• Computers and Concrete
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• v.22 no.1
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• pp.93-100
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• 2018

It is seldom possible that geotechnical materials like rocks and concretes found without joints, cracks, or discontinuities. Thereby, the impact of micro-cracks on the mechanical properties of them is to be considered. In the present study, the effect of micro-crack on the failure mechanism of rock specimens under uniaxial compression was investigated experimentally. For this purpose, thermal stress was used to induce micro-cracks in the specimens. Several cylindrical and disk shape specimens were drilled from granite collected from Zanjan granite mine, Iran. Some of the prepared specimens were kept in room temperature and the others were heated by a laboratory furnace to different temperature levels (200, 400, 600, 800 and 1000 degree Celsius). During the experimental tests, Acoustic Emission (AE) sensors were used to monitor specimen failure at the different loading sequences. Also, Scanning Electron Microscope (SEM) was used to distinguish the induced micro-crack by heating in the specimens. The fractographic analysis revealed that the thin sections heated to $800^{\circ}C$ and $1000^{\circ}C$ contain some induced micro-fractures, but in the thin sections heated to $200^{\circ}C$, $400^{\circ}C$ and $600^{\circ}C$ have not been observed any micro-fracture. In the next, a comprehensive experimental investigation was made to evaluate mechanical properties of heated and unheated specimens. Results of experimental tests showed that induced micro-cracks significantly influence on the failure mode of specimens. The specimens kept at room temperature failed in the splitting mode, while the failure mode of specimens heated to $800^{\circ}C$ are shearing and the specimens heated to $1000^{\circ}C$ failed in the spalling mode. On the basis of AE monitoring, it is found that with increasing of the micro-crack density, the ratio of the number of shear cracks to the number of tensile cracks increases, under loading sequences.

• Composites Research
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• v.16 no.6
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• pp.48-55
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• 2003

This research makes comparisons of empirical fatigue-lives between AC8A A1 alloy and the metal matrix composites(A1/A12O3, A1/A12O3/A12O3p), and also includes comparisons of fatigue-lives between empirical fatigue-lives and estimated fatigue-lives from regular-periodic load testing, AE method to predict fatigue-crack initiation before visible in sight and SEM(scanning electron microscope) photographs of each material. According to the test results of the notched specimen. the fatigue life of the hybrid metal matrix composites and the metal matrix composites, which are more brittle than the base matrix was shorter than that of the base matrix under both types of loads. In addition, the fatigue-life estimated from the damage summation method and that from experiments at random loads were fairly identical.

• Journal of Korea Multimedia Society
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• v.5 no.4
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• pp.426-433
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• 2002

In this paper, we have studied the images which have been reconstructed by using combination of images acquired by the variation of operating frequency. When inner images have been reconstructed, they have been superposed by the surface state effect. In this case, the images of the phase object can be enhanced by the contrast of inner images. In this experiment, there are two kinds of specimens, one is a reference block haying 1/4T, 1/2T, 3/4T side drilled holes as main run piping material 111 the steam generator in NPP(Neuclear Power Plant)s and the another is a part of a hemisphere type specimen having about 1-2㎜ distance gap. It has been shown that the two results of defect shapes have better than before in this processing and phase contrast grow about twice. And we have constructed the acoustic microscope by using a quadrature detector that enables to acquire the amplitude and phase of the reflected signal simultaneously Further more ore have studied the reconstruction method of the amplitude and phase images and the enhancement method of the defect images contrast.

• Journal of the Korean Society for Nondestructive Testing
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• v.23 no.5
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• pp.418-428
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• 2003

Fiber fracture is one of the dominant failure phenomena affecting the total mechanical Performance of the composites. Fiber fracture locations were measured through the conventional optical microscope and the nondestructive acoustic emission (AE) technique and then were compared together as a function of the epoxy matrix modulus and the fiber surface treatment by the electrodeposition method (ED). Interfacial shear strength (IFSS) was measured using tensile fragmentation test in combination of AE method. ED treatment of the fiber surface enlarged the number of fiber fracture locations in comparison to the untreated case. The number of fiber fracture events measured by the AE method was less than optically obtained one. However, fiber fracture locations determined by AE detection corresponded with those by optical observation with small errors. The source location of fiber breaks by AE analysis could be a nondestructive, valuable method to measure interfacial shear strength (IFSS) of matrix in non-, semi- and/or transparent polymer composites.

• Journal of the Korean Society for Nondestructive Testing
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• v.15 no.1
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• pp.277-290
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• 1995

The study was carried out to analyze the fracture behavior and the acoustic emission(AE) characteristics and to find the relationship among tensile strength, fracture toughness and cure pressure in owe process of the carbon fiber reinforced composites of two types, $[0^{\circ}/90^{\circ}]_{2S}$ and $[0^{\circ}\;_2/90^{\circ}\;_2]_S$. AE signals were detected during the curing process, tensile tests and fracture toughness tests by acoustic emission(AE) measurements, respectively. Tensile strengths showed that the less cure pressurizing steps and the side of $[0^{\circ}/90^{\circ}]_{2S}$ specimens had the higher strengths than those of the others. Fracture toughness by the change of test temperature showed nearly same values in the same temperature region, but the higher test temperature had the lower fracture toughness values. In order to examine the relationship between fracture behavior of CFRP in tensile and fracture toughness tests and AE signals, the post processing for AE parameters of AE data and the observations of microscope and SEM have been carried out respectively.

• Composites Research
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• v.20 no.3
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• pp.55-62
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• 2007

Interfacial evaluation and durability of Jute and Hemp fibers/polypropylene (PP) composites were investigated. Moisture content of various treated conditions were measured by thermogravimetic analyzer (TGA). After boiling water test, mechanical properties and IFSS between Jute, Hemp fibers and PP matrix decreased. On the other hand, work of adhesion increased due to swelled fibril by water. Surface energies of Jute and Hemp fibers before and after boiling water test were obtained using dynamic contact angle measurement. IFSS was not always consistent with thermodynamic work of adhesion. In boiling water case, since Jute and Hemp fibers could be swelled by water, surface area and moisture infiltration space increased. Environmental effect on microfailure modes of Jute or Hemp fibers and Jute or Hemp fibers/PP composites were obtained by observing via optical microscope and by monitoring acoustic emission (AE) events and their AE parameters. After boiling water test, unlike Hemp fiber, microfailure process of Jute fiber could occur due to low tensile strength by swelled fibril. In addition, AE events occurred more and AE amplitude and energy became lower than those of before boiling water test.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.06a
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• pp.450-450
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• 2009

최근 전세계적으로 태양전지의 대량보급에 따라 실리콘 원료의 공급에 차질이 생겨 원자재 값이 상승하는 추세에 있다. 결정질 실리콘 태양전지의 제조비용중 실리콘 재료 및 웨이퍼가 차지하는 비율은 약 50~60%정도로 높기 때문에 실리콘 웨이퍼의 두께를 감소시키는 것이 비용절감을 위한 효과적인 방법으로 기대되고 있다. 그러나 실리콘 웨이퍼의 두께가 앓아질수록 제조공정중 균열이나 파손이 발생할 가능성이 높아지기 때문에 이에 따른 실리콘 웨이퍼의 기계적 물성에 대한 연구가 필수적이라 할 수 있다. 본 연구에서는 현재 상용으로 사용되고 있는 크기가 5 인치인 $200{\mu}m$ 두께의 실리콘웨이퍼 (As-saw)를 약 80여개의 시편으로 절단한 후 각각의 파단강도를 부위별로 측정하였다. 또한 표면절단결함을 제거하는 saw damage etching(SDE) 시간을 제어하여 두께가 $150{\mu}m$, $130{\mu}m$인 웨이퍼를 준비하였다. 이들 시험편에 대해서도 부위별 파단강도를 측정하여 as-saw상태의 시험편과 비교하였다. 파단강도 측정은 4 접 굽힘시험을 통하여 측정하였으며 파단면은 주사전자현미경을 통하여 관찰하였다. 또한 실리콘 웨이퍼의 미세균열을 비파괴적으로 검출하기 위하여 100MHz 고주파수를 이용하는 초음파현미경(SAM, scanning acoustic microscope)을 이용하여 균열의 분포를 영상화하였다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.6
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• pp.1836-1842
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• 1996

In this paper, static and fatigue bending strengths of CFRP(carbon fiber reinforced plastic laminates having impact damage(FOD) are evaluated. Composite laminates used for this experiment are CF/EPOXY and CF/PEEK orthotropy laminated plates, which have two-interfaces[${0^0}_4{90^0}_4}$]$_sym$. A steel ball launched by the air gun colides against CFRP laminates to generate impact damages. The damage growth during bending fatigue test is observed by the scanning acoustic microscope(SAM). When the impacted side is compressed, the residual fatigue bending strength of CF/PEEK specimen P is greater that that of CF/EPOXY SPECIMEN B. On the other hand, when the impacted side is in tension, the residual fatigue bending strength of CF/PEEK speicemen P is smaller than that of CF/EPOXY specimen B. In the case of impacted-side compression, fracture is proposed from the transverse crack generated near impact point. On the other hand, fracture is developed toward the impact point from the edge of interface-b delamination in the case of impacted-side tension.

• Transactions of the Korean Society of Automotive Engineers
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• v.8 no.6
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• pp.247-258
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• 2000

It is thought that impact damages and hygrothermals can affect to CFRP (Carbon-fiber reinforced plastic) composite laminated due to the sensitivity on the composite laminated Therefore, this paper focuses on the fracture mechanisms experimentally based on a scanning acoustic microscope (SAM) when subjected to impact damages, i.e., foreign object damages(FOD), and also the influence of impact damages and hygrothermals on residual fatigue bending strength of CFRP laminates. Composite laminates used in the experiment are CF/EPOXY orthotropy laminated plates, which constist of two-interfaces [04/904]s. A steel ball launched by an air gun collides against CFRP laminates to generate impact damages. Bending fatigue tests are periodically interrupted for a nondestructive evaluation (NDE) measurement of the progrossive damages to built the fracture mechanism by impact damages, and three-point fatigue bending tests are carried out to investigate the influence of hygrothermals on the effect on the residual bending fatigue strength of CFRP laminates.

• Proceedings of the KSME Conference
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• 2008.11a
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• pp.322-326
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• 2008

In this paper, we have studied the images which have been reconstructed by using combination of images acquired by the variation of operating frequency. When inner images have been reconstructed, they have been superposed by the surface state effect. In this case, the images of the phase object can be enhanced by the contrast of inner images. There is a kind of specimen, one is a reference block having 1/4T, 1/2T, 3/4T side drilled holes as main run piping material of the steam generator in nuclear power plants. It has been shown that the two results of defect shapes have better than before in this processing and phase contrast grow about twice. And we have constructed the acoustic microscope by using a quadrature detector that enables to acquire the amplitude and phase of the reflected signal simultaneously. Further more we have studied the reconstruction method of the amplitude and phase images, the enhancement method of the defect images' contrast.