• Title/Summary/Keyword: Ag+ solution

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Surface Treatment of Dielectric Ceramic Resonator for High Frequency Devices (고주파용 유전체 세라믹 공진기의 표면처리)

  • Park, Hae-Duck;Kang, Sung-Goon
    • Korean Journal of Materials Research
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    • v.11 no.11
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    • pp.923-928
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    • 2001
  • An electrolytic silver plating process has been successfully developed for terminated electrode parts of dielectric ceramic resonator. High adhesion strength and high Qu is obtained and blister occurance is minimized under plating condition with $HNO_3$750 $m\ell/\ell$ and HF $ 250m\ell/\ell$ solution at $25^{\circ}C$ for 20 minutes. Adhesion strength has the highest value, 3.2 kg/mm$^2$ at etching temperature of $25^{\circ}C$. Adhesion strength, Qu and blister occurance are monotonically increased with the thickness of electrodeposition layer. In case of electrodeposition of Ag, Qu value of 380 has obtained higher than in case of electrolytic Cu plating with Qu value of 325. Therefore, terminated electrode parts of dielectric ceramic resonator reducing dielectric loss can be obtained using prensent process.

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Fabrication of fine BSCCO-2223 precursor powder by spray pyrolysis process (분무 열분해방법에 의한 미세 BSCCO-2223 전구분말의 제조)

  • 김성환;유재무;고재웅;김영국;박기호
    • Progress in Superconductivity
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    • v.5 no.1
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    • pp.65-69
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    • 2003
  • Many researches on fabrication process for BSCCO precursor powders have been developed for high J$_{c}$ BSCCO-2223 tape. Spray pyrolysis method for fabrication of precursor powder has many advantages, such as high purity, fine particle size and low carbon content of BSCCO precursor powder. Fine, spherical powders were prepared by ultrasonic spray pyrolysis from the aqueous solution of metal nitrates. BSCCO precursor powders were synthesized with various solutes concentration and heat treatment conditions. Average particle size for spray pyrolysis powders was $1.5∼3\mu\textrm{m}$. Bi-2223/Ag tape was prepared by PIT method and followed by various sintering conditions. BSCCO precursor powders were characterized by XRD, SEM, EDS, Carbon content and particle size analysis.s.

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A Study on Project Scheduling under Multiple Resource Constraints (다수 자원제약 하에서의 프로젝트 일정계획에 관한 연구)

  • Lee, Jeong-Hun;Kim, Pan-Sool;Moon, Il-Kyeong
    • Journal of Korean Institute of Industrial Engineers
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    • v.36 no.4
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    • pp.219-229
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    • 2010
  • The PERT/CPM are considered as the base procedures for the most successful project scheduling programs. Unfortunately, it is not easy to apply these procedures to real-life projects. This is due to the fact that PERT/CPM assume an infinite number of resources for each activity in project networks. Obviously, the completion time under no constraints is less than when constraints are imposed. One way of approaching this problem is to use heuristic solution techniques. In this paper, we present three heuristics; MRU (Maximum Resource Use) rule, STU (Shortest Time Use) rule, MRUP (Max Resource Use and Period) rule for allocating resources to activities of projects under multiple resource constraints. Comparisons of the project durations show that these heuristic rules are superior to AG3 rule that has been widely used in practice (Elsayed and Boucher, 1994).

THE STUDY ON THE MICROCRYSTAL GROWTH OF SILVER HALIDE IN PHOTOGRAPHIC EMULSION WITH MODIFIERS

  • Kang, Tai-Sung;Ahn, Hong-Chan;Park, In-Yeong;Kim, Chan-Rae
    • Journal of Photoscience
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    • v.1 no.1
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    • pp.63-66
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    • 1994
  • Silver chlorobromoiodide cubic seed emulsion was prepared'in the presence of ammonia and phenylcarbamyl gelatin solution. When benzenethiosulfonate sodium salt (BTS) and 4-hydroxy6-methyl-1,3,3a,7-tetraazaindene (TAI), as growth modifiers, were added in the seed emulsion, the silver halide microcrystals were obtained in the forms of cubo-octahedrons, octahedrons, rhombic dodecahedron by variation of pAg value through controlled double jet. The crystal habits and shapes were determined by means of X-ray diffraction (D/MAX BIB, Rigaku) and electron microscopy (JSM-840, JEOL), respectively.

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A Study on the Preparation of Antibacterial Biopolymer Film

  • Cho, Dong-Lyun;Na, Kun;Shin, Eun-Kyung;Kim, Hyun-JIn;Lee, Ki-Young;Go, Jin-Hwan;Choi, Choon-Soon
    • Journal of Microbiology and Biotechnology
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    • v.11 no.2
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    • pp.193-198
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    • 2001
  • Preparation of antibacterial biopolymer film which is suitable for food packaging film was investigated using K-carrageenan as a base material. K-Carrageenan showed good biodegradability and film-forming characteristic but poor mechanical properties under humid condition. Also, various bacteria grew well on its surface. The poor mechanical properties could be improved by mixing with alginate at a 1:1 ratio and crosslinking with $CaCl_2$ solution. Antibacterial property coul be provided by modifying the K-carrageenan film surface with acrylic acid plasma followed by ion-exchange with $Ag^+$ ions. Such prepared film still showed good biodegradability by various fongi.

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Numerical modelling and finite element analysis of stress wave propagation for ultrasonic pulse velocity testing of concrete

  • Yaman, Ismail Ozgur;Akbay, Zekai;Aktan, Haluk
    • Computers and Concrete
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    • v.3 no.6
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    • pp.423-437
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    • 2006
  • Stress wave propagation through concrete is simulated by finite element analysis. The concrete medium is modeled as a homogeneous material with smeared properties to investigate and establish the suitable finite element analysis method (explicit versus implicit) and analysis parameters (element size, and solution time increment) also suitable for rigorous investigation. In the next step, finite element analysis model of the medium is developed using a digital image processing technique, which distinguishes the mortar and aggregate phases of concrete. The mortar and aggregate phase topologies are, then, directly mapped to the finite element mesh to form a heterogeneous concrete model. The heterogeneous concrete model is then used to simulate wave propagation. The veracity of the model is demonstrated by evaluating the intrinsic parameters of nondestructive ultrasonic pulse velocity testing of concrete. Quantitative relationships between aggregate size and testing frequency for nondestructive testing are presented.

A trail on detection of Sb and As (미량의 As 와 Sb를 분리확인하는 실험)

  • 이명연;김유감
    • YAKHAK HOEJI
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    • v.3 no.1
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    • pp.45-47
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    • 1957
  • A paper chromatographical method is studied to detect As and Sb from a mixed sample applying the principle of Gutzeit's. After spoting the mixed $AsH_3$ sample on the $AgNO_3$ band of paper strip (6 mm $\times$ 300 mm of Whatman No.52 or Toyo No.2 filter paper), the strip is developed by ascending method using N-HCl solution as a developing soluvent. The color spot detection of As and Sb is done by exposing the dried chromatogram to $H_2S$ stream. According to the experiments, the detectable minimum range of As is 3 micrograms and that of Sb is 15 micrograms. The yellow phosphorous interfers to the color spot detection of As and Sb, so that, previously the most of yellow phosphorous from the sample should be removed out.

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manufacturing micro CPL (Capillary Pumped Loop)by using LIGA process (LIGA process를 이용한 micro CPL(Capillary Pumped Loop)제작)

  • Cho, Jin-Woo;Jung, Suk-Won;Park, Joon-Shik;Park, Sun-Seob
    • Proceedings of the KIEE Conference
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    • 2001.07c
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    • pp.1881-1883
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    • 2001
  • We manufactured a micro CPL by LlGA process, a new conceptual ultra-fine and precise forming method, using X-ray lithography process. We fabricated a BN X-ray mask having properties of good X-ray transmittance and large mechanical strength. Micro CPL was manufactured by dividing into an upper plate and a low plate. Each of plates was bonded by Ag paste screen printing. The upper plate was fabricated on glass wafer to observe flow and phase transformation of cooling solution. The lower plate was manufactured by Cu electroplating for good heat transmission. Precision of inner Parts, micro pin and micro channel, of manufactured micro CPL is under ${\pm}2{\mu}m$.

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Ni/Cu Metallization for High Efficiency Silicon Solar Cells (Ni/Cu 전극을 적용한 고효율 실리콘 태양전지의 제작 및 특성 평가)

  • Lee, Eun-Joo;Lee, Soo-Hong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.12
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    • pp.1352-1355
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    • 2004
  • We have applied front contact metallization of plated nickel and copper for high efficiency passivated emitter rear contact(PERC) solar cell. Ni is shown to be a suitable barrier to Cu diffusion as well as desirable contact metal to silicon. The plating technique is a preferred method for commercial solar cell fabrication because it is a room temperature process with high growth rates and good morphology. In this system, the electroless plated Ni is utilized as the contact to silicon and the plated Cu serves as the primary conductor layer instead of traditional solution that are based on Ti/Pd/Ag contact system. Experimental results are shown for over 20 % PERC cells with the Plated Ni/Cu contact system for good performance at low cost.

Interfacial Properties of $\gamma-Alumina/KCI^{(ag)}$ Electrical Double Layer ($\gamma$-알루미나/KCl 수용액의 전기 이중층에서 계면 물성)

  • 홍영호;함영민;장윤호
    • Journal of the Korean Ceramic Society
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    • v.31 no.6
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    • pp.678-684
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    • 1994
  • The surface of alumina is capable of acquiring a change when it is in an aqueous solution. This surface change will have a strong influence on the surrounding ions, particularly those of opposite change known as the counter ions. A site-binding model of the {{{{ gamma }}-alumina/KCl(aq) interface was used to calculated theoretical surface ionization constants and P.Z.C.(Point of zero change) of {{{{ gamma }}-alumina. This paper was carried out to investigate the effect of calcination temperature on the acidic and electrical properties of pure {{{{ gamma }}-alumina prepared by the precipitation method from the Al(NO3)3.9H2O and NH4OH. From the experimental data it was shown that {{{{ gamma }}-alumina have a mainly Br nsted acid site. However, the acidity of {{{{ gamma }}-alumina decreased with increasing calcination temperature at strength Ho +9.3. The surface charge density of {{{{ gamma }}-alumina was increased with electrolyte ionic strength and calcination temperature.

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