• Bulletin of the Korean Chemical Society
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• 제27권10호
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• pp.1609-1612
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• 2006

The determination of the boron isotopic ratio in solutions was achieved by means of a solid state track detector by using an alpha track. The neutron flux was optimized by using a Cd-foil to find the optimum conditions for counting the number of alpha tracks on the selected solid detector caused by the (n, $\alpha$) nuclear reaction of boron. The home-made multi-dot detector plate was utilized in this study to increase the reproducibility of the measurement by uniformly drying the boron solution within the marked circle area on the detector plate. The experimental results of this study verified that the $^{11}B/^{10}B $ isotopic ratio can be measured by observing the number of alpha tracks for different concentrated standard solutions with various isotopic compositions. This technique was applied to the determination of $^{10}B$ enrichment factor in a biological sample for a boron neutron capture therapy.

• 분석과학
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• 제17권5호
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• pp.434-437
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• 2004

Alpha track technology can provide useful isotopic information of boron in the primary coolant water. In the quantitative analysis using the alpha track analysis, the shape or area of sample on the solid track detector becomes very important, especially for the analysis of liquid samples. In this research, a multi-dot plate has been developed for this purpose. The multi-dot plate provides fixed standard shape of the sample solution that stays inside of the printed circle, and consequently increases the reproducibility of the boron analysis.

• Journal of Radiation Protection and Research
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• 제21권3호
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• pp.167-173
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• 1996

알파선 검출 효율 측정을 위한 고체비적검출기의 교정 방법을 제시하였으며, 제시된 교정 방법을 이용하여 CN-85와 LEXAN의 검출 효율을 측정하였다. $0{\sim}5.5MeV$ 에너지 영역의 알파선에 대한 검출 효율을 측정한 결과 CN-85와 LEXAN이 각각 97%, 57%였다. CN-85가 LEXAN에 비해 검출 효율이 높게 나타난 이유는 알파선에 대한 CN-85의 sensitivity가 LEXAN에 비해 좋을 뿐만 아니라 에너지 의존성이 CN-85가 LEXAN에 비해 낮기 때문인 것으로 분석되었으며, CN-85는 알파선의 유도 에너지가 약 3 MeV, LEXAN은 약 1.8 MeV에서 검출 효율이 최대로 나타났다.

• Journal of Radiation Protection and Research
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• 제2권1호
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• pp.1-8
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• 1977

중성자(中性子) 선량(線量) 측정목적(測定目的)으로 사용(使用)할 Posi필름 고체비적검출기(固體飛跡檢出器)의 알파입자(粒子) 비적검출(飛跡檢出) 효율(效率)과 화학부식(化學腐蝕)에 의(依)한 그의 비적형성(飛跡形成) 최적조건(最適條件)을 실험적(實驗的)으로 결정(決定)하였다. $^{10}B$ 및 $^{27}Al$박(箔)과 posi 필름 고체비적검출기(固體飛跡檢出器)로 이루어진 중성자(中性子) 선량계(線量計)를 제작(製作)하고 이것에 의(依)한 중성자(中性子) 선속밀도(線束密度) 및 선량(線量)의 측정범위등(測定範圍等)을 실험결과(實驗結果)와 이론적(理論的)인 근거하(根據下)에서 산출(算出)하였다. 그 결과(結果) posi 필름 고체비적검출기(固體飛跡檢出器)는 핵분열성(核分裂性) 물질(物質)을 입자방출체(粒子放出體)로 병용(倂用)함이 없이 중성자(中性子) 측정(測定)에 효과적(效果的)으로 응용(應用)될 수 있음이 판명(判明)되었다.

• 분석과학
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• 제17권1호
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• pp.8-15
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• 2004

수용액 시료에 포함된 미량의 보론 함량을 분석하는데 적합한 고체트랙 검출기를 선정하기 위하여 알파복합선원 등을 이용하여 검출능력을 비교 검토하였다. 보론의 알파트랙 검출에는 polycarbonate 재질(Lexan 및 CR-39)과 cellulose nitrate 재질(CN-85 및 LR-115))의 고체트랙 검출기를 사용하였다. 알파입자 방출물질로는 복합알파선원, 금속 우라늄 입자 및 보론 표준용액을 사용하였다. 본 연구에서는 에칭조건 및 중성자 조사조건 등에 따른 검출기의 특성을 비교하였으며, 실험 결과 보론 정량에는 CN-85 검출기가 가장 적합한 것을 알 수 있었다. 또한, 선정된 검출기를 이용하여 수용액 매질에 포함된 미량의 보론을 알파트랙 기입방법으로 측정한 실험결과에 대해 검토하였다.

• Nuclear Engineering and Technology
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• 제38권4호
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• pp.353-358
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• 2006

Alpha track analysis for the determination of the trace amount of alpha emitting nuclides in a very small particle was performed as an efficient and powerful technique during safeguard inspection. Metal particles with well-defined spherical shape, size and isotopic compositions as a reference material were used to correlate the number of tracks or track diameter with an isotopic composition eventually to identify the uranium enrichment in the environmental swipe samples. Slopes in the number of tracks versus the exposure time curve provide a simple insight into the uranium enrichment of an unknown particle. Low enriched uranium metal particles result in slopes still steeper than the depleted or natural uranium metal particles. In addition, a linear relationship between track diameter and particle size Is thought to be a useful first stage analytical tool as an efficient and convenient inspection guide. The significance of the simple linear model was also judged using the usual statistical tests.

• 한국환경보건학회지
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• 제28권5호
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• pp.71-76
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• 2002

A survey of radon concentrations in both indoor and outdoor atmospheres was carried out using EIRM and Cup Monitor for the period of February 1996 to March 1997. EIRM were used to measure the indoor and outdoor radon concentration at five major cities university. Cup Monitor were also used to measure the indoor radon concentrations at shopping store, office building, apartment, hospital and house in Seoul. The mean indoor and outdoor radon concentrations at the five major cities(Seoul, Daegu, Daejon, Cwangiu and Busan) were 24.1 Bq/m$^3$and 8.62 Bq/m$^3$, respectively. The ratio of indoor to outdoor radon concentrations ranged front 1.7 to 3.9. Inspection of its seasonal distribute pattern indicates the enhancement during winter relative to summer, consistently for both indoor and outdoor air. The results of the survey showed that the concentrations in basements were clearly higher than those in usual living/working places.

• Nuclear Engineering and Technology
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• 제49권4호
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• pp.881-885
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• 2017

This work presents a new technique for discriminating between alpha particles of different energy levels. In a first study, two groups of alpha particles emitted from radium-226 and americium-241 sources were successfully separated using a CR-39 microfilm of appropriate thickness. This thickness was adjusted by chemical etching before and after irradiation so that lower-energy particles were stopped within the detector, while higher-energy particles were revealed on the back side of the detector. The number of tracks on the front side of the microfilm represented all alpha particles incident on that side from the two sources. However, the number of tracks on the back side of the microfilm represented only the long-range alpha particles of higher energy that arrived at that side. Therefore, by subtracting the number of tracks on the back side from the number of tracks on the front side, one could easily determine the number of tracks for the short-range alpha particles of lower energy that remained embedded in the microfilm. Discrimination of the two energy levels is thus achieved in a simple, fast, and reliable process.

• Nuclear Engineering and Technology
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• 제50권3호
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• pp.432-438
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• 2018

The occurrence of saturation in the CR-39 detector reduces and limits its detection dynamic range; nevertheless, this range could be extended using spectroscopic techniques and by measuring the net bulk rate of the saturated CR-39 detector surface. CR-39 detectors were irradiated by 1.5 MeV high alpha-particle fluence varying from $0.06{\times}10^8$ to $7.36{\times}10^8\;alphas/cm^2$ from Am-241 source; thereafter, they were etched in a 6.25N NaOH solution at a temperature of $70^{\circ}C$ for different durations. Net bulk etch rate measurement of the 1.5 MeV alpha-irradiated CR-39 detector surface revealed that rate increases with increasing etching time and reaches its maximum value at the end of the alpha-particle range. It is also correlated with the alpha-particle fluence. The measurements of UV-Visible (UV-Vis) absorbance at 500 and 600 nm reveal that the absorbance is linearly correlated with the fluence of alpha particles at the etching times of 2 and 4 hour. For extended etching times of 6, 10, and 14.5 hour, the absorbance is saturated for fluence values of $4.05{\times}10^8$, $5.30{\times}10^8$, and $7.36{\times}10^8\;alphas/cm^2$. These new methods pave the way to extend the dynamic range of polymer-based solid state nuclear track detectors (SSNTDs) in measurement of high fluence of heavy ions as well as in radiation dosimetry.

• 분석과학
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• 제18권4호
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• pp.263-270
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• 2005

핵분열트랙은 우라늄, 플루토늄, 토륨 등의 방사성핵종 분석이나, 리튬이나 붕소와 같이 열중성자와 핵반응을 하는 원소분석에 매우 유용하다. 이 방법은 대기 중의 방사성핵종 분석을 통해 핵무기 실험을 검출한다거나, 우주공간의 중이온에 대한 선량측정이나 운석의 우주선 조사과정 추정, 원자력분야의 핵분열률 측정, 암석의 연대 및 역사를 파악하거나, tracer로 사용하는 등 여러 분야에 적용 가능하다. 현재 원자력연구소에서는 알파트랙기입법을 이용한 미량의 보론 분석이나, 핵분열트랙을 이용한 우라늄 등의 핵물질을 포함한 입자분석에 적용하고 있다. 본 총설에서는 트랙형성의 이론적 배경, 에칭된 트랙을 얻는 실제 과정 및 앞으로의 전망 등에 대해 살펴보았다.