• 제목/요약/키워드: All Solid State.

검색결과 393건 처리시간 0.026초

침전법과 고상반응법으로 제조한 $ZnGa_2O_4$ 형광체의 특성 (Characteristics of $ZnGa_2O_4$ phosphor prepared by Precipitation method and Solid-state reaction method)

  • 차재혁;김세준;곽현호;최형욱
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.383-384
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    • 2007
  • The nano and micro-sized $ZnGa_2O_4$ phosphor were prepared by precipitation method and solid-state method. The luminescence, formation process and structure of phosphor powders were investigated by means of XRD, SEM and PL. The result of XRD analysis showed that $ZnGa_2O_4$ spinel structure was formed at as-prepared in the case of precipitation method. However, micro-sized phosphor was required high heating treatment to have a satisfactory spinel structure. The CL intensity of nano-sized phosphor was about 4-fold higher than that of micro-sized phosphor. The emission spectra of all $ZnGa_2O_4$ phosphor show a self activated blue emission band at around 420 nm in the wide range of 300~600 nm.

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Electrical Properties of ZnxMn3-xO4 Ceramics for Application as IR Detectors

  • Kim, Kyeong-Min;Lee, Sung-Gap;Lee, Dong-Jin
    • Transactions on Electrical and Electronic Materials
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    • 제17권4호
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    • pp.227-230
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    • 2016
  • ZnxMn3-xO4 (0.95≤x≤1.20) specimens were prepared using a conventional solid state reaction method. All specimens were sintered in air at 1,200℃ for 12 h, cooled at a rate of 2℃/min to 800℃, and subsequently quenched to room temperature. We investigated the electrical properties of ZnxMn3-xO4 specimens with various amounts of ZnO for use as IR detectors. At a composition of x≥1.15, the ZnO phase precipitates beside the spinel structure. The electrical resistivity at room temperature, activation energy, responsivity, and detectivity of a Zn1.10Mn1.90O4 specimen are 653.2 kΩ-cm, 0.392 eV, 0.016 V/W, and 7.52×103 cmHz1/2/W, respectively.

모의 콘크리트 환경에서 강철 철근의 부식을 모니터링하기 위한 현장 고체 기준 전극 평가 (Assessment of In-Situ Solid-State Reference Electrode for Monitoring Corrosion of Steel Rebar in Simulated Concrete Environments)

  • 카르틱 수비아;박태준;이한승
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2023년도 봄 학술논문 발표대회
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    • pp.281-282
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    • 2023
  • The solid-state reference electrodes made of polyaniline-coated MnO2 (SSRE-PAM) and their electrochemical characteristics were studied in simulated concrete pore solutions (SCPS) containing 0 and 3.5% NaCl. Saturated calomel electrodes (SCE) have been used to conduct electrochemical studies on the stability behavior of SSRE-PAM. Open circuit potential (OCP) and potentiodynamic polarization techniques were used to assess the corrosion performance of steel rebar exposed in SCPS with 0 and 3.5% NaCl using SSRE-PAM. The results demonstrate that the SSRE-PAM was capable of identifying steel rebar in a concrete environment that was either passive or active. Potentiodynamic polarization parameters such as Ecorr and Icorr for steel rebar in SCPS containing 0 and 3.5%)NaCl are greater than that of the passive condition (0% NaCl). All the studies validate the importance of using SSRE-PAM for corrosion monitoring applications in concrete structures.

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Comparison of changes in functional characteristics of fermented soybean with different microbial strains

  • Hyewon Lim;Bosung Kim;Heewon Jung;Sungkwon Park
    • 농업과학연구
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    • 제49권4호
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    • pp.995-1001
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    • 2022
  • The purpose of this study was to compare the effect of solid-state fermentation on soybean using three microbial strains under four different fermentation times. Soybean was fermented for 12, 24, 36 or 48 hours with highly proteolytic microbes, either Bacillus amyloliquefaciens (BA), B. subtilis (BS), or B. subtilis var. natto (BN), and levels of total protein concentration, protein distribution, and antioxidant activity were analyzed. Total protein was highest in the BS 12 h group (9.21 ㎍·µL-1) and lowest in BN 48 h (6.80 ㎍·µL-1), respectively (p < 0.001). Furthermore, three microbes decomposed large molecular weight proteins as well as major allergens of soybean such as β-conglycinin, Gly m Bd 30K, and glycinin. Each treatment group showed the highest degradation rate at 48 h fermentation and among the three microbes, BS showed a relatively higher degradation rate. The radical scavenging ability, known as an indicator of antioxidant activity, showed a significant increase in all treatment groups except BA 24 h. The results from this study suggest that protein concentration, and degradation and antioxidant activity were affected by different types of microbial trains and fermentation period and that B. subtilis fermentation might be the most effective way to increase nutritional and functional properties of soybean.

Flexible 기판 위의 전고상 전기변색 소자 제작 (All-solid-state electrochromic devices on flexible substrate)

  • 나윤채;심희상;조인화;성영은
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.129-129
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    • 2003
  • 전기변색(electrochromism)은 전기화학적 산화, 환원 과정을 통해 가역적인 광학특성의 변화를 갖는 현상을 말하며, 이를 이용한 전기변색소자(electrochromic device)는 전력 소모가 적고 변색효율이 크다는 장점으로 인해 smart window, display, mirror 등에 응용될 수 있다. 전기변색소자는 구조상 투명 기판, 투명 전도체, 환원 착색 물질 (cathodic coloration material), 산화 착색 물질(anodic coloration material), 그리고 투명 이온 전도체로 구성된다. 일반적으로 투명 기판으로는 열적 안정성이 좋은 유리기판을 사용하여 window에 응용할 수 있는 장점이 있는 반면 다양한 형태를 갖는 소자를 제작하기에는 그 한계가 있다.

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Synthesis of New Bicyclic Aziridines Containing Chalcone Analogs and Investigation of Their Photochromic Properties

  • Besharati-Seidani, Tayebeh;Mahmoodi, Nosrat O.
    • Bulletin of the Korean Chemical Society
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    • 제34권3호
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    • pp.875-883
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    • 2013
  • Ten new derivatives of 1,3-diazabicyclo[3.1.0]hex-3-enes linked via ether linkage to chalcones were synthesized and characterized by UV, FT-IR, $^1H$ NMR and $^{13}C$ NMR spectral techniques. The spectra of all synthesized compounds, confirmed structure-photochromic behavior relationships (SPBR) both in solution or in solid state by irradiation under UV light at 254 nm. In other efforts for first time photochromic behavior of ketoaziridines has been investigated.

초음파 분무 열분해법에 의한 $(Zr, SN)TiO_4$ 구형 미분말의 합성 (Preparation of Spherical (Zr, Sn)TiO4 Powders by Ultrasonic Spray Pyrolysis)

  • 조서용;이종흔;김명철;박순자
    • 한국세라믹학회지
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    • 제31권5호
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    • pp.465-470
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    • 1994
  • Fine, spherical (Zr, SN)TiO4 powders were prepared from the aqueous solution of metal chlorides by ultrasonic spray pyrolysis. Single phase (Zr, SN)TiO4 powders could be obtained above $700^{\circ}C$ (=temperature of the reactor) and all powders exhibited sizes in the range of 0.1 to 2.0 ${\mu}{\textrm}{m}$ and a narrow size distribution. The sintering properties of the prepared powders were better than those of the powders from solid-state reaction.

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Does the prosthesis weight matter? 3D finite element analysis of a fixed implant-supported prosthesis at different weights and implant numbers

  • Tribst, Joao Paulo Mendes;Dal Piva, Amanda Maria de Oliveira;Borges, Alexandre Luiz Souto;Rodrigues, Vinicius Aneas;Bottino, Marco Antonio;Kleverlaan, Cornelis Johannes
    • The Journal of Advanced Prosthodontics
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    • 제12권2호
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    • pp.67-74
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    • 2020
  • PURPOSE. This study evaluated the influence of prosthesis weight and number of implants on the bone tissue microstrain. MATERIALS AND METHODS. Fifteen (15) fixed full-arch implant-supported prosthesis designs were created using a modeling software with different numbers of implants (4, 6, or 8) and prosthesis weights (10, 15, 20, 40, or 60 g). Each solid was imported to the computer aided engineering software and tetrahedral elements formed the mesh. The material properties were assigned to each solid with isotropic and homogeneous behavior. The friction coefficient was set as 0.3 between all the metallic interfaces, 0.65 for the cortical bone-implant interface, and 0.77 for the cancellous bone-implant interface. The standard earth gravity was defined along the Z-axis and the bone was fixed. The resulting equivalent strain was assumed as failure criteria. RESULTS. The prosthesis weight was related to the bone strain. The more implants installed, the less the amount of strain generated in the bone. The most critical situation was the use of a 60 g prosthesis supported by 4 implants with the largest calculated magnitude of 39.9 mm/mm, thereby suggesting that there was no group able to induce bone remodeling simply due to the prosthesis weight. CONCLUSION. Heavier prostheses under the effect of gravity force are related to more strain being generated around the implants. Installing more implants to support the prosthesis enables attenuating the effects observed in the bone. The simulated prostheses were not able to generate harmful values of peri-implant bone strain.

The effect of finite strain on the nonlinear free vibration of a unidirectional composite Timoshenko beam using GDQM

  • Ghasemi, Ahmad Reza;Mohandes, Masood
    • Advances in aircraft and spacecraft science
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    • 제3권4호
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    • pp.379-397
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    • 2016
  • In this manuscript, free vibrations of a unidirectional composite orthotropic Timoshenko beam based on finite strain have been studied. Using Green-Lagrange strain tensor and comprising all of the nonlinear terms of the tensor and also applying Hamilton's principle, equations of motion and boundary conditions of the beam are obtained. Using separation method in single-harmonic state, time and locative variables are separated from each other and finally, the equations of motion and boundary conditions are gained according to locative variable. To solve the equations, generalized differential quadrature method (GDQM) is applied and then, deflection and cross-section rotation of the beam in linear and nonlinear states are drawn and compared with each other. Also, frequencies of carbon/epoxy and glass/epoxy composite beams for different boundary conditions on the basis of the finite strain are calculated. The calculated frequencies of the nonlinear free vibration of the beam utilizing finite strain assumption for various geometries have been compared to von Karman one.

클로로프로파미드와 싸이클로덱스트린과의 포접 화합물에 관한 연구 (Inclusion Complexation of Chlorpropamide with Cyclodextrins)

  • 정경혜;김길수;구영순
    • 약학회지
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    • 제30권2호
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    • pp.87-95
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    • 1986
  • Inclusion complexation of $\alpha$-cyclodextrin($\alpha$-CD), $\beta$-cyclodextrin($\beta$-CD) and tri-O-methyl-$\beta$-cyclodextrin(tri-O-methyl-$\beta$-CD) with chlorpamide(CPA) in aqueous solution and in the solid state were studied by the solubility method, spectroscopy (UV, IR), differential scanning calorimetry (DSC) and powder X-ray diffractometry, and all their molar ratios were found to be 1:1. The solid complexes of CPA with three kinds of cyclodextrins were prepared by a freezedrying method, and their dissolution behaviors were examined. As a result, the release of CPA from the inclusion complexes was significantly improved. The intrinsic dissolution rate of CPA in cyclodextrin inclusion complexes was about 51 times ($\alpha$-CD inclusion complex) and 12 tmies ($\beta$-CD inclusion complex) larger than that of intact CPA.

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