• Title/Summary/Keyword: Alkaline treatment

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Changes in Surface Shape and Physical Properties of Acetate Fabrics by Alkaline and Cellulase Treatment (알칼리와 셀룰라아제 처리에 의한 아세테이트 직물의 표면 형태 및 성능의 변화)

  • 이애진;이혜자;유혜자
    • Textile Coloration and Finishing
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    • v.13 no.1
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    • pp.9-17
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    • 2001
  • The purpose of this study is to present basic data for the enzymatic modification of acetate fabrics. The weight loss and rate of weight loss of acetate fabrics increased with increasing NaOH concentration and treating time. Acetyl value decreased as the weight loss became higher. The weight loss of alkaline-treated acetate fabrics were directly proportional to the concentration and treating time of cellulase. The optimum temperature and pH in cellulase treatment were $55^\circ{C}$ and pH 3.5. The surface shape revealed that density of fiber decreased by alkaline-treatment. With the treating time of cellulase, fibrillation occurred. In case of higher weight loss in alkaline treatment, fibril is removed after 180 min. The tensile strength decreased by alkaline and cellulase treatment. Especially, in case of higher weight loss of alkaline treatment, tensile strength decreased suddenly. Alkaline treatment increased the drapability of acetates, while cellulase treatment increased it initially but decreased gradually with treatment time. The dyeability after alkaline treatment was improved for reactive dye, but deteriorated for disperse dye. The cellulase treatment of acetate lowered the dyeability for both types of dyes.

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The Effect of Sodium Acetate in Alkaline Treatment of Acetate Fabrics (아세테이트 직물의 NaOH 처리시 무기염 첨가에 따른 영향)

  • Sung, Jong-Mi;Kim, Hye-Rim;Song, Wha-Soon
    • Fashion & Textile Research Journal
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    • v.7 no.1
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    • pp.85-90
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    • 2005
  • The effect of sodium acetate to reduce the fiber damage and hardening of acetate fabrics during alkaline treatment is studied. The optimal condition is controlled concentration 2%, at $50^{\circ}C$ for 6 minutes and at $70^{\circ}C$ for 2 minutes through the result of weight loss, shrinkage and tensile strength. Alkaline treated acetate fabrics under optimal condition show softer than untreated acetate fabrics. Alkaline treatment with sodium acetate brings the reduction in hardening and shrinkage in internal fiber of acetate fabric. Also, alkaline treatment with sodium acetate improves the tensile strength of acetate fabrics compared with only alkaline treatment. The moisture regain of acetate fabrics is also improved by alkaline treatment under optimal condition.

Comparison of Sewage Sludge Solubilization through Different Pretreatment Methods (전처리 방법에 따른 하수슬러지 가용화 비교연구)

  • Kwon, Jae-Hyun;Kim, Bong-Jun;Kim, Min-Kyu;Yeom, Ick-Tae;Kim, Hyung-Soo
    • Journal of Korean Society of Water and Wastewater
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    • v.17 no.4
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    • pp.567-573
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    • 2003
  • The pretreatment process was carried out to solubilize the sewage sludge for enhancing its biodegradability using alkaline treatment, ultrasonic treatment(15kHz), ozone treatment and different combination of these three methods: alkaline followed by ultrasonic as well as ozone, and ultrasonic followed by alkaline. The solubilization efficiency was evaluated based on the SCOD/TCOD ratio and VSS/TS ratio. In results, the proper condition of alkaline treatment was shown as 30meq/l of NaOH, pH 12 and 3hours of reaction time. Solubilization efficiency increased to 17% from initial 2% based on SCOD/TCOD ratio under this condition. In ultrasonic treatment, the higher ultrasonic power, the longer treatment time and the lower sludge volume resulted in higher solubilization respectively. There was a rapid increase in solubilization efficiency after 20 minute, then it was measured as 32% of SCOD/TCOD ratio in 1 hour at a ultrasonic power of 1,300W with 1/sludge. Solubilization efficiencies in combined treatment using alkaline and ultrasonic were 47-53% higher than single treatment at a sonicated time of 1 hour. Ozone treatment followed by alkaline treatment also represented the enhanced solubilization compared to ozone treatment. Therefore, ultrasonic or ozone treatment assisted by alkaline could achieve the short treatment time as well as high solubilizetion efficiency.

Effects of Alkaline Treatment on the Characteristics of Chemical Pulps for Papermaking (알칼리 처리가 제지용 화학펄프의 특성에 미치는 영향)

  • Won, Jong-Myoung;Kim, Min-Hyun
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.3
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    • pp.106-112
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    • 2011
  • The effects of alkaline treatment on the WRV, crystalline structure and sheet structure of softwood and hardwood bleached kraft pulp were investigated. Sodium hydroxide and sodium carbonate were used as chemicals for alkaline treatment and two levels of alkali dosage (5%, 10%) were applied respectively. Alkali treated and untreated pulp were refined to three levels (550, 450 and 350 mL CSF). WRV of the alkali treated pulps depended on the alkaline type and concentration. It was found that the crystalline structures of softwood and hardwood pulp were not changed by refining. Sodium carbonate and lower concentration of sodium hydroxide treatment did not caused any modification of cellulose crystalline structure, while higher concentration of sodium hydroxide treatment caused the partial modification of cellulose crystalline structure. Alkaline treatment of hardwood bleached kraft pulp led to the shrinkage of fiber diameter and bulky structure of sheet. Alkaline treatment of softwood bleached kraft pulp did not cause the significant change in fiber shrinkage and bulk of sheet.

Lipase Treatment of Polyester Fabrics

  • Kim, Hye-Rim;Song, Wha-Soon
    • Fibers and Polymers
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    • v.7 no.4
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    • pp.339-343
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    • 2006
  • The aim of this paper is to improve moisture regain of PET fabrics using a lipase treatment. Effects of nine lipase sources, lipase activator and nonionic surfactant on moisture regain of PET fabrics are examined. Moisture regains of lipase-treated samples improve by two times in average compared with untreated and buffer-treated samples. Alkaline treatment creates larger pitting by more aggressive attack into fiber which is proved by SEM and water contact angle measurement. Moisture regain by alkaline treatment ($0.568%{\pm}0.08$) does not improve. However, lipase-treatment (L2 treatment) improves moisture regain up to 2.4 times ($1.272%{\pm}0.05$). Although lipase treatment is more moderate than alkaline treatment, lipase hydrolysis on PET fabrics improves moisture regain, efficiently. K/S values improved confirm that carboxyl and hydroxyl groups are produced on the surface of PET fabrics by lipase hydrolysis. Moisture regain and dyeability improve by lipase hydrolysis on PET fabrics.

Development of an After-treatment Agent, Using an Alkaline Hair Treatment (알칼리성 모발처리제를 이용한 후처리제 개발)

  • Kim, Hye-Kyun
    • Journal of Digital Convergence
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    • v.15 no.1
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    • pp.509-517
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    • 2017
  • As the effectiveness of ionic water that mainly used for the purpose of treatment has been widely known with the recent "well-being" trend, people's interest in it is also gradually increasing. Especially, the alkaline ionic water for drinking purpose could conveniently provide different types/amount of inorganics required for different dietary life depending on nature and race, could effectively provide alkaline inorganics that could be insufficient to modern Korean people, and also could provide alkaline inorganics that prevent/cure/relieve pregnant women's morning sickness. Applying the suggested performance/manufacturing method of alkaline ionic water through the performance assessment of alkaline electrolytic ionic water of the developed product, it would be necessary to have additional researches on the improvement of product or parallel development that could be applied to diverse areas.

Antimicrobial efficacies of alkaline disinfectant solution and commercial disinfectants against Brucella ovis

  • Yoo, Jong-Hyun
    • Korean Journal of Veterinary Service
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    • v.32 no.4
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    • pp.347-351
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    • 2009
  • Bruella spp. involves a considerable danger of public health and farm animal industry. In this study, we assessed the disinfection efficacy of alkaline disinfectant solution and three commercial farm disinfectants (quaternary ammonium compound, sodium dichloroisocyanurate, potassium monopersulphate/sodium dichloroisocyanurate) against Brucella ovis. A bactericidal efficacy test by broth dilution method was used to determine the lowest effective dilution of selected disinfectants following exposure to test bacteria for 30 minutes at $4^{\circ}C$. Disinfectants and test bacteria are diluted with distilled water (DW), hard water (HW) or organic matter suspension (OM) according to treatment condition. Three commercial disinfectant showed excellent antimicrobial activity (up to dilution of $\times200$ in OM treatment). Alkaline disinfectant solution demonstrated favorable bactericidal efficacy against B. abortus (at dilution of $\times20$ in OM treatment). Three commercial farm disinfectants possess excellent efficacy against B. ovis. Alkaline disinfectant solution has lower potency than commercial farm disinfectant but could help to limit the spread of brucellosis.

Recycling of Waste Paper with Alkaline Cellulolytic Enzyme(III) - Elimination of sticky contaminants and bleaching of recycling pulp- (호알칼리성 목질 분해 효소를 이용한 페지 재생(제3보) -페지의 이물질 제거 및 표백-)

  • 강석현;이중명;박성배;엄태진
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.1
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    • pp.30-36
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    • 2004
  • Waste papers(MOW and ONP) were deinked with alkaline cellulolytic enzyme from Coprinus cinereus 2249. The effectiveness of alkaline enzyme on sticky contaminant removal and bleaching of recycling pulp was investigated. The conclusions obtained from the results are as follows. The brightness of deinked pulps MOW and ONP was most high in 0.4IU enzyme treatment. \circled2 The removal effect of sticky contaminant was enhanced with alkaline cellulolytic enzyme treatment. Bleaching with sodium hydrosulfite was most effective in one and two stage bleaching after enzyme treatment of mixed wastepaper of MOW and colored paper. \circled4 The brightness of alkaline enzyme deinked ONP was increased 20% with $H_2O$$_2$ bleaching.

A Study on the Weight Loss of Island-in-a Sea Fabrics by Ultrasonic (초음파를 이용한 해도직물의 감량 가공에 관한 연구)

  • 신현세;윤철수;임병완
    • Textile Coloration and Finishing
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    • v.16 no.1
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    • pp.40-47
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    • 2004
  • Alkaline treatment gives Sea-Island type yam to produce microfiber and silk-like touch. But this treatment have some problems in dyeing and finishing process. To solve some problem occurred in dyeing and finishing of polyester fabric, the ultrasonic treatment technique was used recently. This study was carried out to confirm the effect of the ultrasonic treatment on alkaline weight loss finishing of polyester fiber under general alkaline treatment conditions; NaOH concentration 2, 3, 4, and 5%, treatment time 5, 10, 15, and 20 minutes, treatment temperature 70, 80, 90, and 99'E, respectively. On the other hand, the three way lay out method was used to test of significant obtained data from alkaline treatment. It was found that weight loss increased with increasing the NaOH concentration, temperature, and time. Also, in case of PET/Co-PET fabrics by ultrasonic, weight loss and dissolution of microfiber were superior to PET/Co-PET fabrics without ultrasonic. Tensile strength and modulus decreased with increasing NaOH concentrations and hydrolysis time. Therefore, the effect of alkali hydrolysis by ultrasonic application was better than that of the conventional method.

A Study on the Alkaline Degradation Properties of Silk Fabrics for Costume Heritage Restoration (유물 복원을 위한 실크 직물의 알칼리에 의한 열화 특성 연구)

  • Jeon Cho-Hyun;Kwon Young-Suk;Lee Sang-Joon;Cho Hyun-Hok
    • Textile Coloration and Finishing
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    • v.17 no.4 s.83
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    • pp.41-47
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    • 2005
  • Costume heritages of an excavated silk fabrics should be preserved without damage. In order to artificially restore the excavated silk fabrics, alkaline aqueous solution, as a simulated corpse, and two kinds of silk fabrics were used. Two kinds of silk fabrics were treated by aqueous alkaline solution according to strength retention value(100, 80, 60, 40, 20$\%$). The fine structure and physical properties of alkaline treated silk fabrics were investigated with various techniques such as wide-angle X-ray diffraction, tensile test, weight loss, shrinkage, SEM. and yellowness. As the alkaline treatment time increased tensile strength of silk fabrics decreased. However, weight loss and shrinkage slightly increased. The diffraction intensity of $\beta-form$ crystal declined and $\alpha-form$ crystal diffraction intensity disappeared with the treatment.