• 접착 및 계면
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• 제6권2호
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• pp.13-20
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• 2005

환경 친화적인 자연섬유 강화 고분자 복합재료의 계면 전단강도는 총체적인 기계적 물성을 조절하는데 매우 중요한 역할을 수행한다. Ramie와 Kenaf 섬유 강화 에폭시 복합재료의 계면 전단강도는 최종 물성을 위한 최적 조건을 찾아내기 위해 미세역학시험법과 비파괴 음향방출시험을 이용하여 평가했다. Ramie와 Kenaf 섬유의 동적 접촉각을 측정했고, 계면 접착에서 젖음성과 상호 관련시켜서 해석하였다. Ramie와 Kenaf 섬유의 기계적 물성은 단섬유 인장시험을 통해 조사했고, 통계학적으로 uni-와 bimodal Weibull 분포를 통해서 분석하였다. Ramie와 Kenaf 섬유에 대한 실제 신장율의 clamping 효과의 영향도 평가할 수 있었다. 두 가지의 다른 미세파괴 형상은 섬유다발과 단섬유 복합재료로부터 오는 축방향의 debonding과 섬유상의 fracture는 인장과 압축하중하에서 관찰할 수 있었다.

• 콘크리트학회지
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• 제6권3호
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• pp.173-179
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• 1994

국내 사용을 위하여 시험 생산된 에폭시 도막 철근에 대하여 운반, 가공시에 요구되는 기계적인 성능을 중심으로 품질을 시험 평가하고 시공 지침을 제안하기 위하여 기초적 자료를 축적하고자 하였다. 시험결과 에폭시 도막의 부착성능과 내마모성은 규격의 요구조건을 만족시키는 결과를 보이고 있다. 내굴곡성능도 규격의 기준은 만족시키고 있으나 도막이 두꺼울수록 내굴곡성이 약해지며 특히, 가공시 굽힙 각도는 $120^{\circ}$를 초과하지 않아야 할 것으로 판단되었다. 또한 저온에서 굴곡시 상당수의 도막 균열을 나타내어 저온에서의 가공에 대하여 제한이 확인되었다. 충격에 대한 저항성능은 규격은 만족되고 있으나 다소 약함을 보이고 있어 가공 운반시 주의가 요구될 것으로 판단된다. 국내에서 시험 생산된 에폭시 도막의 성능 시험 결과, 규격에서 요구되는 기계적인 성능을 대체로 만족하였다.

• The Journal of Advanced Prosthodontics
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• 제8권4호
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• pp.290-295
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• 2016

PURPOSE. The aim of this study was to evaluate the effect of paracetic acid (PAA) and ozone disinfection on the tensile bond strength (TBS) of silicone-based resilient liners to acrylic resins. MATERIALS AND METHODS. One hundred and twenty dumbbell shaped heat-polymerized acrylic resins were prepared. From the mid segment of the specimens, 3 mm of acrylic were grinded off and separated parts were reattached by resilient liners. The specimens were divided into 2 control (control1, control7) and 4 test groups of PAA and ozone disinfection (PAA1, PAA7, ozone1 and ozone7; n=10). While control groups were immersed in distilled water for 10 min (control1) and 7 days (control7), test groups were subjected to PAA (16 g/L) or ozone rich water (4 mg/L) for 1 cycle (10 min for PAA and 60 min for ozone) per day for 7 days prior to tensile tests. Measurements of the TBS were analyzed using 3-way ANOVA and Tukey's HSD test. RESULTS. Adhesive strength of Mollosil decreased significantly by application of ozone disinfection. PAA disinfection had no negative effect on the TBS values of Mollosil and Molloplast B to acrylic resin. Single application of ozone disinfection did not have any negative effect on TBS values of Molloplast B, but prolonged exposure to ozone decreased its adhesive strength. CONCLUSION. The adhesion of resilient liners to acrylic was not adversely affected by PAA disinfection. Immersion in ozonated water significantly decreased TBS of Mollosil. Prolonged exposure to ozone negatively affects adhesion of Molloplast B to denture base materials.

• The Journal of Advanced Prosthodontics
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• 제12권6호
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• pp.369-375
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• 2020

PURPOSE. This study evaluated the availability of multi-directionally forged (MDF) titanium (Ti) as a component of removable partial dentures (RPDs). MDF-Ti remarkably improved the mechanical properties of RPDs due to its ultrafine-grained structure. MATERIALS AND METHODS. The wear resistance, plaque adhesion, and machinability of MDF-Ti were tested. As controls, commercially pure (CP) titanium was used for wear, plaque adhesion, and machinability tests. For wear resistance, the volume losses of the titanium teeth before and after wear tests were evaluated. Plaque adhesion was evaluated by the assay of Streptococcus mutans. In the machinability test, samples were cut and ground by a steel fissure bur and carborundum (SiC) point. An unpaired t-test was employed for the analysis of the significant differences between MDF-Ti and the control in the results for each test. RESULTS. Wear resistance and plaque adherence of MDF-Ti similar to those of CP-Ti (P>.05) were indicated. MDF-Ti exhibited significantly larger volume loss than CP-Ti in all conditions except 100/30,000 g/rpm in machinability tests (P<.05). CONCLUSION. Although the wear resistance and plaque adherence of MDF-Ti were comparable to those of controls, MDF-Ti showed better machinability than did CP-Ti. MDF-Ti could be used as a framework material for RPDs.

• Journal of Periodontal and Implant Science
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• 제28권2호
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• pp.249-264
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• 1998

The present study evaluates the effects of calcium sulfate and DFDB on alveolar bone regeneration and cementum formation and connective tissue adhesion in intrabony angulated 1 wall defects of dogs. Four millimeter-deep angulated one-wall intrabony defects were surgically created in the mesial & distal aspects of premolars and with flap operaion alone(control group), with calcium sulfate(experimental group 1), with composit graft of 50% calcium sulfate and 50% DFDB(experimental group 2), with DFDB alone(experimental group 3). Histologic analysis following 8 weeks of healing revealed the following results: 1. The lengths of connective tissue adhesion was $1.05{\pm}0.48mm$ in the control, $1.30{\pm}0.67mm$ in the test group I, $0.97{\pm}0.22mm$ in the test group II and $0.93{\pm}0.15mm$ in the test group III. There was no statistical significance between control and all experimental groups. 2. Changes in alveolar bone level was $0.97{\pm}0.27mm$ in the control group, $1.45{\pm}0.42mm$ in the test group I, $2.00{\pm}0.33mm$ in the test group II, $1.88{\pm}0.34mm$ in the test group III. There was no statistically significant difference between control and experimental group I. There was a statistically significant difference between the control and experimental group II,III.(p<0.05). There was no statistically significant difference between all experimental group. 3. Cementum formation was $1.13{\pm}0.17mm$ in the control, $1.78{\pm}0.31mm$ in the test group I, $2.17{\pm}0.38mm$ in the test group II, $2.15{\pm}0.47mm$ in the test group III with statistically significant differences between control group and all experimental group(P<0.05). There was no statistically significant differences between all experimental group. These results suggest that the use of composit graft of 50% calcium sulfate and 50% DFDB and DFDB alone in angulated 1 wall intrabony defects has little effects on connective tissue adhesion, but has significant effects on new bone and new cementum formations.

• 접착 및 계면
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• 제5권2호
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• pp.22-36
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• 2004

Several in-situ testing methods of adhesively bonded joints under static short-time tensile loading are critically analyzed in terms of experimental procedure and data evaluation. Due to its rather homogeneous stress state across the glue line, the tensile-shear test with thick single-lap specimens, according to ISO 11003-2, has become the most important test process for the determination of realistic materials parameters. This basic method, which was improved in both, the experimental part by stepped adherends and easily attachable extensometers and the evaluation procedure by numeric substrate deformation correction and test simulation based on the finite element method (FEM), is therefore demonstrated by application to several kinds of adhesives and metallic adherends. Multi-axial load decreases the strength of a joint. This effect, which is illustrated by an experimental comparison, impedes the derivation of realistic mechanical characteristics from measured force-displacement curves. It is shown by numeric modeling that tensile-shear tests with thin plate substrates according to ISO 4587, which are widely used for quick industrial quality assurance, reveal an inhomogeneous stress state, especially because of relatively large adherend deformation. Complete experimental determination of the elastic properties of bonded joints requires independent measurement of at least two characteristics. As the thick-adherend tensile-shear test directly yields the shear modulus, the tensile butt-joint test according to ISO 6922 represents the most obvious complement of the test programme. Thus, validity of analytical correction formulae proposed in literature for the derivation of realistic materials characteristics is verified by numeric simulation. Moreover, the influence of the substrate deformation is examined and a FEM correction method introduced.

• Journal of the Korean Wood Science and Technology
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• 제35권6호
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• pp.100-107
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• 2007

현대인들은 실내에서 보내는 시간이 하루 중 90% 달하는 것을 간주할 때 실내의 공기는 현대에게 중요한 요소임을 알 수 있다. 1960년대 이후로 산업이 급격히 발전하면서 건축 재료는 천연재료에서 화학물질을 기본으로 하는 재료로 변하게 되고 에너지 절약의 대책으로 건물의 기밀도를 높임으로써 건축자재에서 발생하는 유해물질이 현대인에게 악영향을 미치기 시작했고 이런 요소들이 근원이 되어 새집증후군을 유발하게 되었다. 생활수준이 높아지면서 사람들은 건강에 대한 관심도 높아지게 되고 보다 유익한 친환경 건축자재를 요구하게 되었다. 본 연구에서는 황토, 물, 수지, 경화제, 무기물 충전제를 이용한 친환경 황토 마감재를 개발하였고 한국형 목조 주택 내장벽에 사용할 수 있는 최적의 비율을 연구하였다. 그리고 이런 황토 마감재가 실내벽에 사용 시 요구물성인 내잔갈림성, 내세척성, 내충격성, 부착강도를 측정하였고 황토마감재의 특성인 원적외선 실험과 포름알데히드, TVOC 방산 농도를 통하여 친환경성에 대한 평가를 하였다.

• Restorative Dentistry and Endodontics
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• 제28권1호
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• pp.11-22
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• 2003

This study compared the dentin adhesion to composite resin according to air-dry, blot dry, application of rewetting agent on air-dry or blot dry dentin surface by microleakag test and SEM observation. For microleakage test, class V cavity preparations with dentinal margins were prepared on both buccal and lingual surfaces of 40 extracted human molars. For SEM observation, occlusal dentin of 20 extracted human molars were exposed. After etched the dentin, prepared teeth were randomly divided into four groups; D group: air dry for 10-15 sec., B group: blot dry with moist cotton pellet, D-R group: air dry and rewet with Aqua-Prep F for 20 sec., B-R group: blot dry and rewet with Aqua-Prep F for 20 sec. Treated cavities and surfaces were filled or constructed using One-Step adhesives and Aelitefil composite resins. Specimens were stored in distilled water for 24 hours. For microleakage test, the specimens were thermocycled and soaked into 2% methylene blue. The specimens were sectioned longitudinally and evaluated for microleakage under steromicroscope. The data were statistically analysed by Kuskal-Wallis Test, Mann-Whitney and Wilcoxon signed ranked tests. For SEM observation, the specimens were bisectioned mesiodiatally. After decalcified and deproteinized, specimens were observed under SEM. The results of this study were as follows; 1. The microleakges on dentinal margin were the highest in D group compared with B group, D-R group, and B-R group(p<0.05). But there was no significant difference between B group, D-R group and B-R group. 2. D group showed gap and a few resin tags between dentin and composite resin. 3 B group, D-R group, and B-R groups showed close adaptation between dentin and composite resin. It showed that resin rags in B group were numerous and long, in D-R group were few and short, in B-R group were numerous and short or long. 4. Adhesive layer showed in D-R group ($10{\;}\mu\textrm{m}$) and B-R group ($3{\;}\mu\textrm{m}$) In conclusion, use of rewetting agent to dry dentin was efficient to dentin adhesion, also it did not provide reverse effect on blot dry dentin.

• 접착 및 계면
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• 제22권3호
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• pp.85-90
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• 2021

섬유강화 복합재료를 이용하여 다양한 제품을 개발하고 있다. 제품화를 위해서는 기본적으로 복합재료의 인장강도 평가를 진행해야 한다. ASTM D3039 규격을 기반으로 섬유강화 복합재료가 평가되는데, 인장시편에 대한 변수 및 평가 조건에 따른 변수가 섬유강화 복합재료의 인장강도에 변화를 유발시킨다. 본 연구에서는 섬유강화 복합재료의 인장강도를 평가하는 ASTM D3039 기준을 따라 실험을 하되 탭, 시편의 두께, 탭을 붙이기 위한 접착제의 종류, 지그의 압력에 따른 섬유강화 복합재료의 인장강도 결과의 변화를 확인하였다. 시편의 두께에 따라 인장강도 및 인장탄성률의 변화가 있었다. 시편의 두께는 1-1.5 mm이 최적이며, 지그의 압력은 0.28 MPa, 탭을 붙이는 접착제는 접착력이 가장 우수한 구조용 접착제를 사용하는 것이 효과적이었다. 다양한 실험적 변수로 인해 오류를 일으킬 수 있었다. 접착제 및 탭, 지그 등에 대한 정확한 설정을 통해 효과적인 복합재료 평가가 이루어지길 희망한다.

• 열처리공학회지
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• 제15권3호
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• pp.118-126
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• 2002

TiCN thin films were deposited on tool steels at $510^{\circ}C$ by PECVD from a $TiCl_4+N_2+CH_4+H_2+Ar$ gaseous mixture. The microstructures and preferred orientation were investigated. The micro-scratch tests were performed using a system equipped with an acoustic emission sensor. Critical loads were determined to evaluate the adhesion of TiCN to substrate. The influences of the microstructures of substrates, double layered coatings, and coatings after nitriding(duplex coating) were investigated. The experimental results showed that the microstructures of substrates and double layered coating did not affect the critical loads considerably. By the duplex coating, critical loads were not always increased. In some cases, duplex coatings decreased critical loads significantly despite of absence of black layer. In this study, we tried to relate the results of scratch test to the residual stress analysis. Nitriding before the coating reduces the tensile residual stress in the film, which gives rise to low critical load in scratch test.