• Journal of Korea Foundry Society
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• v.29 no.6
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• pp.265-269
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• 2009

The optimum RRA heat treating conditions and SCC (stress corrosion cracking) resistance of semi-solid Al-Zn-Mg-Cu alloy fabricated by inclined cooling plate were compared with those of conventional mould cast alloys. The non-stirring method characterized by using a cooling plate can effectively eliminate dendritic structure and form a fine globular semisolid microstructure in as-cast Al-Zn-Mg-Cu alloy and the SCC resistance of semi-solid Al-Zn-Mg-Cu alloy was higher than that of conventional mold cast alloy. Also, after retrogressed treatment at RRA heat treatment of semi-solid Al-Zn-Mg-Cu alloy, retrogressed treatment time has increased more than 10 minutes at $180^{\circ}C$ to recovery the T6 heat treatment strength.

• Journal of Powder Materials
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• v.30 no.6
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• pp.470-477
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• 2023

The effects of annealing on the microstructure and mechanical properties of Al-Zn-Mg-Cu-Si alloys fabricated by high-energy ball milling (HEBM) and spark plasma sintering (SPS) were investigated. The HEBM-free sintered alloy primarily contained Mg₂Si, Q-AlCuMgSi, and Si phases. Meanwhile, the HEBM-sintered alloy contains Mg-free Si and θ-Al₂Cu phases due to the formation of MgO, which causes Mg depletion in the Al matrix. Annealing without and with HEBM at 500℃ causes partial dissolution and coarsening of the Q-AlCuMgSi and Mg₂Si phases in the alloy and dissolution of the θ-Al₂Cu phase in the alloy, respectively. In both alloys, a thermally stable α-AlFeSi phase was formed after long-term heat treatment. The grain size of the sintered alloys with and without HEBM increased from 0.5 to 1.0 ㎛ and from 2.9 to 6.3 ㎛, respectively. The hardness of the sintered alloy increases after annealing for 1 h but decreases significantly after 24 h of annealing. Extending the annealing time to 168 h improved the hardness of the alloy without HEBM but had little effect on the alloy with HEBM. The relationship between the microstructural factors and the hardness of the sintered and annealed alloys is discussed.

• Journal of Korea Foundry Society
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• v.32 no.1
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• pp.38-43
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• 2012

The effects of Mg and Cu amounts on the casting characteristics and tensile property of Al-Zn-Mg-Cu alloys were investigated for the development of high strength aluminium alloys for gravity mold casting. Increase of copper amounts in Al-6%Zn-3%Mgy% Cu alloys resulted in reduction of the fluidity of these alloys and had little effects on the tensile property of these alloys. Increase of magnesium amounts from 1.0wt% to 3.3wt% in Al-6%Zn-x%Mg-0.5%Cu alloys resulted in reduction of the elongation of these alloys from 12% to 3% and increase of the tensile strength of these alloys from 340MPa to 450MPa, but had little effects on the fluidity of these alloys.

• Applied Microscopy
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• v.36 no.2
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• pp.47-55
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• 2006

In this paper a transmission electron microscope (TEM) observation of fine Cu precipitates distributed randomly in Al-2.5Cu-1.5Mg wt.% alloy is first reported. This new observation happened to occur when an ion milling was peformed to remove oxides on the specimen, particularly, aged 100 hours at $150^{\circ}C$. Meanwhile the oxides were identified to be $Cu_2O$ particles. For this work involved with analysis of diffraction rings, the formulation of the electron diffraction rings pattern for powder particles was made. Finally the significance of this unexpected ion milling effort on the alloy was discussed

• Journal of Korea Foundry Society
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• v.16 no.6
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• pp.556-564
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• 1996

Variation of shape and size of solid particles and solute redistribution in Mg-9wt.%Al, AI-4.5wt.% Cu, and AI-7wt.%Si alloys were investigated when they were heated to semi-solid temperatures and held without stirring. In the case of Mg-9wt.% Al and Al-4.5wt.%Cu alloys, the polygonal shaped solid particles were agglomerated with non-uniform distribution, and there were no disappearance of the solid/solid boundary until the end of melting. But in the case of an Al-7wt.%Si alloys, two or three spherical shaped particles were coalesced or separated individually, and the coalesced particles had no solid/solid interface on the contrary to the prevous case. The maximum size of solid particles during isothermal heating at high temperature was smaller than that at lower temperature, but the time required to reach the maximum size at high temperature was shorter than that at lower temperature. The concentrations of main solute atom whose distribution coefficient is lower than 1, decreased in the primary solid particles as the liquid fraction increased, and the gradient of solute concentration was steeper in Mg-9wt.%Al alloy and Al-4.5wt.%Cu alloy than that of Al-7wt.%Si alloy.

• Journal of the Korean institute of surface engineering
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• v.40 no.5
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• pp.241-244
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• 2007

$MgF_2$/Cr/$MgF_2$, $MgF_2$/Cu/$MgF_2$ and $MgF_2$/Al/$MgF_2$ multi-layered thin films were fabricated by evaporation system. $MgF_2$ and Cr(Cu, And Al) was selected as a low refractive index material and mid reflector layer, respectively. Optical properties including color effect were systematically studied in terms of different film layer by using spectrophotometer. Experimental results were compared to the simulation result. The films consistings of $MgF_2$/Cr/$MgF_2$, $MgF_2$/Cu/$MgF_2$, $MgF_2$/Al/$MgF_2$ multi-layered thin films showed wavelength range of $430{\sim}780nm$, typically color range between greenish yellow and orange at view angle of $45^{\circ}$. It was confirmed that this experimental result was well matched with simulation result.

• Journal of Korea Foundry Society
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• v.34 no.4
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• pp.130-135
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• 2014

Efforts have been made to develop new silicon-free aluminum casting alloys that possess high electrical and thermal conductivity. In this research Al-Fe-Cu-Mg alloys with various Cu and Mg contents were investigated for their various properties. As the Cu or Mg content was increased, the electrical conductivity gradually decreased, while the tensile strength of the Al-Fe-Cu-Mg alloy tended to be improved. It was found that fluidity was generally inversely proportional to the Cu content, but the alloys containing 1%Mg showed considerably low fluidity, regardless of the Cu content.

• Journal of the Korea Organic Resources Recycling Association
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• v.20 no.3
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• pp.60-70
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• 2012

Zn, Cu, Fe, Al contents of sludges produced from sewage treatment plants and night soil treatment plant in Pocheon City, Gyeong-gi Province were investigated. And the accumulated contents of those metals in the earthworm Eisenia fetida were also investigated while 15, 30, 45, 60, 75, 90, 105 grams(dw) of sludges were cumulatively supplied to the earthworms. Zn contents of sludges were 75.1~196.1 mg/kg, Cu contents 3.74~76.1 mg/kg, Fe contents 219.9~857.8 mg/kg, Al contents 198.4~991.7 mg/kg, all of which would not cause acute toxicity to the earthworm, but could cause sublethal effects on earthworm and reduce the density of next generation's population. However, cumulative supplies of sludges didn't increase the bioaccumulation rates of metals in the earthworm body, and BAFs of those metals after 60g of sludge supply were 0.0~0.43, which meant that the accumulated Zn, Cu, Fe, Al contents in the earthworm were lower than those of sludges.

• Journal of the Korean Society of Mechanical Technology
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• v.20 no.6
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• pp.818-823
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• 2018

In this study, the effect of pre-aging treatment for inhibition of natural aging of Al-4.8Zn-1.3Mg alloy by extrusion process was investigated. Firstly, the as-cast microstructure of Al-4.8Zn-1.3Mg alloy billet and its evolution during homogenization($460^{\circ}C$, $4h+510^{\circ}C$, 5h) were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), hardness analysis. The as-cast microstructures of Al-4.8Zn-1.3Mg alloy reveal $Mg_2Zn$, $Al_5Cu$, $Al_{13}Cu$ formed between dendrities. After homogenization, MgZn, $Al_4Cu$, $Al_{13}Cu$ phases precipitated into the matrix. In addition, standard deviation of homogenized billet was improved than as-cast billet from 2.62 to 0.99. According to pre-aging($100^{\circ}C$, 1h) Al-4.8Zn-1.3Mg alloy by extrusion process, yield strength and tensile strength deviation improved more than condition by natural aging.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1000-1001
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• 2006

Two atomized alloy powders were pre-compacted by cold and subsequently hot forged at temperatures ranging from 653K to 845K. The addition of Cu and Mg causes a decrease in the eutectic reaction temperature of Al-10Si-5Fe-1Zr alloy from 841K to 786K and results in a decrease of flow stress at the given forging temperature. TEM observation revealed that in addition to Al-Fe based intermetallics, $Al_2Cu$ and $Al_2CuMg$ intermetallics appeared. The volume fraction of intermetallic dispersoids increased by the addition of Cu and Mg. Compressive strength of the present alloys was closely related to the volume fraction of intermetallic dispersoids.