• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.03a
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• pp.81-84
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• 1997

The hot deformation behavior of SiCp/AA2024 composites reinforced with different sizes of SiCp reinforcements (1, 8, 15, 36, and 44${\mu}{\textrm}{m}$) was investigated by hot torsion tests. The hot restoration of the composites depending on the SiCp reinforcements particle size was studied from the effective stress - strain curves. Dynamic recrystallization (DRX) was occurred in the SiCp/AA2024 composites during the hot deformation at 320 - 43$0^{\circ}C$ under a strain rate of 1.0/sec. Also, the critical strain for DRX decreased with decreasing the reinforcement size of SiCp from 44 to 8${\mu}{\textrm}{m}$. The composite reinforced with SiCp of 8${\mu}{\textrm}{m}$ showed the highest flow stress (265 MPa) and the work hardening rate at 32$0^{\circ}C$ under a strain rate of 1.0/sec.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2011.05a
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• pp.39-39
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• 2011

Surface hardening mechanism of AA 2024 was investigated when shot peeningprocess with shot ball of Zn alloy was applied. Zn alloy was transferred into surface region of AA 2024, forming lamellar structure of Al and Zn phase. Nanocrystallization of AA 2024 and alloyed Zn phase was achieved by the different mechanisms. Furthermore, precipitations in AA 2024 remained undissolved. Lamellar structure with different nano-sized grains of two different phase and randomly distributed precipitations contributed to the surface hardening.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 1998.05a
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• pp.116-116
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• 1998

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 1998.05a
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• pp.117-117
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• 1998

• Journal of the Korean institute of surface engineering
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• v.53 no.2
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• pp.80-86
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• 2020

This paper is concerned with type of imperfections present within the anodic oxide films on AA2024 and surface hardness of the anodic film measured after ink-impregnation. The anodic oxide films were formed for 25 min at 40 mA/㎠ and 15±0.5℃ and 300 rpm of magnet stirring rate in 20% sulfuric acid solution. The ink-impregnation allows clear observations of not only the imperfections within the anodic oxide films but also an indentation mark on the oxide film surface made by a pyramidal-diamond penetrator for the hardness measurement. There were observed four different regions in the anodic oxide films on AA2024 and the surface hardness of the anodic oxide films appeared to be crucially dependent on the type of defects, showing 60~100 H_v on the oxide surface region I with large size black defect, 100~140 H_v on the oxide surface region II with large size grey defect, 140~170 H_v on the oxide surface region III with mall size black and/or grey defects and 170~190 H_v on the oxide surface region IV without defects. The pyramidal indentation marks were observed to be distorted in the regions with a large size black and grey defects, while no distortion of the indentation mark was observed in the regions with small size defects and without visible defects.

• Journal of Powder Materials
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• v.26 no.4
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• pp.275-281
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• 2019

An artificial neural network (ANN) model is developed for the analysis and simulation of correlation between flake powder metallurgy parameters and properties of AA2024-SiC nanocomposites. The input parameters of the model are AA 2024 matrix size, ball milling time, and weight percentage of SiC nanoparticles and the output parameters are density and hardness. The model can predict the density and hardness of the unseen test data with a correlation of 0.986 beyond the experimental data. A user interface is designed to predict properties at new instances. We have used the model to simulate the individual as well as the combined influence of parameters on the properties. Moreover, we have analyzed the calculated results from the powder metallurgical point of view. The developed model can be used as a guide for further composite development.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.10a
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• pp.216-219
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• 1997

Hot workability of SiCp/AA2024 composites reinforced with different vol. % of SiCp reinforcements (0, 5, 10, 15, 20, and 30 vol. %) was investigated by hot torsion tests. Hot restoration of the composites was studied from the flow curves and deformed microstructures. Dynamic recrystallization (DRX) was occurred in all the composites during the hot deformation at 370-43$0^{\circ}C$ under a strain rate of 1.0/sec. Also, the flow stress of the composites increased with increasing the SiCp reinforcement vol. % and the difference of flow stress between the composites decreased with increasing the deformation temperature.

• Journal of the Korean institute of surface engineering
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• v.53 no.6
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• pp.351-359
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• 2020

Formation behavior and properties of PEO (Plasma Electrolytic Oxidation) film on AA2024 were investigated under application of pulsed current as a function of Na3PO4 concentration in 0.05 M Na2SiO3 solution by analyzing voltage-time behavior, in-situ observation of arc generation, observation of surface morphology and measurements of thickness and surface roughness. Arc generation voltage decreased with increasing Na3PO4 concentration. Color difference of PEO films between edge and inner part disappeared by addition of Na3PO4. It was also observed that size of nodules on PEO film decreased with increasing Na3PO4 concentration. Thickness of PEO films formed on AA2024 increased with increasing Na3PO4 concentration. Whereas, surface roughness of PEO films decreased with increasing Na3PO4 concentration up to 0.05 M of Na3PO4 which is attributed to the deceased size of nodules on the PEO films. However, the surface roughness increased with increasing Na3PO4 concentration more than 0.07 M of Na3PO4 which seems to be due to the formation of non-uniform PEO films with smooth surface and large size pores formed by orange-colored big arcs. The experimental results suggest that added sodium phosphate less than 0.2 M in an alkaline silicate solution can contribute to the formation of relatively thick and uniform thickness of PEO films under arc generation voltage lower than 300 V.

• Corrosion Science and Technology
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• v.22 no.2
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• pp.90-98
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• 2023

In this study, cobalt oxide (Co₃O₄) and cobalt-doped magnetite (CoFe₂O₄) nanoparticles were synthesized by a hydrothermal method. They were then used as corrosion inhibitors for corrosion protection of AA2024-T3 aluminum alloys. These obtained nanoparticles were characterized by x-ray diffraction, field-emission scanning electron microscopy, and Zeta potential measurements. Corrosion inhibition activities of Co₃O₄ and CoFe₂O₄ nanoparticles were determined by performing electrochemical measurements for bare AA2024-T3 aluminum alloys in 0.05 M NaCl + 0.1 M Na₂SO₄ solution containing Co₃O₄ or CoFe₂O₄ nanoparticles. Corrosion protection for AA2024-T3 aluminum alloys by a water-based epoxy with or without the synthesized Co₃O₄ or CoFe₂O₄ nanoparticles was investigated by electrochemical impedance spectroscopy during immersion in 0.1 M NaCl solution. The corrosion protection of epoxy coating deposited on the AA2024-T3 surface was improved by incorporating Co₃O₄ or CoFe₂O₄ nanoparticles in the coating. The corrosion protection performance of the epoxy coating containing CoFe₂O₄ was higher than that of the epoxy coating containing Co₃O₄.

• Corrosion Science and Technology
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• v.19 no.1
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• pp.8-15
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• 2020

In this paper, the efficiency and the inhibition mechanisms of cobalt salts (cobalt nitrate and cobalt-exchange silica Co/Si) for the corrosion protection of AA2024 were investigated in a neutral aqueous solution by using the electrochemical impedance spectroscopy (EIS) and polarization curves. The experimental measurements suggest that cobalt cation plays a role as a cathodic inhibitor. The efficiency of cobalt cation was important at the concentration range from 0.001 to 0.01 M. The formation of precipitates of oxides/hydroxides of cobalt on the surface at low inhibitor concentration was confirmed by the Scanning Electron Microscopy/Energy Dispersive X-Ray Spectroscopy (SEM/EDS) analysis. EIS measurements were also conducted for the AA2024 surface covered by water-based epoxy coating comprising Co/Si salt. The results obtained from exposure in the electrolyte demonstrated the improvement of the barrier and inhibition properties of the coating exposed in the electrolyte solution for a lengthy time. The SEM/EDS analysis in artificial scribes of the coating after salt spray testing revealed the release of cobalt cations in the coating defect to induce the barrier layer on the exposed AA2024 substrate.