A-I 7 were deduced. Several plots of ($D_F$-$D_P$) against DpjDT showed reasonable parabola and temperature dependence and the maximum density increase occurred when the pressed density was approximately 50% theoretical. The parabolic relationship was confirmed by linear plot of ($D_F$-$D_P$) against (1-$\frac{D_P}{D_T})$).

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.12 no.6
• /
• pp.292-298
• /
• 2002

Densified cordierite matrixes added alumina platelets were studied as a ceramic substrate material having a low thermal expansion coefficient, low dielectric constant and proper strength. Amorphous-type cordierite powders were filled with four kinds of alumina platelet powders in various compositions. All samples were sintered at $1300^{\circ}C$ for 2 h in an air atmosphere. Improved flexural strength of about 80 MPa, low dielectric constant of 5.0 at 1 MHz and low thermal expansion coefficient of $3.5 \times 10^{-6}/^{\circ}C$ were obtained by the control of the microstructure. Isolated micropores were formed in the matrix and the porosity was dependent on the platelet content and size. In the 10 vol% of alumina platelet content, the isolated micropores were 3~8 $\mu \textrm{m}$ in size, and an increase in dielectric constant by adding alumina platelet filler was inhibited by the micropores.

• Journal of the Korean Ceramic Society
• /
• v.36 no.2
• /
• pp.122-129
• /
• 1999

Alumina tapes, having various weight ratios of alumina powder/(alumina+binder+plasticizer), X, and binder / (binder+plsticizer), Y, were prepared and their complex modulus was measured using Micro Fourier Rheometer. As the X and Y ratios increased, Transfer function(TF) magnitude and Transfer function (TF) phase increased and decreased, respectively, indicating that the elastic modulus of the tapes depends on the weight ratios. The temperature dependence of the viscosity of the tapes was visualized by the decreased TF magnitude and the increased TF phase. The Y ratio dependence of the complex modulus related to the glass transition temperature of the tapes and the moduls change by the Y ratio was higher than that by the X ratio within the comperature of the tapes and the modulus changes by the Y ratio was higher than that by the X ratio within the composition range, investigated in the present study. The measurement of the complex modulus of the alumina tapes suggested that the TF phase should be higher that 17$^{\circ}$for the tapes to be utilized for 3-dimensional shaping.