• 한국산학기술학회논문지
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• 제13권11호
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• pp.4963-4967
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• 2012

본 연구에서는 마그네슘 합금 AZ91D를 소재로 18인치 휠을 개발하고 동일사양의 알루미늄 휠과 해외 시판중인 마그네슘 휠과 기계적인 성질을 비교하였다. 저압주조 방식에 의해 18인치 마그네슘 휠 시제품을 제작하여 동일 사양의 알루미늄 휠 대비 26% 의 경량화를 이룩하였고, 신판 마그네슘 휠 대비 동등 수준의 연신율, 인장강도, 경도를 달성하였다. 향 후 주조와 열처리 공정 개선을 통해 항복강도 향상이 필요한 것으로 판단된다.

• 한국레이저가공학회지
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• 제18권1호
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• pp.1-6
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• 2015

High welding speed and narrow weld seam are favorable for welding of magnesium alloy. Magnesium alloy is recommended for the smart frame because it has several advantages such as low density, high thermal conductivity, EMI shielding capability and good cast ability. This study is for the assembly welding of the magnesium smart frame with high productivity, good performance and low cost. The window for battery on AZ91D frame produced by die-casting was prepared by CNC machining. Corresponding AZ31 blank of 0.2mm thickness was prepared by die-blanking cut. All system set was fixed at the stationary bed but the laser beam was manipulated by scanner up-to 1,000mm/s speed. The weld joint between AZ31 sheet and AZ91D frame was welded by fiber laser on 850~1,000W output power. The joint showed penetration enough but some humping bead. The distortion by the weld heat was almost free because of the quick dissipation of the heat by small beam size and fast welding. Consequently, the thinner magnesium foil was assembled successfully to the magnesium frame of mobile phone.

• 한국표면공학회지
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• 제50권6호
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• pp.432-438
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• 2017

AZ91D casting alloy requires an advanced plasma anodizing processing because large amount of defects are liable to generate during anodization. In this study, plasma electrolytic oxidation (PEO) of AZ91D Mg alloy was conducted by the application of either constant voltage or current using a pulse mode and its effects on pore formation, surface roughness and corrosion resistance were investigated. The PEO films showed a three-layer structure. The PEO film thickness was found to increase linearly with voltage. The surface roughness, Ra, ranged between $0.2{\mu}m$ and $0.3{\mu}m$. The corrosion resistance increased from RN 3.5 to 9.5 by the PEO treatment when evaluated according to the 72 hour salt spray test. The PEO-treated surface exhibited higher pitting potential than the raw material.

• 한국주조공학회지
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• 제28권1호
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• pp.20-24
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• 2008

The characteristics, such as roughness, thickness, microhardness and corrosion resistance, of plasma electrolytic oxide coatings on AZ91D alloy were investigated under the processing condition of various coating times. The coatings on AZ91D alloy consisted of MgO, $MgAl_{2}O_{4}$ and $Mg_{2}SiO_{4}$ oxides. The surface roughness and thickness of coatings became larger with increasing the coating time. The microhardness in cross section of coatings was much higher than not only that in surface but that in the conventional anodic oxide coatings, which increased progressively as the coating time increased. After being immersed in 3.5%NaCl solution and methyl alcohol, the corrosion resistance of AZ91D alloy was markedly improved by plasma electrolytic oxidation coating treatment, and the AZ91D alloy coated for 50min revealed excellent corrosion resistance.

• 열처리공학회지
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• 제28권5호
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• pp.229-238
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• 2015

The effects of Sn addition and solution treatment on corrosion behavior were studied in AZ91 magnesium casting alloy. The addition of 5%Sn contributed to the introduction of $Mg_2Sn$ phase, to the reduction in dendritic cell size and to the increase in the amount of secondary phases. After the solution treatment, trace amount of $Al_8Mn_5$ particles were observed in the ${\alpha}$-(Mg) matrix for the AZ91 alloy, while $Mg_2Sn$ phase with high thermal stability was additionally found in the AZ91-5%Sn alloy. Before the solution treatment, the AZ91-5%Sn alloy had better corrosion resistance than the Sn-free alloy, which is caused by the enhanced barrier effect of the (${\beta}+Mg_2Sn$) phases formed more continuously along the dendritic cell boundaries. It is interesting to note that after the solution treatment, the corrosion rate of both alloys became increased, but the Sn-added alloy showed higher corrosion rate than the Sn-free alloy. The microstructural examination on the corroded surfaces revealed that the remaining $Mg_2Sn$ particles in the solution-treated AZ91-5%Sn alloy play a role in accelerating corrosion by galvanic coupling with the ${\alpha}$-(Mg) matrix.

• 열처리공학회지
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• 제31권5호
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• pp.231-236
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• 2018

The purpose of this study was to investigate the microstructural characteristics and hardness distribution of AZ91 magnesium alloy furnace-cooled to room temperature after solution treatment, and to compare the results with those of as-cast condition. The as-cast alloy showed a partially divorced eutectic ${\beta}(Mg_{17}Al_{12})$ phase and discontinuous precipitates (DPs) with a lamellar morphology, while only DPs were observed in the furnace-cooled alloy. The DPs in the furnace-cooled AZ91 alloy had various apparent interlamellar spacings, which would be ascribed to the different transformation temperatures during the furnace cooling. The average hardness for the furnace-cooled alloy is similar to that for the as-cast alloy. It is interesting to note that the hardness values of the furnace-cooled alloy were distributed over a narrower range than those of the as-cast alloy. This is likely to be caused by the relatively more homogeneous microstructure of the furnace-cooled alloy in comparison with the ascast one.

• 한국재료학회지
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• 제9권7호
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• pp.715-723
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• 1999

마그네슘은 20여년간 자동차 산업에서 휠소재로 사용되어 왔다. 마그네슘 휠은 무게가 알루미늄 휠보다 25% 가벼워서 주행성이 우수하다. 이 연구의 목적은 사형주조 및 영구금형주조 공정에 의한 AZ91D 합금제 췰을 개발하는 것이다 보호개스$(SF_6+CO_2)$를 사용하는 비플럭스 용해기술을 적용하여 용탕의 산화와 불순물의 유입을 배제하였다 마그네슘 용탕은 가압식 펌프시스템을 사용하여 가열된 파이프를 통하여 모울드에 자동으로 공급된다. 열처리 및 인고트의 조성에 따른 AZ91B 합금제 휠의 기계적 특성을 조사하였다.

• 소성∙가공
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• 제8권3호
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• pp.283-283
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• 1999

In the present study, the effect of microporosity on the tensile properties of as-cast AZ91D magnesium alloy was investigated through experimental observation and numerical prediction. The test specimens were fabricated by die-casting and gravity-casting. For gravity-casting, the inoculation and use of various metallic moulds were applied to obtain a wide range of microporosity. The deficiency of the interdendritic feeding of the liquid phase acted as d dominant mechanism on the formation of the micropores in the Mg-Al-alloys, rather than the evolution of hydrogen gas. Although tensile strength and elongation has a nonlinear and very intensive dependence upon microporosity, the yield strength appeared to have a linear relationship with microporosity. However, it was possible to quantitatively estimate the linear contribution of microporosity on the individual tensile property far a range of microporosity, which was below about B %. The numerical prediction suggests that the effect of microporosity on fractured strength and elongation decreased as the strain hardening exponent increased. Furthermore. the shape and distribution of micropores may play a more dominant role than local plastic deformation on the tensile behavior of AZ9lD alloy.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.516-521
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• 2002

A study was carried out to grow an understanding of the microstructural development of friction stir welds on an AZ91D magnesium alloy, and to evaluate the mechanical properties of the welds. AZ91D plates with the thickness of 4mm were used, and the microstructural development of the weld zone was investigated using optical and scanning electron microscopes. Square butt welding joint with good quality was obtained at the conditions of under 187mm/min of travel speed with 1100 to 1250 rpm of tool rotation speed. The microstructure within the weld region consisted of fine equiaxed grains with no evidence of the original dendritic structure. The hardness tests showed slightly increased harness in the weld region, and the minimum hardness measured is in that of the parent material. Tensile strength of the weld zone was remarkably improved due to very fine recrystallized structure. XRD pattern of weld zone revealed the removal of $\beta$ intermetallic compounds, $Mg_{17}$Al$_{12}$, which had been distributed in the base metal.l.

• 한국재료학회지
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• 제23권2호
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• pp.112-115
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• 2013

One of the most important characteristics of Mg alloys is the high ratio of strength to weight. This is why there is a high demand for applications with these alloys in the transportation industries to reduce the fuel consumption and to save energy. In addition, magnesium (and its alloys) is of considerable interest as a structural material, especially in the aerospace and automotive industries thanks to its low density. However, its major drawback is its high sensitivity to corrosion. Therefore, its use requires the application of a surface treatment. This study used a die-casted AZ91D Mg alloyand all the samples were annealed (in $120^{\circ}C$). The surface microstructure and phase distribution in thin-walled AZ91D magnesium components cast on a hot-chamber die-casting machine were investigated by optical microscopy and scanning electron microscopy. The reflectance differences in the bulk state comparison with the annealing state are caused by hydrogenation presence of the Mg layer under an oxidation surface layer.