• Title/Summary/Keyword: Advanced chemical resistance test method

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Consideration of Geosynthetics Chemical Resistance Test for Long-Term Performance Evaluation (장기성능 평가를 위한 토목섬유 화학저항성 시험 고찰)

  • Jeon, Han-Yong;Jang, Yeon-Soo;Gong, Hak-Bong
    • Proceedings of the Korean Geotechical Society Conference
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    • 2009.03a
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    • pp.222-232
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    • 2009
  • In this study, the real site test conditions were considered and applied to suggest the improved test method for geosynthetics chemical resistance. For this, index and performance tests were done to specify and regulate the more approached test method. Accelerated model by Arrhenius equation was applied to interpretate the experimental data. Through analysis and comparison the overall experimental results, we could suggest the possibility and setup the advanced chemical resistance test method for geosynthetics.

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Consideration of Geosynthetics Chemical Resistance Test for Long-Term Performance Evaluation (장기성능 평가를 위한 토목섬유 화학저항성 시험 고찰)

  • Jeon, Han-Yong;Jang, Yeon-Soo
    • Journal of the Korean Geotechnical Society
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    • v.25 no.7
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    • pp.55-64
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    • 2009
  • In this study, improved test methods, which consider the real site test conditions, were suggested to measure for geosynthetics chemical resistance. For this purpose index and performance tests were done to specify and regulate the test method most approaching to the installation condition and accelerated model by Arrhenius equation was applied to interpretate the experimental data. Through the analysis and comparison of the overall experimental results, we could suggest the possibility and setup of the advanced chemical resistance test method for geosynthetics fitting to the field installation conditions.

Effects of Heat Treatment on Surface Properties of Aluminum 6061 Alloy After Anodization (알루미늄 6061 합금 양극산화 후 열처리에 따른 표면 특성 관찰)

  • Seungmin, Lee;Chanyoung, Jeong
    • Corrosion Science and Technology
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    • v.21 no.6
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    • pp.495-502
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    • 2022
  • Anodization is a representative electrochemical surface treatment method that can improve both heat resistance and corrosion resistance by forming an anodization film on the surface of the aluminum. However, these properties can be changed after an additional heat treatment process. In this study, Al 6061 was subjected to an anodization process at 60 V for 1 hour, 5 hours, or 9 hours. An additional heat treatment process was performed at 500 ℃ for 30 minutes. Field emission scanning electron microscopy (FE-SEM) analysis revealed that the thickness of the anodized film was increased in proportion to the anodization time. Both pore size and pore diameter of the anodized film was also increased after anodization. After an additional heat treatment process, there were no significant changes in the thickness, pore size, or pore diameter of the anodized film. Heat resistance was confirmed through thermal analysis and chemical resistance was evaluated with a potentiodynamic polarization test.

An Electro-chemical Combined-stress Degradation Test of Rubber for Automotive Radiator Hoses (자동차 냉각기 호스용 고무의 전기화학적 복합노화시험)

  • Kwak, Seung-Bum;Seo, Boo-Seok;Choi, Nak-Sam
    • Transactions of the Korean Society of Automotive Engineers
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    • v.19 no.4
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    • pp.107-113
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    • 2011
  • Coolant rubber hoses for automotive radiators under thermal and mechanical loadings can be degraded and thus failed due to the influences of the locally formed electricity. In this study, an advanced test method was developed to simulate the failure problem of the rubber hose. For carbon black filled EPDM (ethylene-propylene dine monomer) rubber used as a radiator hose material the ageing behaviors by the electro-chemical stresses combined with a tensile strain were analyzed. As the tensile strain increased, the current of the rubber specimen reduced indicating an increase of the internal defects and electrical resistance of the rubber specimen. Elongation at break and IRHD hardness rapidly decreased with increasing the ageing time. Both electro-chemical stress and mechanical tensile stress clearly accelerated the degradation of EPDM rubber.

An Electrochemical Study on the Corrosion Resistance Improvement of Galvanizing Steel by Dipping to Solution with Inhibitor (인히비터 첨가용액의 침지에 의한 용융아연도금 강판의 내식성 개선에 관한 전기화학적 연구)

  • Moon, Kyung-Man;Cho, Hwang-Rae;Kang, Tae-Young;Lee, Myung-Hoon;Kim, Yun-Hae
    • Journal of Advanced Marine Engineering and Technology
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    • v.31 no.2
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    • pp.173-181
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    • 2007
  • Recently, galvanizing method is predominantly being used not only a economical point of view but also due to it s stability and long life. For example, guard rail of high way, all kinds of structures for ship etc. were protected with galvanizing and demand of galvanized structural materials was being increased with more and more. However, galvanized structures were inevitably being deteriorated with time eventually because they were corroded with solution of galvanizing film and exfoliation of it s film in the present severe corrosive environment. Therefore, it is necessary to improve the corrosion resistance of the galvanizing film through various methods such as variation of chemical composition of galvanizing bath, chromate treatment and coating treatment. In this study, three test specimens such as pure galvanizing, galvarium, and chromate treatment were submerged at tap water with inhibitor addition. And the effect of their corrosion resistance improvement was comparatively investigated with electrochemical method. Corrosion current density of the galvanized steel was the largest among three specimens, however, the galvarium steel showed the lowest corrosion current density. Futhermore, these three kinds of test specimens indicated considerably excellent corrosion resistance by dipped at tap water with inhibitor addition. Especially, the galvanized steel showed the best effect of corrosion resistance improvement than other test specimens.

Development of MBR System Commercialization Technology Using a Membrane with a Good Fouling Resistance (막 오염 저항성이 우수한 분리막을 이용한 MBR 시스템의 실증화 기술개발)

  • Choi, J.H.;Lee, J.B.;Kim, I.C.
    • Membrane Journal
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    • v.18 no.1
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    • pp.35-43
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    • 2008
  • In this study, we tried to solve membrane fouling with membranes made by fine nano-particle in MBR process. And we confirmed good fouling resistance in pilot test. In this test, we confirmed our membrane with titania out-standing quality by testing in the pilot long-term test by comparing to other company product. Our membrane keep up steadily $20{\sim}25 L/m^2{\cdot}hr$ high flux in $7,000{\sim}13,000mg/L$ MLSS high sludge concentration. In addition to this quality, we studied membrane flux character related membrane arrangement, membrane-air line arrangement, air-line hole size, cleaning solution concentration, treatment method, etc. Using the optimization of this additional parameter, we tried to search method of maximizing membrane quality.

The Corrosion Behavior Study by AC Impedance Method for the Aging Heat Treated Nimonic 80A Superalloy (교류임피던스법에 의한 Nimonic 80A 초내열합금 시효열처리재의 부식거동 고찰)

  • 백신영
    • Journal of Advanced Marine Engineering and Technology
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    • v.23 no.6
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    • pp.761-769
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    • 1999
  • In this paper the effect of aging heat treatment to the Corrosion behavior for the Nimonic 80A superalloy was studied by AC Impedance methods. Tested solution was 3.5% with tempera-ture $25^{\circ}C$ Electro-chemical corrosion test were carried out for the Nimonic 80A super-alloy which solution heat treated at $1080^{\circ}C$ for 8 hours followed by aging heat treated at $650^{\circ}C,\;700^{\circ}C,\;750^{\circ}C\;800^{\circ}C$ and $850^{\circ}C$ with 16hours under vacuum environment. The obtained results were as follows; 1. Base metal and solution-treated materials were exhibited similar corrosion tendency as Ran-dle equivalent cell. The value of passive film resistance was 579 ohms for the base metal and 124,770 ohms for the solutionized metal such a difference was arose by the ${{\gamma}_^'}$ precipitate on the metal surface during heat treatment. 2. The measure value of $R_p$ for heat-treated at $650^{\circ}C,\;700^{\circ}C,\;800^{\circ}C$and $850^{\circ}C$ were 97,943, 93, 111, 26,961, 15,798 and 11,780ohm respectively. Which indicated that the passive film resistance Rp was reduced as aging temperature increased due to the growth of grain size and sensitization at the grain boundary. 3. The similar tendency was exhibited for corrosion behavior of the electro-chemical corrosion polarization method and AC impedance method and confirmed that AC impedance method was useful tool for corrosion research.

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Significant Attenuation of Aden-associate Virus Gene Expression by Catechol-conjugated Heparin Surface Coating (카테콜기가 도입된 헤파린의 표면고정화에 의한 아데노연관바이러스의 발현 억제에 관한 연구)

  • Do, Minjae;Lee, Slgirim;Jang, Jae-Hyung;Lee, Haeshin
    • Journal of Adhesion and Interface
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    • v.17 no.4
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    • pp.149-154
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    • 2016
  • In this study, natural polymer-based virus neutralizing agent was developed in an attempt to replace the conventional sterilization method for mammalian cell culture. A catechol conjugated heparin was synthesized by using EDC chemistry, and it show unique binding ability to virus which has heparin affinity (adenovirus, adeno-associated virus). To evaluate neutralization ability of catechol conjugated heparin, adeno-associated virus was used for test model, instead of using a pathogenic virus. The catechol conjugated heparin exhibited resistance to high concentration of salt and complete inactivation of adeno-associated virus. The result suggests that the catechol conjugated heparin, which is biocompatible and efficiency, may replace conventional sterilization method for mammalian cell culture.

Electrochemical Combined-Stress Degradation Test and Failure Mechanisms of EPDM Rubber for Automotive Radiator Hoses (자동차 냉각기 호스용 EPDM 고무의 전기화학적 복합노화시험 및 고장메커니즘)

  • Kwak, Seung Bum;Choi, Nak Sam;Shin, Sei Moon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.1
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    • pp.1-8
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    • 2013
  • Coolant rubber hoses for automotive radiators can degrade under thermal and mechanical loadings and thus fail owing to the influences of locally formed electricity. In this study, an advanced test method was developed to simulate the failure of a rubber hose. The aging behavior of carbon-black-filled ethylene-propylene diene monomer (EPDM) rubber used as a radiator hose material under a combination of electrochemical stresses and tensile strain was analyzed. The changing behaviors of the current and the resistance as a function of the aging time were analyzed in consideration of the tensile strain, voltage, and aging temperature. Sectioned specimens clarified the failure mechanisms of the aged skin layer under the combined electrochemical stresses.

Influence of Sintering Additives and Temperature on Fabrication of LPS-SiC (액상소결법에 의한 탄화규소 제조시 소결조제와 온도의 영향)

  • JUNG HUN-CHAE;YOON HAN-KI
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2004.11a
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    • pp.266-270
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    • 2004
  • SiC materials have been extensively studied for high temperature components in advanced energy system and advanced gas turbine because it has excellent high temperature strength, low coefficient of thermal expansion, good resistance to oxidation and good thermal and chemical stability etc. However, the brittle characteristics of SiC such as low fracture toughness and low strain-to fracture still impose a severe limitation on practical applications of SiC materials. For these reasons, SiC/SiC composites can be considered as a promising for various structural materials, because of their good fracture toughness compared with monolithic SiC ceramics. But, high temperature and pressure lead to the degradation of the reinforcing jiber during the hot pressing. Therefore, reduction of sintering temperature and pressure is key requirements for the fabrication of SiC/SiC composites by hot pressing method. In the present work, monolithic Liquid Phase Sintered SiC (LPS-SiC) was fabricated by hot pressing method in Ar atmosphere at $1800^{\circ}C$ under 20MPa using $Al_2O_3,\;Y_2O_3\;and\;SiO_2$ as sintering additives in order to low sintering temperature and sintering pressure. The starting powder was high purity $\beta-SiC$ nano-powder with all average particle size of 30mm. The characterization of LPS-SiC was investigated by means of SEM and three point bending test. Base on the composition of sintering additives-, microstructure- and mechanical property correlation, tire compositions of sintering additives are discussed.

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