• 제목/요약/키워드: All-solution-process

검색결과 726건 처리시간 0.031초

방전 플라즈마 소결법에 의한 ZnS 나노입자의 소결과 광학적 특성 (Sintering and Optical Properties of ZnS Nanoparticles Sintered by Spark Plasma Sintering)

  • 김창일;김유비;여서영;홍연우;윤지선;박운익;정영훈;조정호;백종후
    • 한국전기전자재료학회논문지
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    • 제30권6호
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    • pp.349-355
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    • 2017
  • Zinc sulphide (ZnS) nanoparticles were fabricated by hydrothermal synthesis at $180^{\circ}C$ for 12 h. Two kinds of ZnS powder (hydrothermal synthesized ZnS and commercial ZnS) were investigated by X-ray diffraction (XRD) and scanning electron microscopy (SEM) for phase and microstructure, respectively. The XRD patterns showed that all ZnS nanoparticles have a sphalerite (cubic) structure. The nanoparticles of two different ZnS powders were sintered by spark plasma sintering. The sintered ZnS were analyzed by XRD, SEM, and FT-IR. We found that the transmittance of the infrared region is highly dependent on the density and crystal structure of sintered ZnS and the purity of the starting ZnS powder.

Composition of Biologically Active Substances and Antioxidant Activity of New Zealand Deer Velvet Antler Extracts

  • Je, Jae-Young;Park, Pyo-Jam;Kim, Eun-Kyung;Kim, Hyun-A;Lim, Dong-Hwan;Jeon, Byong-Tae;Ahn, Chang-Bum
    • 한국축산식품학회지
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    • 제30권1호
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    • pp.20-27
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    • 2010
  • Deer velvet antler was subjected to the extraction process using boiling water at three different temperatures (100, 110 and $120^{\circ}C$) and 70% ethanol solution. Functional components such as uronic acid, sulfated-glycosaminoglycans (sulfated-GAGs) and sialic acid in the extracts were analyzed, and their antioxidant activities were investigated using several in vitro models. Uronic acid and sulfated-GAGs content of each extract significantly decreased with increasing extraction temperature (p<0.05), while the residues obtained from the upper and middle part of the antler had a higher uronic acid content than the residues obtained from the base section. Sialic acid contents were highest in compounds extracted at $110^{\circ}C$, followed by 120 and $100^{\circ}C$. The 70% ethanol extracts also had a high levels of uronic acid content, but not for sulfated-GAGs and sialic acid. All extracts showed good antioxidant ability in a dose-dependant manner, with the $100^{\circ}C$ residue exhibiting the strongest activity compared to the 110 and $120^{\circ}C$ extracts. In relation to the hydroxyl radical scavenging activity and reduction power, the 70% ethanol extract exhibited the strongest activity. Furthermore, the velvet antler extracts inhibited apoptosis in hydrogen peroxide-induced PC-12 cells.

음영처리기법의 비교를 통한 실내공간 조명효과의 예측 (The Prediction of Interior Luminous Effect Through a Comparison of Shading Algorithms)

  • 홍승대;박현장
    • 한국디지털건축인테리어학회논문집
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    • 제5권1호
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    • pp.9-16
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    • 2005
  • In Interior design, light is the most important factor in deciding color, texture and illumination level which are the basic factors of spatial design. To apply rendering technologies on prediction of illuminating effect, it is important to understand and analyse the basic properties of the illumination models that are local illumination model and global illumination model. The illumination models in computer graphics express the factors which determine the surface color, texture and light distribution through the reflection. The purpose of this study is to propose the best way of shading algorithm in interior space provided by the computer, based on the experimental analysis that 5 shading methods are applied to the interior space. The results of this study were as followed. 1) Local illumination models that are Lambert shading, Ground shading and Phong shading are not suitable to the prediction of interior illumination effect. 2) Ray tracing that is global illumination model could be adopted to interior illumination effects. Ray tracing is a very versatile algorithm because of the large range of lighting effects it can model. 3) Neither radiality nor ray tracing offers a complete solution for simulating all interior illumination effects. 4) Radiosity excels at rendering diffuse-to-diffuse inter-reflections and ray tracing excels at rendering specular reflections. By merging both shading techniques, that offers the best of both. Using computer technologies to simulate lighting in preliminary design stage which will provide information for designers and occupants to determine the effect of using artificial light sources at each stage of their design process. Further study in illumination analysis, prediction of illumination effect, and lighting calculation is required as computer media expands.

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住宅 取得시 發生하는 消費者 問題와 對應行動에 관한 硏究 (A Study on the Problems of the Occupants on the Purchasing Housing)

  • 조현경;강순주
    • 가정과삶의질연구
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    • 제10권1호통권19호
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    • pp.139-156
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    • 1992
  • The purpose of this study is to provide basic data for the solution of occupant problems related to the house purchasing. For the purpose, the content of problems and actual conditions of house purchasing are examined. Also the structural analysis of occupant's evaluation of housing purchasing is executed. For these purposes, a survey was conducted using questionnaires. Data analysis was conducted from 263 house owners in Seoul. Major findings of this study can be summarized as follows ; 1) The frequency and the contend of occupation's problems with house purchasing are studied. The rate of housing problem occurrence is 71.2%, so the majority of respondents experience problems. The most common problems are the difference from supplier's description(53.2%). The rate of housing problems occurrence is qenerally high with the houses of mult-housedhold houses and mult-family houses type. 2) There is a significant difference in housing satisfaction extend according to the existence of an housing problem experience. Therefore, it can be inferred that experience of housing problem has an important effects upon the housing satasfaction extent. 3) Occupants' countermoves to the housing problems are examined. Occupants make active regotiation with house suppliers only on the direct damages such as an economical loss or a living difficulty. However, they usually make no countermove at all on the other indirect troubles. House suppliers make correction only when occupants' countermove actively, but refuse to do when occupant's reactions are not active. 4) As a means of countermove, most occupants depend on direct personal regotiation with house suppliers. The rate of using a specialist or public and private consultant is extremely low. 5) Problems with house purchasing and the countermove process of both occupant and house supplier are displayed in the figure(Fig. 4-4).

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저가 탄소섬유용 Lignin/Chlorinated Polyvinyl Chloride 블렌딩 섬유의 제조 및 특성 (Preparation and Characterization of Lignin/Chlorinated Polyvinyl Chloride Blended Fibers for Low-cost Carbon Fiber)

  • 조채현;이상오;강다경;홍성화;강찬규;이재웅
    • 한국염색가공학회지
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    • 제32권2호
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    • pp.111-120
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    • 2020
  • In this study, lignin/chlorinated poly(vinyl chloride)(CPVC) blended fibers have been produced for the development of low-cost carbon fiber. Carbon fiber manufacturing was accomplished through stabilization and carbonization process. The lignin/CPVC blended fibers were prepared by wet spinning method. Dimethylacetamid e(DMAc) and cychlohexanone in a ratio of 5:1(wt%) was employed as co-solvent. The ratio of lignin/CPVC was prepared at 0/10, 1/9, 2/8, 3/7, 4/6, and 5/5(wt%). The spinning solution was extruded at a rate of 0.1 to 0.4ml/min according to the blending ratio. The speed of the rollers was the same for all ratios(draw ratio=1). Analysis of fiber cross-section by scanning eletron microscopy(SEM) showed that as the lignin ratio increased in the same coagulation bath and distilled water, the pore size of the spinning fiber decreased. Therefore, the highest tensile strength of the blending fibers was 6.3±1.2MPa at the 5/5 ratio. The carbon fiber also showed the best tensile strength of 120.78±2.43MPa at 5/5 ratio.

오디오 신호 처리를 위한 초저전력 DSP 프로세서 (Ultra-low-power DSP for Audio Signal Processing)

  • 권기석;안민욱;조석환;이연복;이승원;박영환;김석진;김도형;김재현
    • 한국방송∙미디어공학회:학술대회논문집
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    • 한국방송공학회 2014년도 하계학술대회
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    • pp.157-159
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    • 2014
  • In this paper, we introduce SlimSRP, an ultra-low-power digital signal processor (DSP) solution for mobile audio and voice applications. So far, application processors (APs) have taken charge of all the tasks in mobile devices. However, they have suffered from short battery life problems to deal with complex usage scenarios, such as always-on voice trigger with continuous audio playback. From extensive analysis of audio and voice application characteristics, SlimSRP is designed to relive the performance and power burden of APs. It employs three-issue VLIW architecture, and the major low-power and high-performance techniques include: (1) an optimized register-file architecture friendly for constants generation, (2) a powerful instruction set to reduce the number of register file accesses and (3) a unique instruction compression scheme that contributes to saved memory size and reduced cache miss. An implementation of SlimSRP runs at up to 200MHz and the logic occupies 95K NAND2 gates in Samsung 28LPP process. The experimental results demonstrate that a MP3 decoder application with a 128kbps 44.1kHz input can run at 5.1MHz and the logic consumes only 22uW/MHz.

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$TiO_2$ 담지체에 합성된 Li-Zr 메조포러스 분자체 ; 이산화탄소 흡착 응용 (Synthesis of Li-Zr incorporated mesoporous $TiO_2$ and its application in $CO_2$ adsorption)

  • 말간단 바기아락스미;팽메이메이;푸시파라지 헤마라다;마니 기니쉬;장현태
    • 한국산학기술학회:학술대회논문집
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    • 한국산학기술학회 2010년도 추계학술발표논문집 1부
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    • pp.110-114
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    • 2010
  • Li-incorporated mesoporous $TiO_2$ materials with various pore-sized istributions were synthesized by using triblockcopolymers via a sol-gel process in a queous solution. The properties of the se materials were characterized by HR-TEM, XRD, and BET analysis. All particles have spherical morphology with a diameterrange of $1-3{\mu}m$. The mesoporous $TiO_2$ materials calcined at $400^{\circ}C$ and their specific surface area, average pore size and crystallite sizes were 210 $m^2g^{-1}$, 6.4 nm and 8.8 nm respectively. The Li-incorporated mesoporous $TiO_2$ were tested for $CO_2$ adsorption and its adsorption capacity is 90mg/g. The Li-incorporated mesoporous $TiO_2$ ar eobserved to be thermally stable, recyclable and greens or bent for $CO_2$ capture. The effect of bimetallic $ZrLiTiO_2$ is also studied for $CO_2$ adsorption.

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Photocatalytic Oxidation of 2-Mercaptoethanol to Disulfide using Sb(V)-, P(V)-, and Ge(IV)-porphyrin Complexes

  • Shiragami, Tsutomu;Onitsuka, Dai;Matsumoto, Jin;Yasuda, Masahide
    • Rapid Communication in Photoscience
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    • 제3권4호
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    • pp.70-72
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    • 2014
  • Visible-light irradiation of MeCN solution containing di(hydroxo)metallo(tetraphenyl)porphyrin complex $(tppM(OH)_2$: 1a; $M=Sb(V)^+Br^-$, 1b; $M=P(V)^+Cl^-$, 1c; M=Ge(IV)) and 2-mercaptoethanol (2-ME) as a substrate under aerated condition gave bis(2-hydroxyethyl)disulfide (2-HEDS) as an oxidative product of 2-ME. It is indicated that the oxidation of 2-ME should proceed with a photocatalytic process by 1, because the turn over number (TON) for the formation of 2-HEDS was over unit. The TON was determined to be 642 as a maximum value when 1a was used as a sensitizer. The formation of 2-HDES was extremely slow under argon atmosphere. The fluorescence of 1 was not quenched by 2-ME at all, and the free energy change (${\Delta}G$) with electron transfer (ET) from 2-ME to excited triplet state of $1(^31^*)$ was estimated as a negative value. The quenching rate constant ($k_r$) of $^31^*$ by 2-ME, obtained by the kinetics for the formation of 2-HEDS, strongly depends on ${\Delta}G$. These findings indicate that 1-sensitized oxidation was initiated by photoinduced ET from 2-ME to $^31^*$ to generate both radical cation of 2-ME ($2-ME^{+\bulle}$) and porphyrin radical anion ($1^{-\bulle}$), resulting that the formation of 2-HEDS can be proceeded by the dimerization of $2-ME^{+\bulle}$, and through a catalytic cycle due to returning to 1 by the ET from $1^{-\bulle}$ to molecular oxygen.

Information entropy based algorithm of sensor placement optimization for structural damage detection

  • Ye, S.Q.;Ni, Y.Q.
    • Smart Structures and Systems
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    • 제10권4_5호
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    • pp.443-458
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    • 2012
  • The structural health monitoring (SHM) benchmark study on optimal sensor placement problem for the instrumented Canton Tower has been launched. It follows the success of the modal identification and model updating for the Canton Tower in the previous benchmark study, and focuses on the optimal placement of vibration sensors (accelerometers) in the interest of bettering the SHM system. In this paper, the sensor placement problem for the Canton Tower and the benchmark model for this study are first detailed. Then an information entropy based sensor placement method with the purpose of damage detection is proposed and applied to the benchmark problem. The procedure that will be implemented for structural damage detection using the data obtained from the optimal sensor placement strategy is introduced and the information on structural damage is specified. The information entropy based method is applied to measure the uncertainties throughout the damage detection process with the use of the obtained data. Accordingly, a multi-objective optimal problem in terms of sensor placement is formulated. The optimal solution is determined as the one that provides equally most informative data for all objectives, and thus the data obtained is most informative for structural damage detection. To validate the effectiveness of the optimally determined sensor placement, damage detection is performed on different damage scenarios of the benchmark model using the noise-free and noise-corrupted measured information, respectively. The results show that in comparison with the existing in-service sensor deployment on the structure, the optimally determined one is capable of further enhancing the capability of damage detection.

연소 안정성 평가 시험을 위한 펄스건 설계 및 개발 시험 (Development and Design of Pulse Gun for Combustion Stability Rating Test)

  • 고영성;이광진;이수용;이대성
    • 한국항공우주학회지
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    • 제31권9호
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    • pp.103-109
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    • 2003
  • 액체 로켓 엔진의 개발 과정 중 필연적으로 선행 연구가 수행되어야 하는 연소 안정성 평가 시험(Stability Rating Test)을 위한 펄스건의 국내 자체 개발을 시도하였다. 개발 초기 단계에서의 몸체의 파열 현상을 해결하기 위해 재질을 변경하고 몸체의 두께를 증가시켰다. 또한 기밀성 유지를 위하여, 멤브레인을 장착하여 기폭 시험전의 기밀 시험을 수행하였으며, 기밀 시험 치구를 제작하여 기폭 후의 기밀을 확인하였다. 실제 SRT를 수행하기 위해서는 펄스건의 cavity 홀더 부분의 재사용이 바람직하므로, 이를 해결하기 위해 재설계/재시험 과정이 수행되었다. 이러한 일련의 시험을 통하여 기폭 푸에도 접촉면 상태가 매우 양호한 SRT 적용 부품이 홀더의 디자인을 확정하여 펄스건 개발을 완료하였다.