• Title/Summary/Keyword: Adhesive Strength Test

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Room-temperature Bonding and Mechanical Characterization of Polymer Substrates using Microwave Heating of Carbon Nanotubes (CNT 마이크로파 가열을 이용한 고분자 기판의 상온 접합 및 기계적 특성평가)

  • Sohn, Minjeong;Kim, Min-Su;Ju, Byeong-Kwon;Lee, Tae-Ik
    • Journal of the Microelectronics and Packaging Society
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    • v.28 no.2
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    • pp.89-94
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    • 2021
  • The mechanical reliability of flexible devices has become a major concern on their commercialization, where the importance of reliable bonding is highlighted. In terms of component materials' properties, it is important to consider thermal damage of polymer substrates that occupy large area of the flexible device. Therefore, room temperature bonding process is highly advantageous for implementing flexible device assemblies with mechanical reliability. Conventional epoxy resins for the bonding still require curing at high temperatures. Even after the curing procedure, the bonding joint loses flexibility and exhibits poor fatigue durability. To solve this problems, low-temperature and adhesive-free bonding are required. In this work, we develop a room temperature bonding process for polymer substrates using carbon nanotube heated by microwave irradiations. After depositing multiple-wall carbon nanotubes (MWNTs) on PET polymer substrates, they are heated locally with by microwave while the entire bonding specimen maintains room temperature and the heating induces mechanical entanglement of CNT-PET. The room temperature bonding was conducted for a PET/CNT/PET specimen at 600 watt of microwave power for 10 seconds. Thickness of the CNT bonding joint was very thin that it obtains flexibility as well. In order to evaluate the mechanical reliability of the joint specimen, we performed lap shear test, three-point bending test, and dynamic bending test, and confirmed excellent joint strength, flexibility, and bending durability from each test.

Study of Mechanical and Hygroscopic Characteristics of Nanoclay/Epoxy Nanocomposites (나노클레이/에폭시 나노-복합재료의 기계적 및 흡습 특성에 관한 연구)

  • Kim, Do Hyoung;Kim, Jung Kyu;Kim, Hak Sung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.2
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    • pp.139-145
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    • 2016
  • In this study, the moisture related hygroscopic characteristics and mechanical properties of epoxy-clay nanocomposites were investigated by experiments as a function of the weight fraction of nanoclay. The hygroscopic and mechanical properties including the moisture saturation amount, moisture diffusivity, adhesive strength, and tensile properties were obtained by moisture absorption test and various tensile tests, respectively. Also, the molecular dynamics (MD) simulation was devised to study of hygroscopic characteristics of nanocomposites and the results were compared to experimental results as a function of the nanoclay content. It was demonstrated that the proposed MD simulation technique can be successfully used for the prediction of the effects of the nanoclay on the moisture diffusion characteristics.

Monitoring Technology on the Surface Condition after Conservation Treatment of Stone Cultural Heritage (석조문화재의 보존처리 후 표면상태 모니터링 기술 연구)

  • Park, Sung Mi;Chun, Yu Gun;Lee, Myeong Seong
    • 보존과학연구
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    • s.34
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    • pp.32-48
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    • 2013
  • This study examined the applicability of deterioration monitoring techniques to establish efficient conservation and management system for stone cultural heritage which conservation treatment has been done. It was confirmed that deterioration mapping combined with photography and grid work, and adhesive tape test for the surface were very applicable to investigate the surface change due to deterioration, and assess the degree of granular disintegration quantitatively. The portable microscopic survey and ultrasonic measurement were efficient techniques to observe mineral looseness and microcrack, and to track the strength change of the stone before-and-after the conservation treatment. These techniques can be easily used by manage practitioners in the field through simple guidance and technical education. Also, it can contribute to build a long-term and methodical conservation and management system of the stone cultural heritage.

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Effect of Photoinitiators on Adhesion Properties of 2-EHA/AA PSA (광개시제의 종류에 따른 2-EHA/AA 점착제의 접착특성)

  • Yoon, Hong-Beom;Kim, Ho-Gyum;Min, Kyung-Eun
    • Polymer(Korea)
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    • v.38 no.4
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    • pp.491-495
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    • 2014
  • Pressure sensitive adhesive (PSA) based on 2-ethylhexyl acrylate (2-EHA)/acrylic acid (AA) copolymer was synthesized using different photoinitiators. Results showed that PSA with Irgacure$^{(R)}$651 (benzyldimethylketal) and Irgacure$^{(R)}$184(1-hydroxy-cyclohexylphenyl ketone) proved to be good for adhesion properties. This may be attributed to strong absorption near 350 nm wavelength and also high solubility in monomer mixtures. The addition of Irgacure$^{(R)}$819, bisacylphosphine oxides as a photoinitiator caused cohesive failure with high loading in a peel test owing to the additional radical formation. It is assumed that the insoluble photoinitiator reacts with oxygene, which may act as a hydrogen donor.

Properties of Particleboard Using Byproduct of Plywood Manufacture - Evaluation on the Elements of Surface Layer and Pre-treatment of Particles (합판 공장 부산물을 이용한 파티클보드의 물성에 관한 연구 - 표층 구성요소 및 파티클 전처리 여부에 따른 비교 -)

  • Hwang, Jung Taek;Pi, Duck Won;Kang, Seog Goo
    • Journal of the Korean Wood Science and Technology
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    • v.41 no.1
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    • pp.33-41
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    • 2013
  • This study was performed to analyse cause of quality deterioration using byproduct of plywood and to determine physical and mechanical properties of particleboard used new bonding condition we found. The result of bending strength of Com-Ply board using EMDI is 57.7 $N/mm^2$ on linear direction and 25.1 $N/mm^2$ on vertical direction. EMDI has better water-resisting qualities than Urea formaldehyde adhesive according to result of thickness swelling and water absorption test. Pre-treatment soaked particle 72 hours in water caused increase of HCHO emission.

Numerical Study on Failure Mechanism of Tunnel Shotcrete Lining (터널 숏크리트 라이닝 파괴 메커니즘에 대한 수치해석적 고찰)

  • Shin, Hyusoung;Shin, Dongin;Bae, Gyujin;Kim, Donggyu
    • Journal of the Korean GEO-environmental Society
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    • v.10 no.7
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    • pp.167-177
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    • 2009
  • This study investigates a failure mechanism of a tunnel shotcrete lining with respect to a concentrated load due to blocky rock mass. First of all, it is carried out to survey relevant researches to shotcrete failures by literature reviews and to numerically re-investigate the failure modes of shotcrete lining given by previous researches. Through this study, the failure modes are relocated with the conditions which induce each failure mode newly proposed by this study. In addition to this, the arching shape of tunnel lining, which has not been considered in the previous research despite of inherent geometrical characteristics in tunnels, is taken into consideration in numerical investigation on lining failure in this study. As a result, it is shown that more simplified failure modes can be found on the tunnel boundary condition and the corresponding failure condition to each mode can be different from ones of the previous study due to a tunnel arching effect.

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Repair of seismically damaged RC bridge bent with ductile steel bracing

  • Bazaez, Ramiro;Dusicka, Peter
    • Steel and Composite Structures
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    • v.26 no.6
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    • pp.745-757
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    • 2018
  • The inclusion of a ductile steel bracing as means of repairing an earthquake-damaged bridge bent is evaluated and experimentally assessed for the purposes of restoring the damaged bent's strength and stiffness and further improving the energy dissipation capacity. The study is focused on substandard reinforced concrete multi-column bridge bents constructed in the 1950 to mid-1970 in the United States. These types of bents have numerous deficiencies making them susceptible to seismic damage. Large-scale experiments were used on a two-column reinforced concrete bent to impose considerable damage of the bent through increasing amplitude cyclic deformations. The damaged bent was then repaired by installing a ductile fuse steel brace in the form of a buckling-restrained brace in a diagonal configuration between the columns and using post-tensioned rods to strengthen the cap beam. The brace was secured to the bent using steel gusset plate brackets and post-installed adhesive anchors. The repaired bent was then subjected to increasing amplitude cyclic deformations to reassess the bent performance. A subassemblage test of a nominally identical steel brace was also conducted in an effort to quantify and isolate the ductile fuse behavior. The experimental data from these large-scale experiments were analyzed in terms of the hysteretic response, observed damage, internal member loads, as well as the overall stiffness and energy dissipation characteristics. The results of this study demonstrated the effectiveness of utilizing ductile steel bracing for restoring the bent and preventing further damage to the columns and cap beams while also improving the stiffness and energy dissipation characteristics.

Studies on Manufacture of Thin Composite Panel for Substitute Use of Plywood (I) - On the Optimum Manufacturing Condition of Composites - (합판대용(合板代用) 박판상(薄板狀) 복합재(複合材) 제조(製造)에 관(關)한 연구(硏究) (I) - 복합재(複合材) 제조(製造)의 최적조건(最適條件)에 관(關)하여 -)

  • Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.23 no.2
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    • pp.55-69
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    • 1995
  • The primary objective of this research was to investigate optimum manufacturing condition of thin composite panels composed of sawdust, polyethylene film and polypropylene net. At the study the experiment was designed to make thin board in which sawdust offers effectiveness as core composing material, polyethylene as adhesive with added urea resin, and polypropylene as stiffness and flexibility in the composition panel. 100 types of thin composite panels were manufactured according to press-lam and mat-forming process of various hot pressing conditions(pressure, temperature and time). They were tested and compared with control boards on bending properties(MOR, MOE, SPL, WML), internal bond strength, thickness swelling, linear expansion and water absorption. At the same time the visual inspections of each types of panels were accomplished. The physical and mechanical properties of composite types passed by visual inspection were analyzed by Tukey's studentized range test. From the statistical analysis, the optimum manufacturing condition of thin composite panels were selected. Compared with two manufacturing processes, mat-forming process performed better than press-lam process in all tested properties. The optimum manufacturing conditions resulted from the experiment and statistical analysis were able to determine as following: the press temperature was shown the most good result at 130$^{\circ}C$ in mat forming process and 140$^{\circ}C$ press lam process, the press time 4 min in both processes, but the press pressure was 25-10kg/$cm^2$ in mat forming and 15k/$cm^2$ press lam process.

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A Study on the Cold Pad Batch Dyeing of a String Wallcovering with Reactive Dyestuff (반응성염료를 이용한 스트링벽지 패딩염색에 관한 연구)

  • Lee, Joonhan;Kang, Youngwoong;Kim, Sunmee
    • Journal of Fashion Business
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    • v.21 no.2
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    • pp.105-112
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    • 2017
  • A string wallcovering is a kind of textile wallcovering which is made of cellulose fiber yarn laminated on base paper. Compared with normal paper or PVC wallpaper, a string wallcovering is preferred continually in the interior design market, as it is not only environmentally friendly but it also has less cost on mass production without the weaving process and has a natural visual effect, excellent functionality such as thermo keeping, permeability, sound absorption. However, in the dyeing process, it is not appropriate to use plenty of energy such as water, electricity, steam or chemicals considering the environmental trend and the government policy plenty of energy such as water, electricity, steam or chemicals. Currently, a string wallcovering is made of raw white yarn and padding with direct dye or pigment which includes toxic elements, especially the use of direct dye is restricted in a part of the developed country due to inclusion of azo. In this study, we researched dyeing based on cold pad batch dyeing of a string wallcovering with reactive dyestuff. The peel strength and bending depth test confirmed that the optimum adhesive type and spread amount improved the water resistance of the string wallcovering. Also, pad batch dyeing with optimum reactive dyestuff enhanced the color fastness to light and rubbing in dry and wet conditions. Additionally, for improvement of color fastness to rubbing in a wet condition, the additional treatment finishing without soaping process which is used water. The results of this study can be used as basic data for environmentally friendly and energy saving of the textile wallcovering.

The effect of a desensitizer and $CO_2$ laser irradiation on bond performance between eroded dentin and resin composite

  • Ding, Meng;Shin, Sang-Wan;Kim, Min-Soo;Ryu, Jae-Jun;Lee, Jeong-Yol
    • The Journal of Advanced Prosthodontics
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    • v.6 no.3
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    • pp.165-170
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    • 2014
  • PURPOSE. This study was aimed to evaluate effect of the desensitizing pretreatments on the micro-tensile bond strengths (${\mu}TBS$) to eroded dentin and sound dentin. MATERIALS AND METHODS. Forty-two extracted molars were prepared to form a flat dentin surface, and then they were divided into two groups. Group I was stored in distilled water while group II was subjected to a pH cycling. Each group was then subdivided into three subgroups according to desensitizing pretreatment used: a) pretreatment with desensitizer (Gluma); b) pretreatment with $CO_2$ Laser (Ultra Dream Pluse); c) without any pretreatment. All prepared surfaces were bonded with Single Bond 2 and built up with resin composite (Filtek Z250). The micro-tensile bond test was performed. Fracture modes were evaluated by stereomicroscopy. Pretreated surfaces and bonded interfaces were characterized by scanning electron microscope (SEM). The data obtained was analyzed by two-way ANOVA (${\alpha}$=0.05). RESULTS. For both sound and eroded dentin, samples treated with desensitizer showed the greatest ${\mu}TBS$, followed by samples without any treatment. And samples treated with $CO_2$ laser showed the lowest ${\mu}TBS$. SEM study indicated that teeth with eroded dentin appeared prone to debonding, as demonstrated by existence of large gaps between adhesive layers and dentin. CONCLUSION. Pretreatment with Gluma increased the ${\mu}TBS$ of Single Bond 2 for eroded and sound teeth. $CO_2$ laser irradiation weakened bond performance for sound teeth but had no effect on eroded teeth.