• 제목/요약/키워드: Activated powder

검색결과 260건 처리시간 0.029초

Synthesis of Intermetallics and Nanocomposites by High-Energy Milling

  • Bernd F. Kieback;H. Kubsch;Alexander Bohm;M. Zumdick;Thomas Weissgaerber
    • 한국분말재료학회지
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    • 제9권6호
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    • pp.416-421
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    • 2002
  • Elemental powders are used in high energy milling processes for the synthesis of new compounds. The low temperature solid state reactions during milling in inert gas atmosphere may result in intermetallic phases, carbides, nitrides or silicides with a nanocrystalline structure. To obtain dense materials from the powders a pressure assisted densification is necessary. On the other side the defect-rich microstructure can be used for activated sintering of elemental powder mixtures to obtain dense bodies by pressureless sintering. Results are discussed for nanocrystalline cermet systems and for the sintering of aluminides and silicides.

입상형 활성백토의 입자크기에 따른 수성도료의 특성 (Properties of Water-Based According to Particle Size of Granular Activated Clay)

  • 최병철;이상수
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2021년도 가을 학술논문 발표대회
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    • pp.19-20
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    • 2021
  • In order to reduce the emission of harmful substances that degrade indoor air quality, the Ministry of Environment strengthened the standards for the content of VOCs in paints to supply and sell eco-friendly paints. In this related study, an eco-friendly paint mixed with a powder-type absorbent material was prepared and its characteristics were reviewed. As the amount of powder-type absorbent material increased, the workability (viscosity, peeling, etc) decreased. Accordingly, this study aims to examine which particle size is suitable according to the particle size of the granular adsorbent while improving the problem of the powdery adsorbent by using the granular adsorbent. As an experimental plan, the particle size of granular activated clay is selected to be 0.250, 0.425, 0.710(mm), and the decrease rate of VOCs concentration and impact resistance are reviewed. As a result of the experiment, as the particle size of the granular activated clay increased, the decrease rate of the VOCs concentration increased and the impact resistance improved. Therefore, considering the problems that occur after actual painting, the particle size of granular activated clay of 0.425mm is suitable.

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Experimental study on chemical activation of recycled powder as a cementitious material in mine paste backfilling

  • Liu, Yin;Lu, Chang;Zhang, Haoqiang;Li, Jinping
    • Environmental Engineering Research
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    • 제21권4호
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    • pp.341-349
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    • 2016
  • To improve the utilization rate of construction waste as mine backfilling materials, this paper investigated the feasibility of using recycled powder as mine paste backfilling cementitious material, and studied the pozzolanic activity of recycled construction waste powder. In this study, alkali-calcium-sulfur served as the activation principle and an orthogonal test plan was performed to analyze the impact of the early strength agent, quick lime, and gypsum on the pozzolanic activity of the recycled powder. Our results indicated that in descending order, early strength agent > quick lime > gypsum affected the strength of the backfilling paste with recycled powder as a cementitious material during early phases. The strength during late phases was affected by, in descending order, quick lime > gypsum > early strength agent. Using setting time and early compressive strength as an analysis index as well as an extreme difference analysis, it was found that the optimal ratio of recycled powder cementitious material for mine paste backfilling was recycled powder:quick lime:gypsum:early strength agent at 78%:10%:8%:4%. X-ray diffraction analysis and scanning electron microscope were used to show that the hydration products of recycled powder cementitious material at the initial stages were mainly CH and ettringite. As hydration time increased, more and more recycled powder was activated. It mainly became calcium silicate hydrate, calcium aluminate hydrate, etc. In summary, recycled powder exhibited potential pozzolanic activities. When activated, it could replace cementitious materials to be used in mine backfill.

Development of microporous activated carbon using a polymer blend technique and its behavior towards methylene blue adsorption

  • Manocha, S.;Brahmbhatt, Amit
    • Carbon letters
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    • 제12권2호
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    • pp.85-89
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    • 2011
  • Coloured wastewater is released as a direct result of the production of dyes as well as from various other chemical industries. Many dyes and their breakdown products may be toxic for living organisms. Activated carbon is one of the best materials for removal of dyes from aqueous solutions. The present study describes the adsorption behaviour of methylene blue dye on three microporous activated carbons, where two samples (AC-1 and AC-2) were prepared by a polymer blend technique and the other is a microporous activated carbon (ARY-3) sample from viscose rayon yarn prepared by chemical-physical activation. The effects of contact time and activated carbon dosage on decolourisation capacity have been studied. The results show that activated carbon having mixed microporosity and mesoporosity show tremendous decolourisation capacity for methylene blue. In addition, the activated carbon in the powder form prepared by the polymer blend technique shows better decolourisation capacity for methylene blue than the activated rayon yarn sample.

Ni을 첨가한 $MoSi_2$분말성형체의 소결시 치밀화거동의 관찰 (Observation of Densification Behavior during the Sintering of Ni-added $MoSi_2$ Powder Compacts)

  • 이승익
    • 한국분말재료학회지
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    • 제4권4호
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    • pp.298-303
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    • 1997
  • The activated sintering behavior of $MoSi_2$ powder compacts with addition of 0.5 and 1.0 wt.%Ni during the sintering under As atmosphere was studied. The shrinkage was measured and the microstructures were observed by SEM (scanning electron microscopy) and BEI (backscattered electron image) along with the phase analysis by EDS during heating up to 155$0^{\circ}C$ and holding for various time at 155$0^{\circ}C$. The most of shrinkage occurred upon heating and 92% of theoretical density was attained after sintering for 1 hr at 155$0^{\circ}C$. However, little shrinkage ensued even for prolonged sintering over 1 hr at 155$0^{\circ}C$. A liquid film formed at about 135$0^{\circ}C$ along necks and grain boundaries. The polyhedral grain structure composed of $(Mo,Ni)_5Si_3$and $Ni_2Si$ across the $MoSi_2$ grain boundary developed at 155$0^{\circ}C$. It was concluded that the activated sintering of $MoSi_2$ powder by Ni led to the diffusion of Si into Ni decreasing the liquidus temperature and the enhanced diffusion of Mo and Si through such a liquid phase and/or interboundary of $(Mo,Ni)_5Si_3$.

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표면 활성화된 폐 EPDM 분말의 물성과 냄새 성분 분석 연구 (A Study on the Mechanical Properties of Surface Activated Waste EPDM and The Analysis of Odor Materials)

  • 최종만;김섭;정경호;정진수;유태욱;양준호
    • Elastomers and Composites
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    • 제42권4호
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    • pp.249-258
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    • 2007
  • 본 연구에서는 웨더스트립 공정스크랩인 폐 EPDM을 재활용하기 위해 고온전단분쇄기를 이용하여 표면활성화 된 EPDM 분말을 제조하여 이의 물성과 냄새성분분석에 관한 연구를 수행하였다. 본 연구에서 사용되어진 폐 EPDM은 solid, sponge, solid+sponge, solid+metal형으로서 입도분석과 SEM을 통해 입자크기와 입도 분포도를 조사하였고, 가교제를 첨가하여 활성화 된 분말표면의 재가교 여부를 조사하였다. Solid형의 경우 가장 좁은 입도 분포도와 작은 입자크기, 상대적으로 높은 인장 물성을 나타내었다. 화학적 표면 탈황을 유도하기 위해 표면활성화제를 첨가한 결과 표면활성화제의 첨가량이 증가할수록 효율적인 탈황이 유도되었다. TPE제조를 위해 폴리올레핀과의 블렌드 시 활성화된 EPDM 분말의 동적가황 가능성을 확인하기 위하여 가교제를 첨가하여 반응을 진행한 결과 황을 첨가할 경우 가교반응이 진행되지 않았고, DCP(dicumyl peroxide)의 경우 6 phr이 첨가되었을 때 효율적인 표면 가교반응 및 최적의 인장 물성을 나타내었다. 화학적 표면 활성화를 유도한 폐 EPDM 분말의 경우 표면활성화제의 첨가로 인해 냄새가 발생되는데, 이를 제거하기 위하여 수분흡착 공정과 rose oil 첨가 공정을 진행하였으며 GC/MS를 통해 냄새 성분을 분석하였다.