• Title/Summary/Keyword: Al evaporation

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Corrosion resistance of double Al-Mg coating films on steel sheet prepared by PVD method (PVD법에 의해 제작된 Al-Mg 이층 코팅막의 내식특성)

  • Im, Gyeong-Min;Lee, Seul-Gi;Jeong, Jae-In;Yang, Ji-Hun;Lee, Myeong-Hun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2013.05a
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    • pp.150-150
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    • 2013
  • Al-Mg films were prepared onto steel sheet according to deposition condition by eco-friendly electron beam vacuum evaporation method. The influence of Al-Mg films on corrosion resistance was evaluated by salt spray test and electrochemical method etc.. From the experimented results, it was found that the Al-Mg films which showed good corrosion resistance tend to have fine structure with homogenious composition distribution. In addition, it was shown that the property of coating films can be improve by controlling thickness ratio and uniform distribution of intermetallic compounds in Al-Mg films.

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Hydrogen Absorption Characteristics of Al/Pd Film (Al/Pd 박막의 수소 흡수 특성)

  • Cho, Young-Sin
    • Journal of Hydrogen and New Energy
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    • v.17 no.2
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    • pp.234-240
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    • 2006
  • Al film(135.5 nm thick) with Pd film(39.6 nm thick) on the top of it was made by thermal evaporation method. Hydrogen absorption of Al/Pd film was measured by quartz crystal microbalance(QCM) method at room temperature. The sample was activated by hydrogen absorption and desorption cycling at room temperature. Hydrogen was introduced into the film by increasing hydrogen gas pressure step by step up to 640 torr at room temperature. Hydrogen concentration reached up to 25% at $5{\sim}10$ torr. But at high pressure the concentration decreased. This strange tendency was not understood yet. Further study is needed to find out the mechanism of hydrogen absorption in Al in Al/Pd film.

Characterization of CIGS Solar Cell for Flexible Steel Substrate by Surface Roughness (유연 철강기판 표면조도에 따른 CIGS 태양전지의 특성 분석)

  • Kim, Daesung;Hwang, Moonsick;Kim, Daekyong;Lee, Duckhoon;Kim, Taesung
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.11a
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    • pp.58.1-58.1
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    • 2011
  • CIS(CuInSe2)계 화합물 태양전지는 높은 광흡수계수와 열적 안정성으로 고효율 태양전지 제조가 가능하여 태양전지용 광흡수층으로 매우 이상적이다. 미국 NREL에서는 이러한 CIGS 태양전지를 Co-evaporation 방법으로 제조 20%이상의 에너지 변환 효율을 달성하였다고 보고하였다. CIGS 태양전지의 경우 기존의 유리 기판 대신 유연한 철강 기판을 사용해 태양 전지를 flexible하게 제조 할 수 있다는 장점이 있다. 이러한 flexible 태양전지의 경우 기존의 rigid 태양전지의 적용분야 뿐만 아니라 BIPV, 선박, 장난감, 군용, 자동차등 더욱 더 많은 분야에 활용이 가능하다. 본 연구에서는 기존의 rigid한 기판인 soda lime glass와 flexible 기판인 stainless steel 기판으로 소자를 제조하여 효율을 비교 분석 및 stainless steel 기판의 표면 처리 방법에 따라서 표면 조도의 특성을 분석하여 stainless steel 기판별 효율 특성도 비교 분석 하였다. 후면전극으로는 약 $1{\mu}m$의 Mo를 DC Sputtering 방법을 이용하여 증착하였고, CIGS 광흡수층은 약 $2.5{\mu}m$의 두께로 미국의 NREL과 같은 3 stage 방식을 이용하여 광흡수층을 Co-Evaporation 방법으로 제조하였고, 버퍼층인CdS는 약 50nm의 두께로 CBD 방법으로 제조 하였으며, 창층인 ZnO는 약 500nm 두께로 RF Sputtering 방법으로 제조 하였고, 마지막으로 약 $1{\mu}m$ 두께의 Al 전면전극은 Thermal Evaporation 방법으로 제조 하였다. 소자의 물리적, 전기적 특성을 분석하기위해 FE-SEM, AFM, Solar Cell Simulator 분석을 실시하였다.

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Effects of flow direction on the performance of an indirect evaporative cooler (유동 방향이 간접 증발식 냉각기 성능에 미치는 영향)

  • Choo, Hyun-Seon;Lee, Kwan-Soo;Lee, Dae-Young
    • Proceedings of the SAREK Conference
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    • 2006.06a
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    • pp.743-748
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    • 2006
  • Ren et al. analyzed the performance of the indirect evaporative cooler according to the direction of the flow considering evaporation water flow and wetness. However the effect of NTU of each channel on the performance of the indirect evaporative cooler according to the direction of the flow was not analyzed exactly. In this study the effect of the direction of the flow on the Indirect evaporative cooling performance changing NTU of each channel are investigated theoretically. The cooling process of the indirect evaporative cooler by flow direction is modeled into a set of linear differential equations and solved to obtain the exact solutions to the temperatures of the hot fluid, the moist air, and evaporation water. Based on the exact solution in the case of different NTU of each channel, we study the change of the distribution of the temperature according to each flow direction and at the same time analyze the effect of the flow direction on the cooling performance.

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Effect of Electrode Formation Process using E-beam Evaporation on Crystalline Silicon Solar Cell (E-Beam evaporation을 이용한 전극 형성 공정이 결정질 실리콘 태양전지에 미치는 영향 분석)

  • Choi, Dongjin;Park, Se Jin;Shin, Seung Hyun;Lee, Changhyun;Bae, Soohyun;Kang, Yoonmook;Lee, Hae-Seok;Kim, Donghwan
    • Current Photovoltaic Research
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    • v.7 no.1
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    • pp.15-20
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    • 2019
  • Most high-efficiency n-type silicon solar cells are based on the high quality surface passivation and ohmic contact between the emitter and the metal. Currently, various metalization methods such as screen printing using metal paste and physical vapor deposition are being used in forming electrodes of n-type silicon solar cell. In this paper, we analyzed the degradation factors induced by the front electrode formation process using e-beam evaporation of double passivation structure of p-type emitter and $Al_2O_3/SiN_x$ for high efficiency solar cell using n-type bulk silicon. In order to confirm the cause of the degradation, the passivation characteristics of each electrode region were determined through a quasi-steady-state photo-conductance (QSSPC).

Fabrication of $Al_2O_3$ nanotube with etching core material of one-dimensional ZnO/$Al_2O_3$ core/shell structure (1차원 ZnO/$Al_2O_3$ core/shell 구조에서 core 물질 식각방법에 의한 $Al_2O_3$ 나노튜브제작)

  • Hwang, Joo-Won;Min, Byung-Don;Lee, Jong-Su;Kim, Sang-Sig
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.37-40
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    • 2003
  • Amorphous $Al_2O_3$ nanotubes have been fabricated by utilizing the ZnO nanowires as template with wet etching method. ZnO nanowires synthesized by thermal evaporation are conformally coated with $Al_2O_3$ by atomic-layer deposition(ALD) method. The $Al_2O_3$-coated ZnO nanowires are of core-shell structure; ZnO core nanowires and $Al_2O_3$ shells. When the $ZnO/Al_2O_3$ core-shell structure is dipped in $H_3PO_4$ solution at $25^{\circ}C$ for a 6 min, the core ZnO materials are completely etched, and only $Al_2O_3$ nanotubes are remained. This nanotube fabrication is technically easier than others, and simply approachable. Transmission electron microscopy shows that the $Al_2O_3$ nanotubes have various thicknesses that can be controlled.

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High Temperature Oxidation of Thermomechanically Treated Ti-45.4%Al-4.8%Nb Alloys (열기계적 처리한 Ti-45.4%Al-4.8%Nb 합금의 고온산화)

  • Kim Jae-Woon;Lee Dong-Bok
    • Korean Journal of Materials Research
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    • v.14 no.7
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    • pp.457-461
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    • 2004
  • The thermomechanically treated $Ti-45.4\%Al-4.8\%Nb(at\%)$ alloy was oxidized between 800 and $1000^{\circ}C$ in air, and the oxidation characteristics were studied. The dissolution of Nb in the oxide scale was observed from the TEM study. The Pt marker test revealed that the oxidation process was controlled by the outward diffusion of Ti ions and the inward diffusion of oxygen ions. During oxidation, the evaporation of Nb-oxides was found to occur to a small amount. Niobium tended to pile-up at the lower part of the oxide scale, which consisted primarily of an outer $TiO_2$ layer, and an intermediate $Al_{2}O_{3}-rich$ layer, and an inner mixed layer of ($TiO_{2}+Al_{2}O_{3}$).

Electrical Characteristic Change of Al/Pd Film by Hydrogen Gas (수소 기체에 의한 Al/Pd 박막의 전기 특성 변화)

  • Cho, Young-Sin
    • Journal of Hydrogen and New Energy
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    • v.16 no.4
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    • pp.386-390
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    • 2005
  • Al film(135.5 nm thick) with Pd film(39.6 nm thick) on the top of it was made by thermal evaporation method. Electrical resistance change due to hydrogen absorption and desorption was measured by four point measurement method. The sample was activated by hydrogen absorption and desorption cycling at room temp. Hydrogen was introduced into the film by increasing hydrogen gas pressure step by step up to 640 torr at room temp. The resistance change ratio was decreased to 12 % with increasing hydrogen pressure in contrast to normal metal behavior. This strange tendency was not understood yet. Further study is needed to find out the mechanism of hydrogen absorption in Al in Al/Pd film.

The Optical Properties of $ZnS/Na_3AlF_6$ Multi-layer Thin Films with Different Optical Thickness ($ZnS/Na_3AlF_6$ 다층박막의 광학적 두께 변화에 따른 광특성)

  • Jang, Gang-Jae;Jang, Geon-Ik;Lee, Nam-Il;Im, Gwang-Su
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.04a
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    • pp.128-129
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    • 2007
  • $ZnS/Na_3AlF_6$ multi-layer thin film were produced by evaporation system. ZnS were selected as a high refractive index material and $Na_3AlF_6$ were selected as low refractive index material. Optical properties including color effect were systematically studied in terms of different optical thickness by spectrophotometer. In oder to compare with experimental data, the Essential Macleod Program(EMP) was adopted that simulation program. The thin film consisting of $ZnS/Na_3AlF_6$ multi-layer show the wave length of $530{\sim}600nm$, typically color range between purple, blue, green. It was confirmed that this experimental result was well matched with simulation data.

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A study on Brazing Interfacial Properties of $Al_2O_3/Al$ 6061 ($Al_2O_3/Al$ 6061의 접합부 계면특성에 관한 연구)

  • Seo, S.Y.;An, B.G.;Lee, K.Y.
    • Journal of Power System Engineering
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    • v.7 no.3
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    • pp.74-79
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    • 2003
  • Alumina($Al_2O_3$) and Al 6061 were brazed by using Al-12wt% Si filler metal in a high vacuum environment. The interfacial microstructure and mechanical properties of the joints were investigated. The results obtained were as follows. (1) The maximum tensile strength of 54Mpa was acquired at the processing conditions of high vacuum ($3{\times}10^{-6}Torr$), $620^{\circ}C$ and 10min, but this condition will not be used in the industrial area due to high evaporation of Al alloy composition. (2) Reaction products for holding time and brazing temperature worked as stress relieve layer and the fractures after the mechanical properties test were occurred to the ceramic side or reaction layer. (3) The glancing angle X-ray diffraction analysis for the reaction product of $Al_2O_3/Al$ 6061 were processed. the joint strengths were low due to existed $Al_2Si_5\;and\;SiO_2$.

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