• Title/Summary/Keyword: 6W2H

Search Result 2,819, Processing Time 0.031 seconds

A Study On Synthesis of Nanostructured WC/Co composite Powders by Mechanochemical process (기계화학적방법에 의한 나노구조 WC/Co 복합 분말의 제조에 관한 연구)

  • 권대환;안인섭;하국현;김병기;김유영
    • Journal of Powder Materials
    • /
    • v.9 no.3
    • /
    • pp.167-173
    • /
    • 2002
  • A new approach to produce nanostructured WC/Co composite powders by a mechanochemical process was made to improve the mechanical properties of advanced hardmetals. Homogeneous spherical W-Co salt powders were made by spray drying of aqueous solution from ammonium metatungstate($(NH_4)_6(H_2W_{12}O_{40})\cdo4H_2O$,AMT) and cobalt nitrate hexahydrate (Co(NO$_3$)$_2$.6$H_2O$). spray dried W-Co salt powders were calcined for 1 hr at $700^{\circ}C$ in atmosphere of air. The oxide powder was mixed with carbon black by ball milling and this mixture was heated with various temperatures and times in $H_2$. The $WO_3/CoWO_4$ composite oxide powders were obtained by calcinations at $700^{\circ}C$. The primary particle size of W/Co composite oxide powders by SEM was 100 nm. The reduction/carburization time decreased with increasing temperatures and carbon additions. The average size of WC particle carburized at $800^{\circ}C$ by TEM was smaller than 50 nm.

Photometric Observation of the Asteroid-Comet Transition Object 4015 Wilson-Harrington

  • Kim, Myung-Jin;Choi, Young-Jun;Byun, Yong-Ik
    • The Bulletin of The Korean Astronomical Society
    • /
    • v.35 no.1
    • /
    • pp.87.2-87.2
    • /
    • 2010
  • Near-Earth asteroid-comet transition object 4015 Wilson-Harrington is a possible target of the joint European Space Agency (ESA) and Japanese Aerospace Exploration Agency (JAXA) Marco Polo sample return mission. 4015 W-H was discovered showing cometary activity by Albert G. Wilson and Robert G. Harrington at Palomar Observatory in 1949. After recovered in 1979, 4015 W-H has been observed at every apparition, it always was seen as a point source. We made time series observations for 4015 W-H using the 1.8m telescope with 2K CCD at Bohyunsan Observatory, on the nights of 2009 November 17-19. The geocentric distance of 4015 H-W was about 0.38 AU at that time. No trace of cometary activity is seen from our images. From the light curve analysis, we find a double-peaked rotational period of 2.2 hours with amplitude of 0.4 magnitude. Our result is much shorter than previous measurements of 3.6 hours (Harris & Young 1983) and 6.1 hours (Osip et al 1995). We will discuss possible origin of the period variations.

  • PDF

Synthesis of Alkylidyne Complexes of Br$(CO)_2(tmeda)M{\equiv}CC_{6}H_{4}Me$ (M = Cr, Mo, W). Crystal Structure of Br$(CO)_2(tmeda)M{\equiv}CC_{6}H_{4}Me$

  • Park, Joon T.;Cho, Jeong-Ju;Suh, Il-Hwan;Lee, Jin-Ho;Lim, Sung-Su;Ryu, Bo-Young
    • Bulletin of the Korean Chemical Society
    • /
    • v.14 no.2
    • /
    • pp.266-271
    • /
    • 1993
  • The reaction of $(CO_5$)M=C(OMe)Tol (M=Cr, Mo, W and $Tol=p-C_6H_4Me)$ and $BBr_3$ followed by treatment with tetramethylethylenediamine (TMEDA) yields a mixture of two diastereomers, trans, $cis-Br(CO)_2(tmeda)M{\equiv}$CTol [M=Cr(1a), Mo(2a), W(3a)] and cis, $trans-Br(CO)_2(tmeda)M{\equiv}$CTol [M=Cr(1b), Mo(2b), W(3b)], respectively. These compounds have been isolated as crystalline solids and characterized by spectroscopic (infrared, mass, $^1H$ and $^{13}C-NMR)$ data. The trans, cis-Br(CO)2(tmeda)Cr${\equiv}$CTol (1a), has been examine via a single crystal X-ray diffraction study : $BrCrO_2N_2C_{16}H_{23}$, Mr=407.27, triclinic, $P{\bar{1}},\;a=12.792(2),\;b=13.400(5),\;c= 11.645(4)\;{\AA},\;{\alpha}=101.26(2)^{\circ},\;{\beta}=103.04(2)^{\circ},\;{\gamma}=91.88(2)^{\circ},\;{\nu}=1907(1){\AA}^3,\;Z=2,\;{\rho}(calcd)=1.418\;gcm^{-3},\;{\lambda}(MoK{\alpha})=0.71069\;{\AA},\;{\mu}=26.25 cm^{-1},\;F(000)=831.97,\;T=295K,\;R=0.0977$ for 1332 significant reflections $[F_0>5{\sigma}(F_0)]$. There are two essentially equivalent molecules in the crystallographic asymmetric unit. Each molecule is octahedral with the bromide ligand trans to the alkylidyne carbon, the two cis-carbonyl ligands, and the bidentate TMEDA ligand.

Alcohol Fermentation Characteristics of Tapioca Using Raw Starch Enzyme (생전분 분해효소를 이용한 타피오카의 알콜발효 특성)

  • Jeong, Yong-Jin;Baek, Chang-Ho;Woo, Kyoung-Jin;Woo, Seung-Mi;Lee, Oh-Seuk;Ha, Young-Duck
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.31 no.3
    • /
    • pp.405-410
    • /
    • 2002
  • The optimum conditions of the alcohol fermentation with raw tapioca by simultaneous saccharification and alcohol fermentation (SSAF) were studied using raw starch enzyme. The optimum conditions for maximum alcohol production were 0.5% (w/w) of enzyme content, 250% (v/w) of added water content and 96 hr of fermentation time. The alcohol and reducing sugar contents were 11.7% and 306 mg% after 96 hr fermentation, respectively. During the fermentation pH decreased from 6.2 to 4.2 and total acidity increased from 0.11 to 0.43. Alcohol components were detected such as ethanol, methanol, iso-propanol, n-propylalcohol and iso-butylalcohol, besides acetaldehyde. We could construct raw starch fermentation conditions which was 250% (v/w) of added water content and 0.5% (w/w) of enzyme content. However, yield of raw starch alcohol fermentation was lower than that of steaming alcohol fermentation.

Comparative Genetic Characterization of Plasmids of Agrobacterium Species Isolated in Korea (한국산 Agrobacterium plasmid의 유전학적 성상에 관한 연구)

  • Kim, Jung-Hye;Koo, Yong-Bum;Lee, Ki-Yung;Chung, Jae-Kyu
    • Journal of Yeungnam Medical Science
    • /
    • v.1 no.1
    • /
    • pp.41-48
    • /
    • 1984
  • The soil bacterium Agrobacterium tumefaciens is a plant pathogen that cause3 crown gall tumors by infecting the wounded dicotyledonous plants and subsequent integration of bacterial DNA into plant nuclear DNA. Virulent A. tumefaciens strains harbor a large Ti (tumor-inducing) plasmid that carries genes essential for tumorigenesis. In the present study, 13 strains (Malus pumila Mill; $A_{1-3}$, Populus monilifera; $W_{1-6}$, Populus tomentiglandlosa; $P_{1-3}$ and Rosa species; $R_1$) of Agrobacterium isolated in korean crown gall tumors and plasmids were observed in 6 strains ($W_2$, $W_3$, $W_6$, $P_1$, $P_3$ and $A_2$). The test for crown gall tumor formation was resulted only in ATCC15955 and $KW_2$ strains inoculated into the stem of sun flower and the development was observed for 4 and 6 weeks after inoculation. Above two Ti plasmids (pTi) were purified by cesium chloride-ethidium bromide density gradient centrifugation and digested with restriction enzyme and fragments of pTiATCC 15955 and $pTiKW_2$ observed by EcoR I ; 25&27, Hind III; 23&21, BamH I ; each 20 and Hpa I ; 12&27, and sizes of pTiATCC15955 and and $pTiKW_2$ calculated as 200 and 87 kbases. Octopine was isolated from tumor tissue ($W_{1-6}$ and $P_{1-3}$) and these strains confirmed as octopine type.

  • PDF

A Study on the Basic Slacks Pattern for Middle Aged Women Based on Their Lower Body Shape Analysis (중년여성의 하반신 체형분류에 따른 슬랙스 원형 제작)

  • 성옥상;정인향
    • The Research Journal of the Costume Culture
    • /
    • v.7 no.6
    • /
    • pp.140-158
    • /
    • 1999
  • The purposes of this study are to examine the characters of the lower body shape in the middle aged women and to make slacks pattern on the base of four difference body shapes. The lower body shapes were classified into 4 types on the basis of their lateral view silhouettes. The slacks patterns were based on the lower body shape characters and resulted in followings. In “Type 1” of the right body shape with the standard protrusion of abdomen and hips, little difference from conventional patterns was seen in experiment pattern, in which the front waist girth was W/4+0.5㎝+0.5㎝+fold(2.5㎝) and the back waist girth W/4+0.5㎝-0.5㎝+dart(3.5㎝). The front hip girth was defined as H/4+2.0㎝+0.5㎝ and the back hip girth as H/4+2.0㎝-0.5㎝ due to its increased ease amount produced by abdominal fat deposition. In the experimental pattern of “Type 2” with prominent hips, the front and back differences of the waist girth and the hip girth and the hip girth were defined as 1.0㎝ and 2.0㎝ separately. Accordingly, the front waist girth was W/4+0.5㎝+1.0㎝+fold(2.0㎝), the back waist girth W/4+0.5㎝-0.1㎝+dart(6.5㎝), the front hip girth H/4+2.0㎝+1.0㎝ and the back hip girth H/4+2.0㎝-1.0㎝. In “Type 3” with the prominent abdomen and the flat hips, the front waist girth was set up as W/4+0.5㎝+0.5㎝+fold(4.5㎝) for the increased front fold amount and the back waist girth was W/4+0.5㎝+0.5㎝+dart(3.0㎝). The front hip girth was made as H/4+2.5㎝+0.5㎝ and the back hip girth H/4+2.5㎝-0.5㎝. In “Type 4” with prominent abdomen and hips, considered were ① the increased front fold amount due to the abdominal protrusion, ② the increased back dart amount and the decreased back dart length owing to the hips prominent and ③ the front and back differences of waist and hip girth for the lateral view silhouette. Therefore the front waist girth was defined as W/4+0.5㎝+2.0㎝+fold(5.0㎝), the back waist girth as W/4+0.5㎝-2.0㎝+dart(4.0㎝), the front hip girth as H/4+2.0㎝+1.0㎝ and the back hip girth as H/4+2.0㎝-1.0㎝. The sensory evaluation of appearance and comfort was appeared more suitable on the experiment pattern than on the conventional pattern.

  • PDF

Production of Amylase by a Filamentous Fungus, Strain FM04, and Enzymatic Hydrolysis of Food Waste (사상균 FM04에 의한 Amylase 생산 및 음식물 쓰레기의 효소학적 가수분해)

  • 김경철;배영수;김시욱;김성준
    • KSBB Journal
    • /
    • v.18 no.5
    • /
    • pp.363-370
    • /
    • 2003
  • A filamentous fungus, strain FM04 producing amylase was isolated from rotten yam peels and potatoes. The favorable conditions of cultivation factors such as, temperature, pH, and agitation speed of strain FM04 were 28∼30$^{\circ}C$, 5.0∼6.0, and 100 rpm, respectively. Starch was the best carbon source in the amylase production. Therefore, food wastes containing lots of starch were employed as the carbon source of the cultivation for the economical amylase production. 5.2 U/ml of amylase was obtained In the cultivation using 1 % (w/v) of food wastes. The amylase showed the highest activity at enzyme reaction conditions of 60$^{\circ}C$ and pH 4.5 and showed 90% of residual activity after the reaction at 50$^{\circ}C$ for 2 days. In the enzymatic hydrolysis reaction using 20% (w/v) of food wastes and 2.5 U/ml of amylase, 72.6 g/l of reducing sugar was obtained at the reaction condition of 50$^{\circ}C$, pH 4.5 for 2 days.

Experimental study on Thermal Comfort of Electric Vehicle Occupants Using Local Proximity Heating Module (국부 근접 난방 모듈을 이용한 전기차 탑승자의 열쾌적성에 대한 실험적 연구)

  • Chae-Yeol Lee;Jong-Han Im;Jae-Wook Lee;Sang-Hee Park
    • Journal of the Korean Society of Industry Convergence
    • /
    • v.27 no.3
    • /
    • pp.655-663
    • /
    • 2024
  • In order to meet the technological demand for indoor heating systems that ensure winter thermal comfort during the transition from internal combustion engines to electrification, a localized proximity heating module using surface heating elements was developed. The operational performance of heating module was tested in the low temperature chamber. The experiment conditions were varied by changing the chamber temperature (-10, 0℃), the air flow rate (6.2, 6.0, 4.2m3/h), the heater power (100, 80, 60, 40W). Thermal comfort model was confirmed using the CBE Thermal Comfort Tool applying ASHRAE standard 55. Under -10℃ condition, thermal comfort was satisfied at 23.4, 23.2℃ at power of 100W and air flow rate 6.0, 4.6m3/h. Under 0℃ condition, at power of 80W, air flow rate 6.2, 6.0m3/h, and at power of 60W, air flow rate 4.6m3/h showed results of 25.7, 26.1, 23.0℃, respectively, satisfying thermal comfort. This study analyzed the operating performance of the local proximity heating module in the low temperature chamber and applied thermal comfort model to prove applicability of local proximity heating module using surface heating elements and how to utilize the thermal comfort model.

Synthesis and characterization of the two-fold interpenetrated Tb(III)-based metal-organic framework (이중 상호 침투 구조를 갖는 신규 터븀(III) 기반 금속-유기 골격체의 합성 및 특성연구)

  • Song, Jeong Hwa
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.32 no.6
    • /
    • pp.225-230
    • /
    • 2022
  • A new two-fold interpenetrating two-dimensional (2D) Tb(III) metal-organic framework (MOF), [Tb(p-XBP4)2.5(H2O)2]·W(CN)8 (1), was prepared using a p-XBP4 (N,N'-p-phenylenedimethylenbis(pyridin-4-one)), Cs3[W(CN)8], and Tb(NO3)3·6H2O. The single crystal X-ray diffraction indicated that Tb-MOF exhibits a unique two-fold interpenetrating 2-D framework. It was also characterized through Fourier transform infrared spectroscopy (FTIR), and single and powder X-ray diffraction. To probe the molecular magnetic behavior, the magnetic properties of Tb-MOF were investigated by direct-current (DC) and alternating-current (AC) magnetic susceptibilities measurements and discussed.

A Study of Nerve Conduction Velocity of Normal Adults (정상성인의 신경전도속도에 관한 연구)

  • Choi, Kyoung-Chan;Hah, Jung-Sang;Byun, Yeung-Ju;Park, Choong-Suh;Yang, Chang-Heon
    • Journal of Yeungnam Medical Science
    • /
    • v.6 no.1
    • /
    • pp.151-163
    • /
    • 1989
  • Nerve conduction studies help delineate the extent and distribution of the neural lesion. The nerve conduction was studied on upper(median, ulnar and radial nerves) and lower(personal, posterior tibial and sural nerves) extremities in 83 healthy subjects 23 to 66 years of age. and normal values were established(Table 1). The mean motor terminal latency (TL) were : median. 3.6(${\pm}0.6$)milliseconds ; ulnar. 2.9(${\pm}0.5$) milliseconds ; radial nerve. 2.3(${\pm}0.4$) milliseconds. Mean motor nerve conduction velocity(MNCV) along distal and proximal segments: median. 61.2(${\pm}9.1$) (W-E) and 57.8(${\pm}13.2$) (E-Ax) meters per second ; ulnar. 63.7(${\pm}9.1$) (W-E) and 50.(${\pm}10.0$) meters per second. Mean sensory nerve conduction velocity(SNCV) : median. 34.7(${\pm}6.7$) (F-W), 63.7(${\pm}7.1$) (W-E) and 62.8(${\pm}12.3$) (E-Ax)meters per second ; ulnar. 38.0(${\pm}6.7$)(F-W), 63.4(${\pm}7.5$) (W-E) and 57.0(${\pm}10.1$) (E-Ax)meters per second ; radial, 45.3(${\pm}6.8$) (F-W) and 64.2(${\pm}11.0$) (W-E) meters per second ; sural nerve, 43.4(${\pm}6.1$) meters per second. The amplitudes of action potential and H-reflex were also standardized. Mean H latency was 28.4(${\pm}3.2$) milliseconds. And. the fundamental principles, several factors altering the rate of nerve conduction and clinical application of nerve stimulation techniques were reviewed.

  • PDF