• Title/Summary/Keyword: Al-Al bond

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Effects of Al-doping on IZO Thin Film for Transparent TFT

  • Bang, J.H.;Jung, J.H.;Song, P.K.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.207-207
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    • 2011
  • Amorphous transparent oxide semiconductors (a-TOS) have been widely studied for many optoelectronic devices such as AM-OLED (active-matrix organic light emitting diodes). Recently, Nomura et al. demonstrated high performance amorphous IGZO (In-Ga-Zn-O) TFTs.1 Despite the amorphous structure, due to the conduction band minimum (CBM) that made of spherically extended s-orbitals of the constituent metals, an a-IGZO TFT shows high mobility.2,3 But IGZO films contain high cost rare metals. Therefore, we need to investigate the alternatives. Because Aluminum has a high bond enthalpy with oxygen atom and Alumina has a high lattice energy, we try to replace Gallium with Aluminum that is high reserve low cost material. In this study, we focused on the electrical properties of IZO:Al thin films as a channel layer of TFTs. IZO:Al were deposited on unheated non-alkali glass substrates (5 cm ${\times}$ 5 cm) by magnetron co-sputtering system with two cathodes equipped with IZO target and Al target, respectively. The sintered ceramic IZO disc (3 inch ${\phi}$, 5 mm t) and metal Al target (3 inch ${\phi}$, 5 mm t) are used for deposition. The O2 gas was used as the reactive gas to control carrier concentration and mobility. Deposition was carried out under various sputtering conditions to investigate the effect of sputtering process on the characteristics of IZO:Al thin films. Correlation between sputtering factors and electronic properties of the film will be discussed in detail.

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Effect of Tension-Test Temperature on Fracture Behavior and Mechanical Properties in STS/Al/Cu Clad Materials (STS/Al/Cu 클래드재의 파괴거동 및 기계적 물성에 미치는 인장시험 온도의 영향)

  • Bae, Dong-Hyun;Choi, Young-Jun;Chung, Won-Sub;Bae, Dong-Su;Cho, Young-Rae
    • Korean Journal of Metals and Materials
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    • v.47 no.12
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    • pp.811-818
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    • 2009
  • In order to meet increasingly complex and rigorous technical specifications, extensive effort has been devoted to fabricate clad materials with multi-layered metal plates. In this study, novel stainless steel/aluminum/copper (STS/Al/Cu) three-ply clad materials were fabricated by a hot rolling process for cookware applications. The effect of the testing temperature on the mechanical properties of the clad materials and on each component metal was investigated during the tensile tests. The interface properties of the clad materials were also examined by optical microscopy (OM) and an electron probe micro-analyzer (EPMA). The best mechanical and interfacial properties for a warm working process were found in a sample annealed at a temperature of $300^{\circ}C$. For the sample annealed at $400^{\circ}C$, the results of the tensile test indicated that interface delamination occurred only in the region of the Al/Cu interfaces. This was due to the formation of the thick and brittle intermetallic compound of $Al_2Cu$ in the Al/Cu interface. In contrast, no interface delamination was observed in the STS/Al interface, most likely due to its strong bond strength.

Bond Strength Properties of Antiwashout Underwater Concrete (수중 불분리성 콘크리트의 부착 강도 특성에 관한 연구)

  • 김명식;김기동;윤재범
    • Journal of the Korea Concrete Institute
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    • v.12 no.1
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    • pp.89-99
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    • 2000
  • The objective of this study is to investigate the bond strength properties of antiwashout underwater concrete. The arrangement of bars (vertical bar, horizontal upper bar, horizontal lower bar), condition of casting and curing (fresh water, sea water), type of fine aggregate (river sand, blended sand(river sand : sea sand = 1:1), and proportioning strength of concrete (210, 240, 270, 300, 330kgf/$\textrm{cm}^2$)are chosen as the experimental parameters. The test results(ultimate bond stress) are compared with bond and development provisions of the ACI Building Code(ACI 318-89) and proposed equations from previous research(which was proposed by Orangun et. al). The experimental results show that ultimate bond stress of antiwashout underwater concrete which arranged bar on the horizontal lower, used the blend sand, and was cast and cured in the fresh water are higher that other conditions. The ultimate bond stress were increased in proportion to {{{{( SQRT {fcu }) }}3 2. From this study, rational analytic formula for the ultimate bond stress are to be from compressive strength of concrete.

Behavior of tension lap spliced sustainable concrete flexural members

  • Al-Azzawi, Adel A.;Daud, Raid A.;Daud, Sultan A.
    • Advances in concrete construction
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    • v.9 no.1
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    • pp.83-92
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    • 2020
  • The use of spliced reinforcing bars in sustainable concrete members to manage inadequate bars length is a common practical issue which is may be due to some limitations. The lap splicing means two bars overlapped in parallel with specified length called the splice length in order to provide the required bond between the two bars. The bond between sustainable concrete and spliced steel bars is another important issue. The normal strength sustainable concrete specimens of sizes 1700×150×150 mm with tension reinforcement lap spliced were selected according to testing device length limitations. These members were designed to fail in flexure in order to investigate the lap spliced tension bars effect. The selected lap spliced tension bars were of 10 mm size with smooth and deformed surfaces in order to investigate the surface nature accompanied with the splice nature. The sustainable concrete mechanical properties and mix workability were also studied. This study reveals that the effect of number of spliced bars on the response of beams reinforced with smooth bars is found to be more obvious than deformed one. Finite element modeling in three dimensions was carried out for the tested beams using ABAQUS software. A parametric study is carried out using finite elements on considering the following parameters, concrete compressive strength, load type and opening in cross section (hollow section) for weight reduction purposes.The laboratory and numerical results show good agreements in terms of ultimate load and deflection with an average difference of 10% and 15% in ultimate load and deflection respectively.

Growth and characterizations of INAlAs epilayers and InGaAs/INAlAs quantum well structures by low pressure metalorganic chemical vapor deposition (저압 유기금속 화학증착법을 이용한 InAIAs 에피층과 InGaAs/InAIAs 양자 우물 구조의 성장과 분석)

  • 유경란;문영부;이태완;윤의준
    • Journal of the Korean Vacuum Society
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    • v.7 no.4
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    • pp.328-333
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    • 1998
  • Lattice-matched InAIAs epilayers were grown on (001) InP substrate by low pressure metalorganic chemical vapor deposition. The effects of growth conditions on the properties of InAIAs were analyzed, and InGaAs/InAIAs single and multiple quantum wells were successfully grown. It was observed that the optical property of InAIAs epilayers was improved in the temperature range of 620~$700^{\circ}C$ as the growth temperature increased due to the reduction of oxygen incorporation, however, the crystallinity decreased at temperatures higher than $750^{\circ}C$ due to the degraded crystallinity of the bufter layers. The enhanced incorporation of AI into epilayer was observed at high $AsH_3$flow rates and it was explained in terms of the differences in bond strengths of AI-As and In-As. The measured photoluminescence peak energies from InGaAs/InAIAs single quantum wells were consistent with the calculated ones based on transfer matrix method. High-order satellite peaks and fine thickness fringes were observed by high-resolution x-ray diffraction, implying that the high-quality multiple quantum wells with abrupt heterointerfaces were grown.

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Effect of adhesive primers on bonding strength of heat cure denture base resin to cast titanium and cobalt-chromium alloy

  • Kim, Su-Sung;Vang, Mong-Sook;Yang, Hong-So;Park, Sang-Won;Lim, Hyun-Pil
    • The Journal of Advanced Prosthodontics
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    • v.1 no.1
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    • pp.41-46
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    • 2009
  • STATEMENT OF PROBLEM. The poor chemical bonding of a denture base resin to cast titanium framework often introduces adhesive failure and increases microleakage. PURPOSE. This study evaluated the shear bond strengths of a heat cure denture base resin to commercially pure titanium, Ti-6Al-4V alloy and a cobalt-chromium alloy using two adhesive primers. MATERIAL AND MATHODS. Disks of commercially pure titanium, Ti-6Al-4V alloy and a cobalt-chromium alloy were cast. Specimens without the primer were also prepared and used as the controls. The shear bond strengths were measured on a screw-driven universal testing machine. RESULTS. The primers significantly(P < .05) improved the shear bond strengths of the heat cure resin to all metals. However, the specimens primed with the Alloy $primer^{(R)}$(MDP monomer) showed higher bond strength than those primed with the MR $bond^{(R)}$(MAC-10 monomer) on titanium. Only adhesive failure was observed at the metal-resin interface in the non-primed specimens, while the primed specimens showed mixed failure of adhesive and cohesive failure. CONCLUSIONS. The use of appropriate adhesive metal primers makes it possible not only to eliminate the need for surface preparation of the metal framework before applying the heat cure resins, but also reduce the need for retentive devices on the metal substructure. In particular, the Alloy $primer^{(R)}$, which contains the phosphoric acid monomer, MDP, might be clinically more acceptable for bonding a heat cure resin to titanium than a MR $bond^{(R)}$, which contains the carboxylic acid monomer, MAC-10.

AN EXPERIMENTAL STUDY ON ADHESION PATTERN, ADHESION STRENGTH AND FRACTURE PATTERN OF THE ADHESIVE CAST GOLD INLAY (접착형 구조 금 인레이의 접착 형태, 강도 및 파절 양태에 관한 실험적 연구)

  • Han, Seoung-Ryul;Hong, Chan-Ui
    • Restorative Dentistry and Endodontics
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    • v.19 no.1
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    • pp.64-72
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    • 1994
  • Zinc Phosphate Cement hand been used for about more than 100 years in luting of cast gold inlay. But many scientists had been trying to develop the new form of luting agent because the ZPC hand shown the lack of adhesiveness on the tooth structure and the toxicity to the pulp tissue. Recently many researches about the surface treatment of the cast body are being done to increase the adhesion of cement to it. The conventional Class I gold inlays were fabricated in the 20 permanent molars. After the internal surface of the cast body was sandblasted with $Al_2O_3$ particles and was tin-plated, the inlays were cemented with adhesive cement [G I cement and resin cement(Super-Bond & $Panavia_{EX}$)] and the evaluation on the adhesion pattern, adhesive strength and the fracture pattern of the adhesive cast gold inlay was compared to that of the cast gold inlay cemented conventionally with ZPC. The results were as follows : 1. The surface roughness of the cast body was increased significantly after sandblasting with the $Al_2O_3$ particles and the tin oxide layer, which was consisted of round particles, came into being. 2. The bond strength was in the order of Super-Bond, ZPC, Fuji I, $Panavia_{EX}$ group. The group cemented with Super-Bond showed statistically greater strength than the other groups(p<0.05). 3. The group cemented with ZPC was fallen apart by principal adhesion failure and that with Fuji I was by complete adhesion failure. But the group with Super-Bond showed pricncipal cohesive failure pattern and in the group with $Panavia_{EX}$, complete cohesive fracture pattern was shown and small protion of tooth structure was fractured out with cast body and the fractured surface showed the figure just as the enamel prism. 4. Various gaps were shown at the pulpal side regardless of little gap at the side walls of the cavity in all groups. Only the Super-Bond was attached to the tooth structure and the other cements were detached from both the tooth and the cast body.

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Effect of casein phosphopeptide-amorphous calcium phosphate on fluoride release and micro-shear bond strength of resin-modified glass ionomer cement in caries-affected dentin

  • Agob, Jamila Nuwayji;Aref, Neven Saad;Al-Wakeel, Essam El Saeid
    • Restorative Dentistry and Endodontics
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    • v.43 no.4
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    • pp.45.1-45.11
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    • 2018
  • Objectives: This study was conducted to evaluate fluoride release and the micro-shear bond strength of resin-modified glass ionomer cement (RMGIC) in casein phosphopeptide-amorphous calcium phosphate (CPP-ACP)-remineralized caries-affected dentin (CAD). Materials and Methods: Exposed dentin surfaces of 30 human third molar teeth were divided into 2 equal groups for evaluating fluoride release and the micro-shear bond strength of RMGIC to CAD. Each group was subdivided into 3 equal subgroups: 1) control (sound dentin); 2) artificially demineralized dentin (CAD); 3) CPP-ACP remineralized dentin (remineralized CAD). To measure fluoride release, 15 disc-shaped specimens of RMGIC (4 mm in diameter and 2 mm in thickness) were bonded on one flat surface of the dentin discs of each group. Fluoride release was tested using ion chromatography at different intervals; 24 hours, 3, 5, 7 days. RMGIC micro-cylinders were built on the flat dentin surface of the 15 discs, which were prepared according to the assigned group. Micro-shear bond strength was measured after 24 hours water storage. Data were analyzed using 1- and 2-way analysis of variance and the post hoc least significant difference test (${\alpha}=0.05$). Results: Fluoride detected in solutions (at all intervals) and the micro-shear bond strength of RMGIC bonded to CPP-ACP-remineralized dentin were significantly higher than those bonded to artificial CAD (p < 0.05). Conclusions: Demineralized CAD consumes more fluoride released from RMGIC into the solution for remineralization than CPP-ACP mineralized dentin does. CPP-ACP increases the micro-shear bond strength of RMGIC to CAD.

Effects of air-abrasion pressure on the resin bond strength to zirconia: a combined cyclic loading and thermocycling aging study

  • Al-Shehri, Eman Z.;Al-Zain, Afnan O.;Sabrah, Alaa H.;Al-Angari, Sarah S.;Dehailan, Laila Al;Eckert, George J.;Ozcan, Mutlu;Platt, Jeffrey A.;Bottino, Marco C.
    • Restorative Dentistry and Endodontics
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    • v.42 no.3
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    • pp.206-215
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    • 2017
  • Objectives: To determine the combined effect of fatigue cyclic loading and thermocycling (CLTC) on the shear bond strength (SBS) of a resin cement to zirconia surfaces that were previously air-abraded with aluminum oxide ($Al_2O_3$) particles at different pressures. Materials and Methods: Seventy-two cuboid zirconia specimens were prepared and randomly assigned to 3 groups according to the air-abrasion pressures (1, 2, and 2.8 bar), and each group was further divided into 2 groups depending on aging parameters (n = 12). Panavia F 2.0 was placed on pre-conditioned zirconia surfaces, and SBS testing was performed either after 24 hours or 10,000 fatigue cycles (cyclic loading) and 5,000 thermocycles. Non-contact profilometry was used to measure surface roughness. Failure modes were evaluated under optical and scanning electron microscopy. The data were analyzed using 2-way analysis of variance and ${\chi}^2$ tests (${\alpha}=0.05$). Results: The 2.8 bar group showed significantly higher surface roughness compared to the 1 bar group (p < 0.05). The interaction between pressure and time/cycling was not significant on SBS, and pressure did not have a significant effect either. SBS was significantly higher (p = 0.006) for 24 hours storage compared to CLTC. The 2 bar-CLTC group presented significantly higher percentage of pre-test failure during fatigue compared to the other groups. Mixed-failure mode was more frequent than adhesive failure. Conclusions: CLTC significantly decreased the SBS values regardless of the air-abrasion pressure used.

Investigation on Adhesion Properties of Sandwich Composite Structures Considering on Surface Treatments

  • Park, Gwanglim;Oh, Kyungwon;Kong, Changduk;Park, Hyunbum
    • International Journal of Aerospace System Engineering
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    • v.1 no.1
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    • pp.16-20
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    • 2014
  • Recently, various kinds of study on light weight structure are performing in the world. The Al honeycomb sandwich structural type adopt for improvement of lightness and structural stability to major part structure of aircraft or spacecraft. Adhesion badness properties of adhesive and adhesion properties of fillet mainly studied about al honeycomb structure. But study for adhesive properties of sandwich construction with surface treatment of Aluminum alloy barely performed. In this study, adhesive film was used between Al and honeycomb core of honeycomb panel[1]. The study for adhesive properties of sandwich construction with surface treatment of AA 5052 skin was performed.