• Journal of Magnetics
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• 제13권3호
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• pp.110-113
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• 2008

In this study, heavy rare earth garnet $Tb_2Bi_1Ga_1Fe_4O_{12}$ powders were fabricated by a sol-gel and vacuum annealing process. The crystal structure was found to be single-phase garnet with a space group of Ia3d. The lattice constant $a_0$ was determined to be 12.465 ${\AA}$. From the analysis of the vibrating sample magnetometer (VSM) hysteresis loop at room temperature, the saturation magnetization and coercivity of the sample are 7.64 emu/g and 229 Oe, respectively. The N$\acute{e}$el temperature($T_N$) was determined to be 525 K. The M$\ddot{o}$ssbauer spectrum of $Tb_2Bi_1Ga_1Fe_4O_{12}$ at room temperature consists of 2 sets of 6 Lorentzians, which is the pattern of single-phase garnet. From the results of the M$\ddot{o}$ssbauer spectrum at room temperature, the absorption area ratios of Fe ions on 24d and 16a sites are 74.7% and 25.3%(approximately 3:1), respectively. These results show that all of the non-magnetic Ga atoms occupy the 16a site by a vacuum annealing process. Absorption area ratios of Fe ions are dependent not only on a sintering condition but also on the temperature of the sample. It can then be interpreted that the Ga ion distribution is dependent on the temperature of the sample. The M$\ddot{o}$ssbauer measurement was carried out in order to investigate the atomic migration in $Tb_2Bi_1Ga_1Fe_4O_{12}$.

• Food Science and Biotechnology
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• 제15권4호
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• pp.555-558
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• 2006

The chemical reduction of Pseudomonas syringae subsp. phaseolicola alginates produces neutral polymers of D-mannose and L-gulose in source specific ratios. L-Gulose was highly sensitive to degradation by 1N HCl at $100^{\circ}C$. As hydrolysis time increased, gulose recovery decreased to 22% after 4 hr, whereas 98% of the D-mannose was recovered under the same conditions. Thin layer chromatography showed the formation of a second product upon L-gulose acid hydrolysis. This new product had a rate of flow (Rf) value of 0.58, identical to that of 1,6 anhydro-${\beta}$-D-mannopyranose and very close to that of 1,6 anhydro-${\beta}$-D-glucopyranose (Rf=0.60). Because of the difference in acid sensitivity between L-gulose and D-mannose, normal acid hydrolytic techniques applied to reduced alginates produces erroneous mannuronic acid (M): guluronic acid (G) ratio's unless one accounts for the differential rates of destruction of each sugar.

• Geomechanics and Engineering
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• 제25권4호
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• pp.341-345
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• 2021

1D sand compression response to ko-loading experiences volume contraction from low to high effective stress regimes. Previous study suggested compressibility model with physically correct asymptotic void ratios at low and high stress levels and examined only for both remolded clays and natural clays. This study extends the validity of Enhanced Terzaghi model for different sand types complied from 1D compression data. The model involved with four parameters can adequately fit 1D sand compression data for a wide stress range. The low stress obtained from fitting parameters helps to identify the initial fabric conditions. In addition, strong correlation between compressibility and the void ratio at low stress facilitates determination of self-consistent fitting parameters. The computed tangent constrained modulus can capture monotonic stiffening effect induced by an increase in effective stress. The magnitude of tangent stiffness during large strain test should not be associated with small strain stiffness values. The use of a single continuous function to capture 1D stress-strain sand response to ko-loading can improve numerical efficiency and systematically quantify the yield stress instead of ad hoc methods.

• Earthquakes and Structures
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• 제8권2호
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• pp.443-462
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• 2015

Some model building codes stipulate that the design displacement of a building can be computed using the elastic static analysis results multiplied by the deflection amplification factor, $C_d$. This approach for estimating the design displacement is essential and appealing in structural engineering practice when nonlinear response history analysis (NRHA) is not required. Furthermore, building codes stipulate the consideration of accidental torsion effects using accidental eccentricity, whether the buildings are symmetric-plan, or asymmetric-plan. In some model building codes, the accidental eccentricity is further amplified by the torsional amplification factor $A_x$ in order to minimize the discrepancy between statically and dynamically estimated responses. Therefore, this warrants exploration of the reliability of statically estimated design displacements in accordance with the building code requirements. This study uses the discrepancy curves as a way of assessing the reliability of the design displacement estimates resulting from the factors $C_d$ and $A_x$. The discrepancy curves show the exceedance probabilities of the differences between the statically estimated design displacements and NRHA results. The discrepancy curves of 3-story, 9-story, and 20-story example buildings are investigated in this study. The example buildings are steel special moment frames with frequency ratios equal to 0.7, 1.0, 1.3, and 1.6, as well as existing eccentricity ratios ranging from 0% to 30%.

• Computers and Concrete
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• 제22권3호
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• pp.305-317
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• 2018

Steel reinforced Engineered Cementitious Composite (ECC) components have been proposed for seismic structural applications, for example in coupling beams, infill panels, joints, columns, and flexural members. The development of strain in the steel reinforcement of cementitious components has been shown to vary based on both the steel reinforcement ratio and the applied deformation history. Strain in the steel reinforcement of reinforced ECC components is an important structural response metric because ultimate failure is often by fracture of the steel reinforcement. A recently proposed bond-slip model has been successfully calibrated to cyclically tested reinforced ECC beams wherein the deformation history contained monotonically increasing cycles. This paper reports simulations of two-dimensional finite element models of reinforced ECC beams to determine the appropriateness and significance of altering a phenomenological bond-slip model based on the applied deformation history. The numerical simulations with various values of post-peak bond-slip softening stiffness are compared to experimental results. Varying the post-peak bond-slip softening stiffness had little effect on the cracking patterns and hysteretic response of the reinforced ECC flexural models tested, which consisted of two different steel reinforcement ratios subjected to two different deformation histories. Varying the post-peak bond-slip softening stiffness did, however, affect the magnitude of strain and the length of reinforcing bar that strain-hardened. Overall, a numerical model with a constant bond-slip model represented well various responses in reinforced ECC beams with multiple steel reinforcement ratios subjected to different deformation histories.

• Steel and Composite Structures
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• 제32권2호
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• pp.199-212
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• 2019

This paper presents an investigation on seismic behavior of out-of-code Q690 circular high-strength concrete-filled thin-walled steel tubular (HCFTST) columns made up of high-strength (HS) steel tubes (yield strength $f_y{\geq}690MPa$). Eight Q690 circular HCFTST columns with various diameter-to-thickness (D/t) ratios, concrete cylinder compressive strengths ($f_c$) and axial compression ratios (n) were tested under the constant axial loading and reversed cyclic lateral loading. The obtained lateral load-displacement hysteretic curves, energy dissipation, skeleton curves and ductility, and stiffness degradation were analyzed in detail to reflect the influences of tested parameters. Subsequently, a simplified shear strength model was derived and validated by the test results. Finally, a finite element analysis (FEA) model incorporating a stress triaxiality dependent fracture criterion was established to simulate the seismic behavior. The systematic investigation indicates the following: compared to the D/t ratio and axial compression ratio, improving the concrete compressive strength (e.g., the HS thin-walled steel tube filled with HS concrete) had a slight influence on the ductility but an obvious enhancement of energy dissipation and peak load; the simplified shear strength model based on truss mechanism accurately predicted the shear-resisting capacity; and the established FEA model incorporating steel fracture criterion simulated well the seismic behavior (e.g., hysteretic curve, local buckling and fracture), which can be applied to the seismic analysis and design of Q690 circular HCFTST columns.

• Smart Structures and Systems
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• 제22권1호
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• pp.41-55
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• 2018

Damping ratio and frequency have influence on dynamic serviceability or instability such as vortex-induced vibration and displacement amplification due to earthquake and critical flutter velocity, and it is thus important to make determination of damping ratio and frequency accurate. As bridges are getting longer, small scale model test considering similitude law must be conducted to evaluate damping ratio and frequency. Analysis conditions modified by similitude law are applied to experimental test considering different scale ratios. Generally, Nyquist frequency condition based on natural frequency modified by similitude law has been used to determine sampling rate for different scale ratios, and total time length has been determined by users arbitrarily or by considering similitude law with respect to time for different scale ratios. However, Nyquist frequency condition is not suitable for multimode system with noisy signals. In addition, there is no specified criteria for determination of total time length. Those analysis conditions severely affect accuracy of damping ratio. The focus of this study is made on the determination of minimum analysis conditions for different scale ratios. Influence of signal to noise ratio is studied according to the level of noise level. Free initial value problem is proposed to resolve the condition that is difficult to know original initial value for free vibration. Ambient and free vibration tests were used to analyze the dynamic properties of a system using data collected from tests with a two degree-of-freedom section model and performed on full bridge 3D models of cable stayed bridges. The free decay is estimated with the stochastic subspace identification method that uses displacement data to measure damping ratios under noisy conditions, and the iterative least squares method that adopts low pass filtering and fourth order central differencing. Reasonable results were yielded in numerical and experimental tests.

• 한국자기공명학회논문지
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• 제21권3호
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• pp.85-89
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• 2017

Pyrazinamidase (PncA) from Mycobacterium tuberculosis is the hydrolytic enzyme (hydrolase) that can hydrolyze substrate PZA to active form pyrazoic acid (POA). To investigate hydrolytic reaction of M. tuberculosis PncA, 1D NMR spectra were monitored at various molar ratios of PncA and PZA. The line-width of PZA was changed as PncA was added into PZA with different molar ratios. These results suggested that determination of PncA enzymatic activity could potentially serve as an indirect measure of PZA susceptibility.

• 농업과학연구
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• 제48권3호
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• pp.397-412
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• 2021

In Experiment 1, the impact of using diets sufficient in P on the performance of weaned piglet growth with or without a super dose of phytase was investigated. One hundred and twelve piglets were randomized into four treatments with 7 replicates (4 piglets·cage^-1). Bodyweight (BW), daily gain (ADG), daily intake (ADFI) and feed conversion ratios (FCR) were measured over three weeks. Treatments included a positive control (PC) with a Ca : P ratio of 0.80 : 0.50%. and the negative control (NC) had a Ca : P ratio of 0.60 : 0.50%. The PC plus phytase was denoted as PC+, and the NC with the phytase diet was designated as NC+. The PC diet was formulated to meet or exceed the NRC (2012) standards for pigs weighing 7 - 25 kgs. Better results were obtained with the PC diet (p > 0.1) compared to the NC diet. The super dose of phytase in the PC+ diet significantly improved the overall FCR (p < 0.1). For Experiment 2, the impact of different calcium (Ca)/phosphorous (P) ratios with or without supplementation of vitamin D₃ was determined. Ninety-six piglets were randomized into four treatments with 6 replicates (4 piglets·cage^-1). The PC, NC1 and NC2 diets had ratios of 0.80 : 0.50, 0.80 : 0.45, and 0.60 : 0.45%, respectively. The fourth diet (PCV) was the PC diet fortified with vitamin D₃. Improved results were observed with the PC diet (p > 0.1) compared to the NC diets. Supplementing dietary 25-OH-D₃ in the PCV diet led to numerically higher ADG and ADFI scores with lower FCR values at the early nursery stage (p = 0.0044), but the vitamin supplement did not significantly influence the growth.

• Asian-Australasian Journal of Animal Sciences
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• 제17권2호
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• pp.244-249
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• 2004

The effects of supplemental betaine ($Betafin^{(R)}$) in the drinking water (50 g/kg) (WB) or feed (100 g/kg) (FB) were investigated on male broiler chickens ($Cobb{\times}Cobb$) exposed to 4 h episodes of heat stress at $34{\pm}1^{\circ}C$ on day (d) 35 and $36{\pm}1^{\circ}C$ from d 36 to 41. Prior to (d 1 to 34) and following heat exposure (d 35 to 41), betaine supplementation had no significant effect on body weight, total feed intake and cumulative feed conversion ratios of broilers. The total water intake of WB chicks was lower compared to controls. Prior to heat exposure, there was no difference in percentage of mortality among the three dietary groups. Following the heat challenge period, although higher percentage of control chicks succumbed to the heat challenge as compared to those of WB, it was not significantly different. The WB and FB chicks were less hyperthermic than controls in response to the heat challenge. Irrespective of treatment groups, the heat treatment resulted in a marked elevation in heterophil/lymphocyte ratios (HLR). The WB birds, however, had smaller increase in HLR than those of controls during heat exposure. Antibody production against Newcastle disease vaccine on day 35 was not affected by betaine supplementation. On d 42, WB birds had higher antibody production than those of FB. It is concluded that the WB treatment, as measured by HLR, antibody production and mortality rate, has advantages over the FB group under heat stress conditions.