• Title/Summary/Keyword: Adhesion performance

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Adhesive Strength in Tension of High Volume PAE-Modified Cement Mortar with High Flowability for Floor Finishing

  • Do, Jeong-Yun;Soh, Yang-Seob
    • Journal of the Korea Concrete Institute
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    • v.15 no.5
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    • pp.739-746
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    • 2003
  • Various researches on the application of polymer dispersions to the cement mortar and concrete have been carried out in many countries like America, Japan and Germany and so on due to their high performance and good modification effect. PAE of polymer dispersion widely used in situ was employed that the high flowability may be induced in the cement mortar. In order to investigate the modification of cement mortar with high flowability by PAE and fracture mode of adhesive strength properties in tension of that, experimental parameters were set as PAE solid-cement ratio(P/C) and cement: fine aggregate(C:F) and the experiments such as unit weight, flow, consistency change, crack resistance and segregation that inform on the general properties have been done. Adhesion in tension is measured with a view to comprehending the properties and fracture mode in tensile load. Consistency change of cement mortar modified by PAE did grow better as the ratio of PAE solid-cement increased and was much superior to that of resin based flooring such as polyurethane and epoxy which recorded the loss of consistency in 90 min. after mixing. Adhesive strength in tension increased with continuity during curing period and showed the maximum in case of C:F=1:1 and P/C=20%.

Effects of Water Absorption and Surface Treatment on Mechanical Properties of Sisal Textile Reinforced Composites (사이잘 섬유 강화 복합재료의 기계적 특성에 미치는 표면처리와 흡습의 영향)

  • Kim Hyo-Jin;Seo Do-Won;Pak Han-Ju;Jeon Yang-Bae;Lim Jae-Kyoo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.30 no.7 s.250
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    • pp.779-786
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    • 2006
  • Woven sisal textile reinforced composites were manufactured to evaluate fracture toughness, and tensile test. All specimens were immersed in water five times. All specimens are immersed in pure water during 9 days at room temperature, and dried in 1 day at $50^{\circ}C$. Two kinds of polymer matrices such as epoxy and vinyl-ester were used. Fractured surface were investigated to study the failure mechanism and fiber/matrix interfacial adhesion. It is shows that it can be enhanced to improve their mechanical performance to reveal the relationship between fracture toughness and water absorption fatigue according to different polymer matrices. Water uptake of the epoxy composites was found to increase with cycle times. Mechanical properties are dramatically affected by the water absorption cycles. Water-absorbed samples observed poor mechanical properties such as lower values of maximum strength and extreme elongation. The $K_{IC}$ values demonstrate a decrease in inclination with increasing cyclic times of wetting and drying fur the epoxy and vinyl-ester.

Improvement of electromigration characteristics in using Ai interlayer (Cu 배선에 Al층간 물질 첨가에 의한 EM특성 개선)

  • 이정환;박병남;최시영
    • Journal of the Korean Vacuum Society
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    • v.10 no.4
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    • pp.403-410
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    • 2001
  • Acceleration in integration density and speed performance of ULSI circuits require miniaturization of CMOS and interconnections as well as higher current density capabilities for transistors. A leading candidate to substitute Al-alloy is Cu, which has lower resistivity and higher melting point. So we can expect much higher electromigration resistance. In this paper, we are going to explain the major features of EM for MOCVD Cu according to variant conditions. We compared the life time and activation energy of MOCVD Cu with those of I-beam Cu and AA in the same conditions. The electromigration experiments were performed with Cu/Al/TiN multilayer. Experimental results shows that the deposition rate and electromigration characteristics of Cu thin film were improved by the Al interlayer.

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A Study on the Economic Evaluation of Thermal Spray Methods for the Corrosion Protection of Steel (금속용사 방식공법의 경제성 평가에 관한 연구)

  • Jung Sung-Ho
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2005.05a
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    • pp.13-16
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    • 2005
  • Generally, as corrosive protection processing of a steel structure, zinc galvanizing and heavy duty coating paint are applied. However, zinc galvanizing has the difficulty of restriction of a size, or on-site construction. Moreover, heavy duty coating paint has a problem with many administrative and maintenance expenses with short problem of adhesion, corrosion generating of a damage portion, and maintenance management cycle. In this study, a salt water spray test, CASS test, and the electrochemistry examination were carried out for the thermal metal spray method of construction for corrosive protection performance evaluation. Moreover, the corrosive protection life of a thermal metal spray method of construction was quantitatively calculated on the basis of this experiment. in consideration of LCC, the economical efficiency of a general corrosive protection method of construction and a thermal metal corrosive protection method of construction was compared. Consequently, although initial construction expense was estimated 16 to $30\%$ high, as for a thermal metal spray method of construction, it turns out that the administrative and maintenance expenses for 100 years became cheap 9.3 to 13 or more times.

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Development of Membrane Filters with Nanostructured Porous Layer by Coating of Metal Nanoparticles Sintered onto a Micro-Filter (마이크로-필터 상에 소결 처리된 금속 나노입자 코팅에 의한 나노구조 기공층 멤브레인 필터 개발)

  • Lee, Dong-Geun;Park, Seok-Joo;Park, Young-Ok;Ryu, Jeong-In
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.8
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    • pp.617-623
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    • 2008
  • The membrane filter adhered with nanostructured porous layer was made by heat treatment after deposition of nanoparticle-agglomerates sintered in aerosol phase onto a conventional micron-fibrous metal filter as a substrate filter. The Sintered-Nanoparticle-Agglomerates-coated NanoStructured porous layer Membrane Filter (SNA-NSMF), whose the filtration performance was improved compared with the conventional metal membrane filters, was developed by adhesion of nanoparticle-agglomerates of dendrite structure sintered onto the micron-fibrous metal filter. The size of nanoparticle-agglomerates of dendrite structure decreased with increasing the sintering temperature because nanoparticle-agglomerates shrank. When shrinking nanoparticle-agglomerates were deposited and treated with heat onto the conventional micron-fibrous metal filter, pore size of nanostructured porous layer decreased. Therefore, pressure drops of SNA-NSMFs increased from 0.3 to 0.516 kPa and filtration efficiencies remarkably increased from 95.612 to 99.9993%.

Study of Corrosion-Induced Failure Mechanisms of Epoxy Coated Reinforcing Steel (Parts I and II)

  • Lee, Seung-kyoung
    • Proceedings of the Korea Concrete Institute Conference
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    • 1995.04a
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    • pp.396-401
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    • 1995
  • Epoxy coated reinforcing steels (ECRs) were acquired from ten sources and coatings from each source were initially characterized in terms of defects, thickness, solvent extraction weight loss and hardness. Testing involved exposure in three aqueous solutions at elevated temperature (8$0^{\circ}C$) and in chloride-contaminated concrete slabs under outdoor exposure, It was found that the density and size of coating defects was the promary factor affecting ECR performance. The equivalent circuit analysis using electrochemical impedance spectroscopy (EIS) data indicated that the impedance response for well-performing ECR specimens showed no signs of active degradation at the interface although diffusional processes similar to those noted for poorly performing bars occurred here. Experimental results also indicated a relationship between corrosion behavior and bar source. Weight loss upon solvent extraction correlated with impedance reduction from hot water exposure. Coating defects during most of the tests, especially in high pH solutions containing chloride ions. ECRs with excessive coating defects, either initially present or ones which developed in service, performed poorly in every test category regardless of source. Forms of coating failure were extensive rusting at defects, blistering, wet adhesion loss, cathodic delamination, underfilm corrosion and coating cracks. These occurred sequentially or concurrently, depending on the condition of the ECR and nature of the environment

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Characteristics of Organic Thin Film Transistors with Organic and Organic-inorganic Hybrid Polymer Gate Dielectric (유기물과 유무기 혼합 폴리머 게이트 절연체를 사용한 유기 박막 트랜지스터의 특성)

  • Bae, In-Seob;Lim, Ha-Young;Cho, Su-Heon;Moon, Song-Hee;Choi, Won-Seok
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.12
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    • pp.1009-1013
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    • 2009
  • In this study, we have been synthesized the dielectric layer using pure organic and organic-inorganic hybrid precursor on flexible substrate for improving of the organic thin film transistors (OTFTs) and, design and fabrication of organic thin-film transistors (OTFTs) using small-molecule organic semiconductors with pentacene as the active layer with record device performance. In this work OTFT test structures fabricated on polymerized substrates were utilized to provide a convenient substrate, gate contact, and gate insulator for the processing and characterization of organic materials and their transistors. By an adhesion development between gate metal and PI substrate, a PI film was treated using $O_2$ and $N_2$ gas. The best peel strength of PI film is 109.07 gf/mm. Also, we have studied the electric characteristics of pentacene field-effect transistors with the polymer gate-dielectrics such as cyclohexane and hybrid (cyclohexane+TEOS). The transistors with cyclohexane gate-dielectric has higher field-effect mobility, $\mu_{FET}=0.84\;cm^2/v_s$, and smaller threshold voltage, $V_T=-6.8\;V$, compared with the transistor with hybrid gate-dielectric.

A Study of the Fabrication and Enhancement of Film Bulk Acoustic Wave Resonator using Two-Step Deposition Method of Piezoelectric Layer (압전층의 2단 증착법을 이용한 체적 음향파 박막형 공진기의 제작과 성능향상에 관한 연구)

  • Park Sung-Hyun;Chu Soon-Nam;Lee Neung-Heon
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.54 no.7
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    • pp.308-314
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    • 2005
  • The 2 GHz film bulk acoustic wave resonator(FBAR), one of the most necessary device of the next generation mobile communication system, consisted of solidly mounted resonator(SMR) structure using Brags reflector, was researched in this paper The FBAR applied SiO$_{2}$ and W had large difference of the acoustic impedance to reflector Al to electrode and ZnO to piezoelectric layer. Specially, the FBAR applied the two-step deposition method to improve the c-axis orientation and increase reproducibility of the fabrication device had good performance. The electrical properties of plasma such as impedance, resistance, reactance, $V_{pp},\;I{pp}$, VSWR and phase difference of voltage and current, was analyzed and measured by RF sensor with the variable experiment process factors such as gas ratio, RF power and base vacuum level about concerning the thickness, c-axis orientation, adhesion and roughness. The FBAR device about the optimum condition resulted reflection loss(S$_{11}$) of -17 dB, resonance frequency of 1.93 GHz, electric-mechanical coefficient(k$_{eff}$) of 2.38 $\%$ and Qualify factor of 580. It was seen better qualify than the common dielectric filter at present and expected on business to the filter device of 2 GHz bandwidth with the MMIC technology.

Thermally Curable Organic-inorganic Hybrid Coatings on Ophthalmic Lenses by the Sol-Gel Method (졸-겔법에 의한 안경렌즈의 열경화형 유-무기 하이브리드 코팅)

  • Yu Dong-Sik;Lee Ji-Ho;Ha Jin-Wook
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.7 no.3
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    • pp.465-470
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    • 2006
  • Coating are needed on ophthalmic lenses to enhance both the mechanical durability of the relatively soft plastic surface and the optical performance of lenses. Organic-inorganic hybrid materials as molar ratio of 3-glycidoxypropyltrimethoxysilane(GPTS), methyltrimethoxysilane(MTMS) and tetraethyl orthosilicate(TEOS) were used to improve the surface characteristics and the optical properties on allyl diglycol carbonate lenses. Coating for these plastics were at $140^{\circ}C$ for 4hrs, applied using the sol-grl process flow-coating technique. The coated lens properties of transmittance, adhesion, pencil hardness, abrasion resistance, hot water resistance and chemical resistance were investigated. The optimum properties was obtained when the ratio of GPTS : MTMS : TEOS was 1:1:2, respectively.

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Experimental Investigation of Friction and Wear Characteristics of O-Ring (O-ring의 마찰, 마모 특성에 관한 실험적 고찰)

  • Oh, Jun-Chul;Kim, Dae-Eun;Kim, Hyun-Jun;Kim, Mun-Hwan;Kim, Chun-Il
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.10
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    • pp.1125-1131
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    • 2009
  • O-rings are commonly used in machines as a seal. Due to prolonged use the surface of an O-ring can degrade which can lead to leakage as well as contamination. Damage of O-rings used in vacuum applications such as sputter is caused by various mechanisms. Particles detached from the O-ring may cause significant problems on the performance of the system in the vacuum chamber. Therefore, understanding the tribological behavior of O-rings is important to tackle the damage caused by repeated contact. In this work, FKM rubber was used for friction and wear tests conducted to investigate the tribological behavior of O-rings. A reciprocating type of a tribo-tester was used for the tests. The friction coefficient between the steel ball and the FKM specimen was quite high. Also, in order to identify the wear behavior, the surface of the FKM specimen was characterized using both optical and scanning electron microscopes. Evidence of wear due to adhesion and extrusion could be found. The results of this work will aid in improving the durability of O-rings.