• 열처리공학회지
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• 제37권2호
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• pp.66-72
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• 2024

To investigate the effect of deformation condition on microstructure and texture formation behaviors of AZ91 magnesium alloy with three kinds of initial texure during high-temperature deformation, plane strain compression tests were carried out at high-temperature deformation conditions - temperature of 673 K~723 K, strain rate of 5 × 10^-3s^-1, up to a strain of -1.0. To clarify the texture formation behavior and crystal orientaion distribution, X-ray diffraction and EBSD measurement were conducted on mid-plane section of the specimens after electroltytic polishing. As a result of this study, it is found that the main component and the accumulation of pole density vary depending on initial texture and deformation caondition, and the formation and development basal texture components ({0001} <$10\bar{1}0$>) were observed regardless of the initial texure in all case of specimens.

• Corrosion Science and Technology
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• 제8권6호
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• pp.227-231
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• 2009

Mg and Mg alloys have been used for lots of applications, including automobile industry, aerospace, mobile phone and computer parts owing to low density. However, Mg and Mg alloys have a restricted application because of poor corrosion properties. Thus, improved surface treatments are required to produce protective films that protect the substrate from corrosive environments. Environmental friendly Plasma Electrolytic Oxidation (PEO) has been widely investigated on magnesium alloys. PEO process combines electrochemical oxidation with plasma treatment in the aqueous solution. In this study, AZ91 Mg alloys were treated by PEO process in controlling the current with PC condition and treated time, concentration of NaF, NaOH, and $Na_2SiO_3$. The surface morphology and phase composition were analyzed using SEM, EDS and XRD. The potentiodynamic polarization tests were carried out for the analysis of corrosion properties of specimen. Additionally, salt spray tests were carried out to examine and compare the corrosion properties of the PEO treated Mg alloys.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2005년도 춘계학술발표대회 개요집
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• pp.232-234
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• 2005

• 한국주조공학회지
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• 제26권1호
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• pp.34-39
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• 2006

In the present study, the possibility of Mg-Zn-Y alloys as high temperature casting alloys has been investigated. The fluidity of alloys containing yttrium were better than that of commercial AZ91 alloy because the oxide layer on the surface reduced the reaction between melt, and air and mold, which would reduce the resistance during the process of filling the mold. However, this oxide film reduced the hot-tearing resistance. In the case of ZAW942, this alloy exhibited fluidity and hot-tearing resistance better than AZ91 alloy. Because of thermally stable quasicrystal and other phases obstructed the movement of grains, the creep resistance of alloys containing rare earth elements more than 2 wt% was better than that of AZ91 alloy.

• 마이크로전자및패키징학회지
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• 제17권3호
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• pp.71-77
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• 2010

마그네슘 합금은 낮은 밀도를 가지는 장점을 이용하여 자동차, 항공, 이동전화, 컴퓨터 등에 많이 쓰이고 있으나 기계적 강도가 낮고 내부식성이 좋지 않아 사용이 제한되었다. 마그네슘 합금 표면에 내식성 산화층을 형성하기 위하여 환경 친화적인 전해 플라즈마 산화법(PEO)을 연구에 사용하였다, PEO법은 수용약 중에서 플라즈마를 발생시켜 전기화학적 산화막을 형성시키는 방법이다. 인가전압과 전휴가 산화피마에 미치는 영향에 대하여 고찰하였다, 또한, 직류와 펄스전류를 사용하여 결과를 분석하였다. 펄스전류를 사용하고 정전류법을 사용한 경우에 치밀한 산화막을 얻을 수 있었다, 부식특성 분석을 위하여 양극산화분극방법을 이용하였다. 표면의 강도는 처리전의 AZ9ID에 비하여 5배 이상 증가하였다.

• 한국표면공학회지
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• 제30권6호
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• pp.365-373
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• 1997

316L and 420 Stainless steels were deposited onto AZ9ID commercial magnesium alloy by plasma spray process with various gas flow rate of, TEX>$H_2$ secondary gas. And hardness as well as were track volume, coefficient of friction also had been measured. wear and hardness were measured by using reciprocal configuration tribometer and microghardness tester, respectively. Also, the microstructure of the coatings surface the cross sectional area of coating surface and cross sectional area of coaing/Substrate interface had been analyzed with Scanning Electron Microscope(SEM) and Optical microscope(OM). Finally, optimal process parameters for the improvement of coating efficiency such as mechanical property and wear behavior were examined.

• 한국레이저가공학회지
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• 제13권4호
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• pp.21-24
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• 2010

Plasma electrolyte oxidation (PEO) surface treatment of magnesium alloy, an optical analysis method through reflection spectra were measured. As a result, the sample is formed on the membrane form of MgO or $Mg(OH)_2$ is in the form of oxide. The wavelength energy of surface treatment of magnesium alloy sample observed 0.23eV red shift. The measured reflectance spectra observed with the three different signals. This is due to $Mg(OH)_2$ oxide layer formed on porous hole.

• 대한금속재료학회지
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• 제46권1호
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• pp.13-19
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• 2008

To develop a recycling process of magnesium alloy scrap, a fundamental study on the distillation of magnesium alloy melt was carried out. Melt temperature, vacuum degree and reaction time were considered as experimental variables. The amount of vaporized magnesium melt per unit surface area of melt increases with the increase of melt temperature, reaction time and vacuum degree. The vapor condensed at the tip of water cooling Cu-condenser as a form of pine cone. Magnesium and zinc were vaporized easily from the melt. However, It's difficult to separate magnesium and zinc by vacuum distillation because vapor pressure of zinc is similar to one of magnesium. The contents of aluminum, manganese and iron, etc. in residual melt increase due to the decrease of magnesium and zinc content after the distillation of magnesium alloy.

• 한국재료학회지
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• 제29권11호
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• pp.657-663
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• 2019

In this work, we study physical and mechanical properties of oxide films formed on AZ91D magnesium alloy by plasma anodization at different temperatures. It is found that the higher the electrolyte temperature, the lower is the breakdown voltage of oxide layer. This is probably because films formed at higher temperatures are thinner and denser. Moreover, electrolyte temperature plays an important role in the physical properties of the films. As the electrolyte temperature increases from 20 to $50^{\circ}C$, the hardness of the oxide layer increases. Friction test against steel balls indicates that wear scars become narrower for films formed at higher temperatures because the films are harder, as indicated by the Vickers hardness. The thinner and denser nature of the oxide film formed at $50^{\circ}C$ is also advantageous for heat transfer when film is used as a heat sink. Laser flash test results show very fast heat transfer for AZ91D with plasma anodized oxide layer formed at higher temperatures.

• 한국마린엔지니어링학회:학술대회논문집
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• 한국마린엔지니어링학회 2006년도 전기학술대회논문집
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• pp.285-286
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• 2006

Magnesium is the lightest of all the structural metals having density of 1.74. It is approximately 2/3 lighter than aluminium, l/4 lighter than titanium alloy and 1/5 lighter than iron. Among the light-weight alloys, magnesium and its alloys show a good possibility for high performance aerospace and automotive applications, however the widespread use of magnesium alloys has been limited mainly by its poor oxidation and corrosion resistance. In this work, corrosion-resistive thin films were prepared onto the magnesium alloy substrate(AZ91D) by environmental friendly coating technique, ion plating method. And their corrosion protection mechanism were analyzed.