• Title/Summary/Keyword: Adhesive properties

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Evaluation of the Change in Adhesion Strength of GFRP and CFRP with Carbon Nanotube Contents in Epoxy Adhesive with Moisture Change during Curing (에폭시 접착제의 탄소나노튜브 함량과 경화시 습도 변화에 따른 GFRP 및 CFRP의 접착강도 변화 평가)

  • Park, Hee-Woong;Kim, Jong-Hyun;Park, Joung-Man
    • Journal of Adhesion and Interface
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    • v.23 no.1
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    • pp.1-7
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    • 2022
  • As the wind blades become larger, they tend to be made by mixing glass fiber and carbon fiber, and it is important to increase the properties of the adhesive which adheres the two materials. The physical properties of the adhesive vary depending on the content of the additive and curing conditions. In this study, the change in adhesion strength with the difference between the CNT (Carbon Nanotube) content of the epoxy adhesive and the humidity during curing was evaluated. GFRP and CFRP specimens were prepared and adhered using an epoxy adhesive, and to examine changes in characteristics with carbon nanotube contents and with the humidity during curing of the epoxy adhesive, adhesion strength was evaluated by dividing the difference between carbon nanotube content and humidity. To find out the change with the CNT contents, the intelaminar shear strength (ILSS) test was performed by dividing the contents of the CNT into 0, 0.1, 0.3, 0.5, and 1 wt%, and to confirm the change with the humidity conditions, the adhesive was cured by dividing the humidity by 20, 50, and 80%. From the result of the experiment, the adhesive force decreased when the content was excessively large, although the adhesive property was enhanced by adding CNT to the epoxy adhesive. In addition, it was confirmed that the adhesion characteristics were not changed as the humidity increased.

A Study on the Strength Evaluation and Defect Detection Capability of Adhesive Joint with CNTs (CNT를 첨가한 접착조인트의 결함탐지능 및 강도 평가에 관한 연구)

  • Kim, Tae-Hyeong;Kim, Cheol-Hwan;Choi, Jin-Ho
    • Composites Research
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    • v.31 no.4
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    • pp.151-155
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    • 2018
  • Mechanical joint and adhesive joint are two typical joining methods for structures. The adhesive joints distribute the load over a larger area than mechanical joints and have excellent fatigue properties. However, the strength of adhesive joint greatly depends on the environmental conditions and the skill of the operator. Therefore, there is a need for techniques to evaluate the quality of the adhesive joints. The electric resistance method is a very promising technique for detecting defects by measuring the electrical resistance of an adhesive joint in which CNTs are dispersed in an adhesive. In this study, Aluminium-Aluminium adhesive single lap joint specimens were fabricated by using the adhesive dispersing CNTs using a sonicator and a 3-roll mill, and the static strengths and defect detection capabilities of the joints using the electrical resistance method were evaluated according to the CNTs content.

A Study on Improvement of Thermal and Adhesion Properties of Stone/Wood Composites for Stone Bed using CNT-epoxy Adhesive (CNT/Epoxy 접착제를 이용한 돌침대용 석재/목재 복합재의 열적특성 및 접착특성 개선 연구)

  • Kim, Jong-Hyun;Shin, Pyeong-Su;Kwon, Dong-Jun;Moon, Sun-Ok;Park, Joung-Man
    • Composites Research
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    • v.29 no.5
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    • pp.276-281
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    • 2016
  • Improvement of the thermal and adhesion properties of stone/wood composites was studied. Tensile test was performed for wood and stone to know the basic mechanical properties. Real-time temperature of stone and wood was measured when stone and wood was heated. To compare thermal transfer properties of stone/wood composites, two types of specimens were tested: one was stone upper whereas another was wood upper. Real time temperature measurement and lap shear test were performed to know thermal and adhesion properties by using CNT-epoxy adhesive in which CNT was dispersed in epoxy adhesive uniformly. The thermal transfer property was better for the wood upper case than stone upper case. Adding CNT improved the heat transfer as well as mechanical properties including lap shear strength.

Physicomechanical Properties Enhancement of Fast-Growing Wood Impregnated with Wood Vinegar Animal Adhesive

  • Efrida BASRI;SAEFUDIN;Mahdi MUBAROK;Wayan DARMAWAN;Jamal BALFAS;Yelin ADALINA;Yusuf Sudo HADI
    • Journal of the Korean Wood Science and Technology
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    • v.51 no.6
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    • pp.542-554
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    • 2023
  • This study is a continuation of our previous work, which focused on the resistance of jabon wood to termites after impregnation with wood vinegar (WV) and animal-based adhesive (kak). This paper presents the physicomechanical properties of fast-growing jabon wood impregnated with kak at two concentrations (8% and 10%) in wood vinegar or water as a solvent with and without 4% borax. The physical properties of the impregnation solution, that is, viscosity, density, pH, and solid content, were evaluated according to SNI 06-4567-1998. Some physical parameters, such as weight percent gain (WPG), density, water uptake, anti-swelling efficiency (ASE), crystallinity, and mechanical properties, i.e., modulus of elasticity (MOE), modulus of rupture (MOR), and compression strength parallel to the grain (CS), of the impregnated wood were determined. Based on these results, wood impregnated using a mixture of kak in WV presented better physical (increased WPG, density, dimensional stability, and crystallinity) and mechanical (increased MOE/MOR and compression strength) properties than wood impregnated with a water solvent or untreated wood. The wood impregnated using WV and water solvent improved the physical and mechanical properties. The density of the wood increased by 44%-58% and 32%-47%, ASE radial-tangential increased by 38%-45%; 15%-28% after 24 h of water immersion, crystallinity increased by 59%-74%; 36%, MOE increased by 46%-57%; 28%-31%, MOR increased by 29%-34%; 14%-27%, and compression strength increased by 40%-76%; 38%-72% values to untreated wood.

Adhesion Properties of UV-curable Acrylic PSA Tape for Automotive Sidemolding and Emblem (자동차용 사이드 몰딩과 엠블럼 적용을 위한 UV 경화형 아크릴 점착 테이프의 점착물성)

  • Park, Ji-Won;Lee, Seung-Woo;Kim, Hyun-Joong;Won, Dong-Bok;Kim, Dong-Bok;Lee, Kang-Shin;Woo, Hang-Soo;Kim, Eun-Ah
    • Journal of Adhesion and Interface
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    • v.12 no.3
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    • pp.81-87
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    • 2011
  • In this study, UV curing and crosslinking process was introduced for synthesis of acrylic foam tape that can be applied to the the automotive assembly process. Polymerized adhesive are laminated to baseform and varying the thickness of specimens were prepared. To measure basic mechanical properties, stainless steel was used. And in the test peel, dynamic shear and t-block were used. The acrylform adhesive show better results compare with typical adhesive and the properties depand on external factors - thick, wetting time -. To analysis functions of acrylic foam adhesive used to automobile production, evaluate the adhesive properties on the various plastic substrate. In PP and PE are categorized low surface energy materials, their properties have not been expressed. But dynamic shear tests show that some properties could be expressed by the difference break mechanism.

Adhesive Strength and Setting Shrinkage of UP Polymer Mortar Intermixed with Waste Rubber Powder (폐고무분말을 혼입한 UP 폴리머모르타르의 경화수축 및 부착강도)

  • Yeon, Kyu-Seok;Jin, Nan-Ji;Choi, Jong-Yun;Beck, Jong-Man
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 2003.10a
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    • pp.383-386
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    • 2003
  • In this study, the MMA-modified paste mixed waste rubber powder, which has a small elastic modulus and a large modification, was produced by using the soft unsaturated polyester resin(UP) as a binder. Then the adhesive properties according to the matrices in both underwater and air-dry conditions and the hardening shrinkage according to the contents of shrinkage reducing agent(SRA) and of MMA were surveyed. The experimental results show that, regardless of humidity of matrices the adhesive strength of polymer concrete was larger than cement concrete. the adhesive strength of MMA content of 20% was larger than MMA content of 30%. regardless of matrix materials the adhesive strength in water condition were $20{\sim}30%$ comparing with the air-dry condition. The case of MMA content of 20% showed the largest adhesive strength. In the hardening shrinkage experiment, the hardening shrinkage reduced as MMA and SRA contents increased, and the decrease of the hardening shrinkage by SRA was larger.

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AE Characteristics on Microscopic Failure Behavior of Carbon/Epoxy Comosite Prepared by Cocure and Precure Process (Cocure/Precure 경화공정에 의해 제조된 Carbon/Epoxy 복합재료의 미시적 파손거동에 대한 AE 특성)

  • Lee, Jin-Gyeong;Lee, Jun-Hyeon;Lee, Min-Rae;Choe, Heung-Seop
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.10 s.181
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    • pp.2520-2528
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    • 2000
  • Mechanical and physical properties of composite materials make a great difference due to their cure process condition. In order to clarify the effect of cure process condition on the microscopic damage behavior and failure mechanism of Carbon/Epoxy composites, three point bend test has been performed. For this purpose, two kinds of specimens with single adhesive and multiple adhesive layers were prepared. For single adhesive layer, four different types of specimen were used, that is, non-sanding, sanding, cocured, laminated specimens. Three different types of specimen were also used for the multiple adhesive layer, non-sanding, sanding, cocured specimens. Acoustic emission technique has also been employed to monitor the damage progresses associated with each micro-failure mechanism. The characteristics of AE parameters associated with micro-failure mechanism of each specimen were discussed.

Formulation and Pharmaceutical Properties of Transdermal Patch of Flurbiprofen (플루비프로펜 함유 경피 패취제의 제제설계 및 약제학적 성질)

  • 이계주;고유현;우종수;황성주
    • YAKHAK HOEJI
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    • v.43 no.4
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    • pp.447-457
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    • 1999
  • The purpose of this study is to prepare the adhesive type patch containing flurbiprofen, and to demonstrate the feasibility of flurbiprofen administration through the intact skin using adhesive type patch preparation. For this purpose, two pressure sensitive adhesives, Polyisobutylene(PIB) and $Gelva^{\circledR}737$, were selected from the chemical grade of polymers, and the adhesive type patches of flurbiprofen were prepared. The release rate of flurbiprofen from the PIB-based adhesive patch was higher than that from $Gelva^{\circledR}737$ based adhesive patch. The release rate of flurbiprofen from the PIB-based A-type patch with 1.0mm, 1.5mm or 2.0mm thicknesses followed the first order kinetics. In the skin permeation study, using male hairless mouse skin, a monophasic skin permeation profile was observed with 1% flurbiprofen loading dose. The inclusion of palmitic acid or SLS(0.25~0.5%) as an enhancer produced a remarkable enhancement in the skin permeation rate of flurbiprofen, and the percentile ratio of drug and enhancer appeared to be important for the effective enhancement. In the in vivo percutaneous absorption study, the plasma concentration of the optimal formulation was significantly (p<0.01) higher than that of the conventional cataplasma ($Bifen^{\circledR}$). These studies demonstrate a good feasibility of flurbiprofen administration through the intact skin using a transdermal patch, and show a possibility of the development of flurbiprofen patches.

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Effect of Curing Agent on the Curing Behavior and Joint Strength of Epoxy Adhesive (에폭시 접착제의 경화거동 및 접합강도에 미치는 경화촉매제의 영향)

  • Kim, Min-Su;Kim, Hae-Yeon;Yoo, Se-Hoon;Kim, Jong-Hoon;Kim, Jun-Ki
    • Journal of Welding and Joining
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    • v.29 no.4
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    • pp.54-60
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    • 2011
  • Adhesive bonding is one of the most promising joining methods which may substitute for conventional metallurgical joining processes, such as welding, brazing and soldering. Curing behavior and mechanical properties of adhesive joint are largely dependent on the curing agent including hardener and catalyst. In this study, effects of curing system on the curing behavior and single-lap shear strength of epoxy adhesive joint are investigated. Dihydrazide, anhydride and dicyandiamide(DICY) were chosen as hardener and imidazole and triphenylphosphine(TPP) were chosen as catalyst. In curing behavior, TPP showed the delay of the curing rate for DICY and ADH at $160^{\circ}C$, compared to imidazole catalyst due to the high curing onset/peak temperature. DICY seemed to be most beneficial in the joint strength for both steel and Al adherends, although the type of adherends affected the shear strength of epoxy adhesive joint.

Adhesive Membranes of Egg in Five Cobitid Species of Iksookimia (Pisces: Cobitidae) (참종개숙(lksookimia) 어류 5종의 난 부착막 구조)

  • 박종영;김익수
    • The Korean Journal of Zoology
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    • v.39 no.4
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    • pp.419-425
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    • 1996
  • The five spedes of genus Iksookimia from Korea were investigated by electron microscopes to clarify the adhesive membranes on zona radiata. In the late vitellogenic stage the adhesive membranes could be classified into three form as follows: 1) villous form of Iksookimia koreensis, I pumila, and I. hugowolfeldi, 2) cotton-shaped form of I. longicorpus, and 3) vine-shaped form of I. choii. And although I. koreensis, I pumila, and I. hugowolfeldi possessed the same villous form, It was evident that fine structure of the zona radiata varied according to spedes. The adhesive membranes and fine structures of zona radiata in Iksookimla showed a species specificity related to closely their habitats and spawning properties.

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