• 한국항공우주학회지
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• 제34권10호
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• pp.40-47
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• 2006

반사경 지지부의 접착 특성은 인공위성카메라 반사경의 광학적 성능에 지대한 영향을 미치므로 이에 대한 연구가 필수적이다. 이를 위해 본 연구에서는 세 종류의 우주용 접착제의 접착 특성에 관한 연구를 수행하였다. 반사경의 재료인 제로더(Zerodur)와 금속이 접착된 시편을 사용하여 중첩 전단(lap shear) 시험을 수행하였고 금속과 금속이 접착된 시편에 대해서도 시험을 수행하였다. 또한 다양한 온도 환경을 겪더라도 안정적인 접착력이 보장되는지의 여부를 확인하였으며 세 접착제의 접착력을 비교하였다.

• 반도체디스플레이기술학회지
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• 제3권3호
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• pp.11-17
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• 2004

This research has been progressed for adhesive improvement of the Polyimide/Buffer layer/Cu at the COF(Chip On Film) which induced as the alternative plan about high concentration of a circuit or substrates according to demands of miniaturization and high efficiency of various electronic equipment. RF plasma equipment was applied to when plama pretreatment was performed for improvement of adhesive strength of PI and Cr as the buffer layer. Experimental fluents were a species of the buffer layer, depositied time and the ratio of $O_2$/Ar when performed to plasma pretreatment. The results are that Ni was superior to Cr at peel test according to a species of the buffer layer, peel strength and Cu THK were showed proportional relation to deposition structure of the same buffer layer and sample of the Cr depositied time(30 sec) and Cu depositied time(20 min) was showed good adhesion to peel test according to Cr's depositied time and Cu's depositied time. When perform PI's plasma pretreatment peel strength and $O_2$/Ar ratio were showed proportional relation. But $O_2$/Ar(2/5) was best condition since then decreased.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2005년도 춘계학술대회 논문집
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• pp.234-238
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• 2005

One approach to testing the suitability of a adhesive joint for a particular application is to build and test to destruction of a representative sample of the joint. The nondestructive test will not measure strength directly but will measure a parameter which can be correlated to the strength. It is therefore, essential that a suitable nondestructive test is chosen and its results are correctly interpreted. In this paper, typical ultrasonic signal analysis in adhesive joints are evaluated together with interface stress from the result of finite element analysis.

• Restorative Dentistry and Endodontics
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• 제44권4호
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• pp.45.1-45.10
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• 2019

Objectives: Self-adhesive resin cements contain functional monomers that enable them to adhere to the tooth structure without a separate adhesive or etchant. One of the most stable functional monomers used for chemical bonding to calcium in hydroxyapatite is 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP). The aim of this study was to evaluate the influence of the10-MDP concentration on the bond strength and physical properties of self-adhesive resin cements. Materials and Methods: We used experimental resin cements containing 3 different concentrations of 10-MDP: 3.3 wt% (RC1), 6.6 wt% (RC2), or 9.9 wt% (RC3). The micro-tensile bond strength of each resin cement to dentin and a hybrid resin block (Estenia C&B, Kuraray Noritake Dental) was measured, and the fractured surface morphology was analyzed. Further, the flexural strength of the resin cements was measured using the three-point bending test. The water sorption and solubility of the cements following 30 days of immersion in water were measured. Results: The bond strength of RC2 was significantly higher than that of RC1. There was no significant difference between the bond strength of RC2 and that of RC3. The water sorption of RC3 was higher than that of any other cement. There were no significant differences in the three-point bending strength or water solubility among all three types of cements. Conclusions: Within the limitations of this study, it is suggested that 6.6 wt% 10-MDP showed superior properties than 3.3 wt% or 9.9 wt% 10-MDP in self-adhesive resin cement.

• 한국건축시공학회지
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• 제18권4호
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• pp.329-335
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• 2018

본 연구의 목적은 기존 콘크리트 건물의 단면확대 내진보강 기술에서 필요한 고유동 고접착성의 보강 모르타르 배합의 개발이다. 보강 모르타르의 목표성능(플로우 220mm 이상, 압축강도 30MPa, 접착강도 1MPa 이상)을 위해 물-결합재비, 잔골재-결합재비, 폴리머-결합재비, 증점제 사용 및 초속경시멘트의 혼입 등을 변수로 단계적으로 배합실험을 수행하였다. 모르타르의 접착강도는 기존 콘크리트의 다양한 면 처리 상태에 따라 평가하였다. 실험결과로부터 단면증설용 보강 모르타르의 배합을 위해 폴리머-결합재비는 10%, 초속경시멘트의 치환율은 5%가 추천될 수 있었는데, 이 배합은 초기 플로우 220 mm, 높은 초기강도 발현, 압축강도 35 MPa 그리고 접착강도 1.2 MPa 이상의 성능을 보였다.

• 대한치과보철학회지
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• 제33권4호
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• pp.662-684
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• 1995

The purpose of this study was to evaluate the shear bond strength between various resin-bonded retainers and enamel according to the adhesive resins and retention types and observe the bond filure modes with scanning electron microscope(SEM). For this purpose, the followin eight sub-groups were tested in shear bond strength : 1) electrochemically etched group(Verabond) using Panavia EX and Superbond C&B 2) tin-plated group(PG-S) using Panavia EX and Superbond C&B 3) salt-treated group(Verabond) using Panavia EX and Superbond C&B 4) meshtreated group(Verabond) using Panavia EX and Superbond C&B. Thermocycling test was conducted on the condition of 15 second dwell time each in $5^{\circ}C$ and $55^{\circ}C$bath. Shear bond strength was measured by Instron Universal Testing Machine(medel 1125). The obtained results were as follows : 1. After thermocycling, the shear bond strengths of tin-plated group and electrochemically etched group were significantly greater than those of salt-treated group and mesh-treated group. And the shear bond strength of Panavia EX was greater than that of Superbond C&B with salt-treated group and tin-plated group(p<0.05). 2. Before thermocycling, electrochemically etched group using Superbond C&B produced the greatest shear bond strength(p<0.01). 3. The shear bond strength of electrochemically etched group using Superbond C&B was significantly decreased after thermocycling(p<0.01). 4. In observation of bond failure modes before thermocycling, Panavia EX highly exhibited enamel fracture. Tin-plated group using Superbond C&B adhesive failure between metal and resin and electrochemically etched group using Superbond C&B exhibited adhesive failure between enamel and rdsin. 5. In observation of failure modes after thermocycling, Panavia EX exhibited cohesive failure and Superbond C&B exhibited adhesive failure between resin and metal.

• 한국생산제조학회지
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• 제6권3호
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• pp.73-81
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• 1997

This study was to find the best adhesive condition comparing mechanical property in case of hot-melt adhesion using glue-gun, ultrasonic welding with adhesion and only ultrasonic welding in order to adhere thermoplastic resin of polyethylene (PE) in which reliable adhesion was resulted in case of ultrasonic welding with same materials of PE. The best welding condition were acquired at welding time 1 second, welding pressure 250kPa for PE-PE where welding time and welding pressure were increased in accordance with the increase of material strength. At the best ultrasonic welding conditions, bonding strength of PE-PE welding was about 21MPa of which material have tensile strength of 24MPa. Through the analysis of microscophic test for ultrasonic welding structure, it was distinguished between well welded structure with higher intermolecule flow and bad welded structure with lower flow, of which result is mostly correspond with the result of tensile strength test.

• The Journal of Advanced Prosthodontics
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• 제7권4호
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• pp.317-322
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• 2015

PURPOSE. The aim was to evaluate the effect of curing mode and different dentin surface pretreatment on microtensile bond strength (${\mu}TBS$) of self-adhesive resin cements. MATERIALS AND METHODS. Thirty-six extracted human permanent molars were sectioned horizontally exposing flat dentin surface. The teeth were divided into 12 groups (3 teeth/group) according to the dentin surface pretreatment methods (control, 18% EDTA, 10% Polyacrylic acid) and curing mode (self-curing vs. light-curing) of cement. After pretreatment, composite resin blocks were cemented with the following: (a) G-CEM LinkAce; (b) RelyX U200, followed by either self-curing or light-curing. After storage, the teeth were sectioned and ${\mu}TBS$ test was performed using a microtensile testing machine. The data was statistically analyzed using one-way ANOVA, Student T-test and Scheffe's post-hoc test at P<.05 level. RESULTS. For G-CEM LinkAce cement groups, polyacrylic acid pretreatment showed the highest ${\mu}TBS$ in the self-cured group. In the light-cured group, no significant improvements were observed according to the dentin surface pretreatment. There were no significant differences between curing modes. Both dentin surface pretreatment methods helped to increase the ${\mu}TBS$ of RelyX U200 resin cement significantly and degree of pretreatment effect was similar. No significant differences were found regarding curing modes except control groups. In the comparisons of two self-adhesive resin cements, all groups within the same pretreatment and curing mode were significantly different excluding self-cured control groups. CONCLUSION. Selecting RelyX U200 used in this study and application of dentin surface pretreatment with EDTA and polyacrylic acid might be recommended to enhance the bond strength of cement to dentin.

• Composites Research
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• 제26권2호
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• pp.129-134
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• 2013

극저온 환경에 노출되는 구조체의 접착조인트의 경우 피접착물과 접착물 사이에서 열팽창계수 차이로 인해 계면에서 잔류응력이 발생하게 되는데 이에 의해 접착조인트 내부에 미소균열, 층간분리 등의 형태로 파손이 발생할 우려가 있다. 본 연구에서는 높은 비강성, 낮은 열팽창계수의 특성을 지닌 메타 아라미드 섬유를 에폭시 기지재의 보강재로 사용하였다. 표면처리 공정을 간소화하기 위해 전기방사법의 고분자 혼합법(polymer blend method)으로 코어-쉘 구조의 메타 아라미드/에폭시 나노섬유를 제조하였다. 극저온 환경에서 계면특성이 향상된 코어-쉘 구조의 나노섬유를 보강한 에폭시 접착제의 전단물성을 확인하기 위해 환경챔버를 이용하여 $-150^{\circ}C$의 저온에서 단일 겹치기 실험(single lap joint test)을 진행하였다. 또한, DCB(double cantilever beam) 실험을 통해 파괴인성을 측정하였다. 그 결과, 극저온에서 일반 메타 아라미드 나노섬유에 비해 코어-쉘 구조의 메타 아라미드/에폭시 나노섬유를 보강한 접착제 시편이 우수한 계면특성으로 인해 물성이 크게 향상되었음을 확인하였다.

• Restorative Dentistry and Endodontics
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• 제48권2호
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• pp.14.1-14.11
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• 2023

Objectives: This study investigated the effect of an aluminum chloride hemostatic agent on the shear bond strength (SBS) of a universal adhesive to dentin. Materials and Methods: Eighty extracted human molars were trimmed at the occlusal dentin surfaces and divided mesiodistally. According to hemostatic agent application, specimens were randomly allocated into control (C) and hemostatic agent (Traxodent; H) groups. Each group was divided into 4 subgroups according to the adhesive system (n = 20): Scotchbond Multi-Purpose (SBER), Clearfil SE Bond (CLSE), All-Bond Universal etch-and-rinse mode (ALER), and All-Bond Universal self-etch mode (ALSE). SBS was measured for half of the specimens at 24 hours, and the other half were thermocycled in water baths (group T). Fracture surfaces were examined to determine the failure mode. The SBS was measured, and data were analyzed using 1-way analysis of variance, the Student's t-test, and the Tukey honestly significant difference test (p = 0.05). Results: No significant differences in SBS were found between groups C and H for any adhesive system at 24 hours. After thermocycling, a statistically significant difference was observed between CT+ALSE and HT+ALSE (p < 0.05). When All-Bond Universal was applied to hemostatic agent-contaminated dentin, the SBS of H+ALSE was significantly lower than that of H+ALER (p < 0.05). The SBER subgroups showed no significant differences in SBS regardless of treatment and thermocycling. Conclusions: When exposed dentin was contaminated by an aluminum chloride hemostatic agent before dentin adhesive treatment, application of All-Bond Universal in etch-and-rinse mode was superior to self-etch mode.