• Title/Summary/Keyword: Adhesive layer

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A Comparative Study on the Ultrastructures of the Egg Envelope in Fertilized Eggs of Fishes, Characidae, Three Species (카라신과 어류 3종의 수정란 난막 미세구조에 대한 비교 연구)

  • Kim, Dong-Heui;Reu, Dong-Suck;Deung, Young-Kun
    • Applied Microscopy
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    • v.26 no.3
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    • pp.277-291
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    • 1996
  • The structures of the egg envelope in fertilized eggs of three species of characidae, head and tail light fish (Hemigrammus ocellifer), black tetra (Gymnocorymbus ternetzi), and buenos aires tetra (Hemigrammus caudovittatus) were studied using light and electron microscopes. The fertilized eggs in all species were colorless, transparent, spherical and non-floted type. The egg envelopes have a single micropyle resembling the pathway of sperm in the area of the animal pole. The micropyle was surrounded by protruded lines of the egg envelope in a radiated form. Egg envelopes of fertilized eggs in both head and tail light fish and buenos aires tetra consisted of three distinct layers; an outer layer, a middle layer and an inner layer. And that of blacktetra consisted of two layers; an outer layer and an inner layer. Also, an outer layers of both head and tail light fish and black tetra were adhesive types but, in that of buenous aires tetra was non-adhesive type. An outer surface of egg envelope in black tetra was arranged by pores regularly. In that of head and tail light fish and buenos aires tetra have a rough side. An inner layer of egg envelope in fertilized eggs consisted of lamellae alternating with interlamellae of lower electron density; an inner layer of fertilized eggs in head and tail light fish consisted of three layers, that of black tetra was four layers, and that of buenos aires tetra was five layers.

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THE ADHESIVE PATTERNS OF COMPOMER TO SALIVA-CONTAMINATED DENTIN (타액에 오염된 상아질에 대한 콤포머의 접합양상)

  • Cho, Young-Gon;Kim, Byung-Tae;Lee, Suk-Jong
    • Restorative Dentistry and Endodontics
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    • v.25 no.4
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    • pp.575-586
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    • 2000
  • In this study, adaptation of compomer to saliva contaminated dentin was evaluated with scanning electron microscope(SEM) and confocal laser scanning microscope(CLSM). For the SEM study, the occulusal surfaces of thirty two molar teeth were grounded to exposure dentin surfaces. The specimen were randomly assigned to control and three experimental groups with four samples in each group. In control group, Dyract and F-2000 compomer were bonded on the specimens according to the manufactures direction. Experimental groups were subdivided into three groups. They were contaminated with saliva on dentin surfaces ; Experimental group 1 : Saliva was dried with compressed air. Experimental group 2 : Saliva was rinsed with air-water spray and dried. Experimental group 3 : After polymerization of an adhesive, they were contaminated with saliva, and then saliva was rinsed with air-water spray and dried. Dyract and F-2000 compomer were bonded on saliva-treated dentin surfaces. The interfaces between dentin and compomer were observed with SEM. For the CLSM study, Class V cavities were prepared in buccal and ligual surfacess of thirty two molars. The specimens were divided into control and experimental groups. Class V cavities in experimental group were contaminated with saliva and those surfaces in each experimental groups received the same treatments as for the SEM study. Cavities were applied Prime & Bond 2.1 and F-2000 compomer primer/adhesive that were mixed with fluorescein, and then were filled with Dyract and F-2000 compomer. Specimens were embedded in transparent acrylic resin and sectioned buccolingual1y with diamond wheel saw, and then mounted on cover slide for CLSM study. The interface between cavity and compomer was observed by fluoresence imaging with a CLSM. The results were as follows : 1. In SEM exammination of Dyract group, control group, experimental group 2, 3 showed close adaptation to dentin and hybrid layer of $3{\sim}4{\mu}m$ diameter. Interfacial gap between compomer and dentin in experimental group 1 was wider than in control group. 2. In SEM examination of F-2000 group, adaptation to dentin of control group was closer than Dytact control group, but hybrid-like layer was not observed. Interfacial gap between compomer and dentin in experimental group 1 was wider than in Dyract experimental group 1. 3. In dissolution specimens of Dyract and F-2000 group, resin tags penetrated through dentinal tubules in control group and experimental group 1 and 3, but the penetration of resin tag was irregular and partial in experimental group 1. 4. In CLSM exammination of Dyract and F-2000 group, adhesive patterns of control and experimental groups showed same as in SEM. This result suggests the treatment methods, rinsing & drying, repeating all adhesive procedures, will produce good effect on adaptation of compomer to dentin if the dentin surface or polymerized adhesive is contaminated by saliva.

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Effects of Rubber Loading on the Ultrasonic Backward Radiation Profile of Leaky Lamb Wave (고무 접합이 후방복사된 리키 램파 프로파일에 미치는 영향)

  • Song, Sung-Jin;Kwon, Sung-Duk;Jung, Min-Ho;Kim, Young-H.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.5
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    • pp.508-515
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    • 2002
  • The characterization of adhesive property in multi-layer materials has been hot issue for a long time. In order to evaluate adhesive properties, we constructed fully automated system for the backward radiation of leaky Lamb wave. The backward radiation profiles were obtained for the bare steel plate and plates with rubber-loading. The rf waveforms and frequency spectra of backward radiation show the characteristics of involved leaky Lamb wave modes. As the thickness of rubber-loading increased, the amplitude of profile at the incident angle of $13.4^{\circ}$ exponentially decreased. Scanning the incident position over the partially rubber-loaded specimen shows good agreement with the actual rubber-loading. The backward radiation of leaky Lamb wave has great potential to evaluate the adhesive condition as well as material properties of plates.

A Study for Creep Effect of the Interfacial Adhesive Layer on the Behavior of Concrete with CFRP (탄소섬유시트로 보강된 콘크리트 구조물 경계면 재료의 크리프 영향 해석)

  • Park, Yong Deuk;Shin, Seung Kyo;Kang, Suk Hwa;Lim, Yun Mook
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.30 no.3A
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    • pp.221-228
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    • 2010
  • External bonding of carbon fiber reinforced polymer (CFRP) sheets has been widely accepted as a popular method for strengthening of deteriorated RC structures. The long-term behavior of CFRP-strengthened RC structure is often affected by that of the interface between CFRP sheets and concrete. This study aims at applying a viscoelastic model to describe the creep behaviour of the adhesive layer bonding CFRP sheet to concrete, the CFRP-concrete interface. Reviews of available models on concrete creep behavior have been first carried out and then new FE analysis model is proposed. The proposed FE analysis model based on the maxwell model has been verified by previous experimental results. It is shown that the creep effect of interfacial adhesive layer is very important on the long-term behavior of concrete structures strengthened with CFRP.

The Effect of Nano Functionalized Block Copolymer Addition on the Joint Strength of Structural Epoxy Adhesive for Car Body Assembly (차체 구조용 에폭시 접착제의 접합강도에 미치는 나노 기능성 블록공중합체 첨가의 영향)

  • Lee, Hye-rim;Lee, So-jeong;Lim, Chang-young;Seo, Jong-dock;Kim, Mok-soon;Kim, Jun-ki
    • Journal of Welding and Joining
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    • v.33 no.4
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    • pp.44-49
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    • 2015
  • The structural epoxy adhesive used in car body assembly needs the highest level of joint mechanical strength under lap shear, T-peel and impact peel conditions. In this study, the effect of nano functionalized block copolymer addition on the impact peel strength of epoxy adhesive was investigated. DSC analysis showed that the addition of nano functionalized block copolymer did not affect the curing reaction of epoxy adhesive. From single lap shear test, it was found out that the addition of nano functionalized block copolymer slightly decreased the cohesive strength of cured adhesive layer. The addition of nano functionalized block copolymer showed beneficial effect on T-peel strength by changing the adhesive failure mode to the mixed mode. However, the addition of nano functionalized block copolymer just decreased the room temperature impact peel strength. It was considered that the addition of nano functionalized block copolymer could have effect on disturbing the crack propagation only for the case of slow strain rate.

Effect of Weldbond Process on the Weldability of 1.2GPa Grade Galvannealed TRIP Steel for Car Body Manufacturing (차체용 1.2GPa급 합금화아연도금 TRIP강의 용접성에 미치는 Weldbond 공정의 효과)

  • Lee, Jong-Dae;Lee, Hye-Rim;Kim, Mok-Soon;Seo, Jong-Deok;Kim, Jun-Ki
    • Journal of Welding and Joining
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    • v.34 no.6
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    • pp.28-34
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    • 2016
  • Galvannealed(GA) steels are now generally used in car body manufacturing for corrosion resistance. In this study, the weldability and joint mechanical behavior of a newly developed 1.2GPa grade GA ultra high strength TRIP(transformation induced plasticity) steel was investigated for three joining processes, such as adhesive bonding, resistance spot welding and weldbonding. Under both shear and peel stress conditions, the failure mode of the adhesive joints were the mixture of the adhesive cohesive failure, adhesive interface failure and coating layer failure. It means that the adhesion strength of GA coating onto the base metal was similar to that of adhesive bonding onto the GA coating. Under the shear stress condition, the weldbonding exerted to expand the optimal spot welding condition of 1.2GPa GA TRIP steel because the strength of adhesive bond overwhelmed that of the resistance spot weld. Under the peel stress condition, the weldbonding also exerted to expand the optimal spot welding condition of 1.2GPa GA TRIP steel by inducing the tear fracture mode rather than the partial plug fracture mode.

A Study on the Friction and Wear Characteristics of Nitrogen Ions Coated SCM415 Steel (질소이온 코팅 SCM415강의 마찰.마모특성에 관한 연구)

  • Lyu, Sung-Ki;He, Hei-bo;Son, Yu-Sun
    • Tribology and Lubricants
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    • v.23 no.1
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    • pp.14-18
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    • 2007
  • SCM415 alloy was implanted with nitrogen ions using plasma source ion implantation (PSII), at a dose range of $1{\times}10^{17}\;to\;6{\times}10^{17}N^{+}cm^{-2}$. Auger electron spectrometry (AES) was used to investigate the depth profile of the implanted layer. Friction and wear tests were carried out on a block-on-ring wear tester. Scanning electron microscopy (SEM) was used to observe the micro-morphology of the worn surface. The results revealed that after being implanted with nitrogen ions, the frictional coefficient of the surface layer decreased, and the wear resistance increased with the nitrogen dose. The tribological mechanism was mainly adhesive, and the adhesive wear tended to become weaker oxidative wear with the increase in the nitrogen dose. The effects were mainly attributed to the formation of a hard nitride precipitate and a supersaturated solid solution of nitrogen in the surface layer.

The EFFECT OF DENTAL ADHESIVE R~SIN CEMENT ON THE DOGS' DENTAL PULP (접착성(接着性) 레진 세멘트가 가견치수조직(家犬齒髓組織)에 미치는 영향(影響))

  • Yang, Jung-Ok;Cho, Kyew-Zeung
    • Restorative Dentistry and Endodontics
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    • v.12 no.2
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    • pp.101-108
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    • 1987
  • The purpose of this study was to investigate the pulpal responses of dental adhesive resins. A total of 40 cavities of the permanent healthy teeth from 4 dogs were prepared. In the experimental group, the cavities were etched for 1 minute with citric acid and filled with experimental resins (ie. Super-Bond C & B$^{(R)}$). In the control group, the cavities were filled with calcium hydroxide base materials (ie. Dycal$^{(R)}$) without etching. The dogs were sacrificed at one, two, three and four weeks after the time of filling and the specimens were routinely prepared and stained with Hematoxylin-Eosin. The microscopic findings were as follows: Infiltration of inflammatory cells was not observed in both experimental and control groups. Change in the odontoblastic layer was not observed in all control groups but severe swelling was observed in deep dental pulp tissue of the control two and three week cases. Pulp tissue was recovered with plenty of fibrous component in the control four week case and reparative dentin formation was not occurred in all cases. Slight changes of the odontoblastic layer beneath the cavity were observed in the experimental one week case. In experimental two and three week cases, swelling of deep pulp tissue was increased and localized reparative dentin formation was observed. In the experimental four week case, odontoblastic layer was recovered with regular appearance and fibrous component of the pulp was increased, but reparative dentin formation was not evident.

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Analysis of Ultrasonic Resonance Signal for Detecting the Defect of Adhesive Interface in Exit Cone (확대부 내열재의 접착계면 결함 검출을 위한 초음파 공진 신호 분석)

  • Kim, Dong-Ryun;Kim, Jae-Hoon;Lim, Soo-Yong;Park, Sung-Han;Yeh, Byung-Hahn
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2012.05a
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    • pp.230-237
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    • 2012
  • The ultrasonic resonance method was applied to detect the disbond interface and empty layer between steel and FRP of the exit cone. The ultrasonic resonance method can easily detect the disbond interface and empty layer by amplifying the ultrasonic signal, but pulse echo method is difficult to distinguish adhesive interface from disbond interface or empty layer. The resonance frequency was predicted using the pressure reflection coefficient of 3-layered medium, and measured from ultrasonic signal of the test block using Fast Fourier Transform. The ultrasonic resonance proved that the predicted resonance frequency was in good agreement with the measured resonance frequency.

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A Study on the Effect of Primer Processing Method on the Mechanical Properties of Impact Relief Air Cushion Materials Prepared through Thermal Film Laminating (프라이머 가공 방법이 열융착 필름 라미네이팅으로 제조한 고충격 대응 에어쿠션 소재의 물성에 미치는 영향 연구)

  • Kim, Ji Yeon;Kim, Hun Min;Min, Mun Hong
    • Textile Coloration and Finishing
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    • v.34 no.3
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    • pp.173-184
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    • 2022
  • In this study, the TPU film was laminated on an aramid fabric or circular knits in order to implement an air cushion material that can respond to high impact forces in case of a fall and is easy to expand. To increase the bonding strength between the fabric layer and the film layer, a primer layer was formed in two ways: one for thermally bonding and laminating PET film and two for coating and aging hot melt type PUR adhesive. The tensile strength of the aramid air cushion was 2.5 times higher than that of the circular knits, but the tensile elongation of the aramid air cushion was very low compared to that of the circular knits. The tear strength of the aramid air cushion was about twice or more superior to that of the circular knits, the primer treatment method was good at A, and the peel strength was excellent at method A. The aramid air cushion was the lightest in weight. Summarizing the above results, it was best to combine the air cushion material with aramid woven fabric and primer treatment method A to cope with the high impact force applied when falling.