• 한국결정성장학회지
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• 제15권4호
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• pp.145-151
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• 2005

어두운 적색을 나타내는 아프리카산 천연루비의 색상개선을 열처리법과 수열처리법을 이용하여 행한 결과, 열처리법은 색상이 떨어지는 역효과가 발생하였다. 그러나 수열처리법의 경우에는 색상과 투명도가 향상되었다. 아프리카산 천연루비의 색상개선에 대한 수열처리 조건은 다음과 같다. 즉, 수열용매 1M $Na_2CO_3-0.9M\;K_2CO_3$, 반응온도: $450^{\circ}C$, 반응 시간: 48hrs, 충전율: $30\%$, 압력: 375atm이었다. 이와 같은 조건에서 얻어진 루비의 특성을 평가한 결과, ICP/MS와 XRF 분석결과로부터 수열처리 후 $Cr^{3+},\;Fe^{3+},\;Ti^{4+}$ 등의 함량이 수열처리 전의 루비에 비해 감소됨을 알 수 있었으며, 이로 인하여 적색이 밝아지는 것을 색차계 분석결과로부터 알았다. 이 결과는 수열처리 전과 비교하였을 때 $Cr^{3+}$ 이온의 전자전이에 의해 발생되는 발광피크의 강도가 수열처리 후 감소한 PL분석결과와 잘 일치하였다.

• Biomolecules & Therapeutics
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• 제14권1호
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• pp.40-44
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• 2006

Mirtazapine is an antidepressant agent with dual action on both the noradrenergic and serotonergic neurotransmitter systems. A simple high performance liquid chromatographic method has been developed and validated for the quantitative determination of mirtazapine in human plasma. A reversed-phase Cl8 column was used for the determination of mirtazapine with a mobile phase composed of 0.01M ammonium acetate solution (pH 4.2) and acetonitrile (75:25, v/v%) at a flow rate of 1.2 mL/min. Terazosin hydrochloride was used as an internal standard. The fluorescence detector was set at excitation and emission wavelengths of 290 and 350 nm, respectively. Intra- and inter-day precision and accuracy were acceptable for all quality control samples including the lower limit of quantification of 3 ng/mL. Mirtazapine was stable in human plasma under various storage conditions. This method was used successfully for a pharmacokinetic study using plasma samples after oral administration of a single 30 mg dose as mirtazapine base to 8 healthy volunteers. The maximum plasma concentration of mirtazapine was $64.1{\pm}28.0ng/mL$ at 1.8 h, and the area under the curve and elimination half-life were calculated to be $674.1{\pm}218.5ng\;h/mL\;and\;23.4{\pm}3.8h$, respectively.

• 전기화학회지
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• 제7권4호
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• pp.179-182
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• 2004

The aim of this study is to investigate the initiation and propagation of crevice corrosion for ferritic stainless steel in artificial crevice based on micro capillary tube method. The 430 stainless steel in artificial crevice is potentiostatically polarized in different sodium chloride solutions. Potentiodynamic and potentiostatic polarization data were measured in situ. The potentials in the crevice were measured by depth profile using the 0.04 mm diameter micro capillary tube inserted in the crevice. The potentials in the crevice ranged from -220 mV to -360 mV vs SCE from opening to bottom of crevice, which are lower than the external surface potential, -200 mV vs SCE. Such a potential drop induced the change of the metal surface state from passive to active. The surface of metal is located in passive state in -200 mV but the inner surface keeps active state below -220 mV, Thus these results show that the It drop mechanism in the crevice was more objective for evaluation and the method was easier to reproduce. Therefore the potential drop is one of the reasons for crevice corrosion by measuring the potentials in narrow crevice with a new micro measuring system.

• 약학회지
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• 제31권5호
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• pp.330-337
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• 1987

The weak UV absorbing ephedrine alkaloids such as ephedrine, pseudoephedrine, methylephedrine and norephedrine could be analyzed by charge-transfer spectrophotometric method. The results obtained are summarized as follows: (1) It was possible to determine a weak UV absorbing ephedrine alkaloids using the intense charge-transfer UV bands in chloroform. (2) This method was suitable for the spectrophotometric determination of ephedrine alkaloids in mixed pharmaceutical preparation. (3) Linear relationship was found between absorbance and concentration in the range of 1.0$\times$$10^{-5}M$~5$\times$$10^{-5}M$ of ephedrine ($\varepsilon$= 2.72$\times$$10^{4}LM^{-1}cm^{-1}$ and pseudoephedrine ($\varepsilon$=2.84$\times$$10^{4]LM^{-1}cm^{-1}$), 1.0$\times$$10^{-5}M$~5$\times$$10^{-5}$M of methylephdrine ($\varepsilon$=1.68$\times$$10^{4}LM^{-1}cm^{-1}$) and 1/3$\times$$10^{-4}M$~4/3$\times$$10^{-4}M$ of norephedrine ($\varepsilon$=0.74$\times$$10^{4}LM^{-1}cm^{-1}$. (4) CT- complex of ephedrine, pseudoephedrine and methylephedrine has absorption maxima at 293nm and norephedrine have absorption maximum at 253nm. (5) CT-complexes were formed in a 1:1 ratio between ephedrine alkaloids and iodine in chloroform. (6) By UV, IR, and $^1H$-NMR spectra, it could be inferred that CT-complexes were formed by interaction between the basic nitrogen of ephedrine alkaloids as electron (n) donor and iodine as electron ($\sigma$) acceptor.

• 충청수학회지
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• 제23권4호
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• pp.893-902
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• 2010

In this article we study self-dual codes of length 6 over ${\mathbb{Z}}_m$. A classification of such codes for $m{\leq}24$ is given. Main tool for the classification is the new double cosets decomposition method given in the recent article of the author.

• 전자공학회논문지C
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• 제34C권9호
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• pp.84-101
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• 1997

Inferring and recognizing 3D objects form a 2D occuluded image has been an important research area of computer vision. The octree model, a hierarchical volume description of 3D objects, may be utilized to generate projected images from arbitrary viewing directions, thereby providing an efficient means of the data base for 3D object recognition. We present a fast algorithm of finding the 4 pairs of feature points to estimate the viewing direction. The method is based on matching the object contour to the reference occuluded shapes of 49 viewing directions. The initially best matched viewing direction is calibrated by searching for the 4 pairs of feature points between the input image and the image projected along the estimated viewing direction. Then the input shape is recognized by matching to the projectd shape. The computational complexity of the proposed method is shown to be O(n$^{2}$) in the worst case, and that of the simple combinatorial method is O(m$^{4}$.n$^{4}$) where m and n denote the number of feature points of the 3D model object and the 2D object respectively.

• 한국치위생학회지
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• 제11권4호
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• pp.595-602
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• 2011

Objectives : This study purpose were the effect of toothbrushing for decreasing halitosis for gingivitis and periodontitis patients. Methods : The university staffs were examined oral condition and analysised a change of oral health state score after using 3 types of toothbrushing. Results : The results were as followed : OHI-S shows that the decreasing effect takes place in the M. bass method and Tooth pick method, but shows no differences by each method. GI for Self test method shows decreasing effect after 2nd week during education while the M. bass method and Tooth pick method shows after 1st week during education. The M. bass method shows much greater effect of halitosis amongst 3 kind of method. PI for Self test method and Tooth pick method show decreasing effect. Decreasing effect during education shows until 2nd week by 3 kind of method, but it shows no differences after 3rd week. VSC(ppb) for M. bass method and Tooth pick method show decreasing effect. Decreasing effect during education shows after 3rd week by 3 kind of method, but it shows no differences until 2nd week. PHP for Self test method, M. bass method and Tooth pick method show decreasing effect after 2nd week during education. But, there is no differences of decreasing effect by among 3 kind of method. Conclusions : This study reports that it is necessary to carry outt further studies on the improvement of oral health management of adults based on the development of oral health education.

• 융합신호처리학회논문지
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• 제10권4호
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• pp.220-224
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• 2009

본 연구에서는 유체역학 분야의 Yabe 박사 팀에 의해 제안된 CIP법을 이용한 3차원 시간영역 음장해석법의 정밀도에 대해서 자세한 검토를 하였다. 즉, 3차원 CIP 음장해석의 위상오차의 특성과 전파방향에 따른 오차를 명확히 하고, 본 수치 해석법의 유효성을 나타내었다. 다차원 CIP법으로는 M형, C형, A형이 있지만, 본 논문에서는 M형 CIP법을 이용한 음장해석의 정밀도에 대해 검토하였다. 또, 종래의 수치해석법으로 staggered-grid 모델을 이용한 FDTD법에 따른 계산결과와의 비교 검토를 하였다. 본 논문의 검토에 의해 같은 이산화조건에서는 CIP법이 FDTD법보다 해석법이 가진 분산성이 적고, CIP법으로 계산된 음압 파형이 FDTD법으로 계산된 음압 파형보다 변형이 적은 것을 알 수 있었다.

• 한국표면공학회지
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• 제42권1호
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• pp.47-52
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• 2009

Cu-Ag powder having Core-Shell structure was prepared from by electroless plating method using agents such as $AgNO_3$, $NH_{4}OH$, Hydroquinone. Ag coated copper powders were analyzed using scanning electron microscopy(SEM) and energy dispersive X-ray spectrometer(EDX). The silver coating layer of copper powder was affected from various reaction conditions such as molar ratio of $NH_{4}OH$, $AgNO_3$, and pulp density. Free silver was generated below 0.1M or 0.3M and above of $NH_{4}OH$ mole ratio. Silver coating layer thickened as addition of $AgNO_3$. When the pulp density reached 12% with 0.2M $NH_{4}OH$, and 0.15M $AgNO_3$ at $4^{\circ}C$, silver was homogeneously distributed around the copper particles and free silver particles were not generated.

• 화약ㆍ발파
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• 제41권3호
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• pp.13-25
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• 2023

종래의 벤치발파 공법은 한 발파의 모든 발파공에 역기폭을 적용하지만 MDS (mixture detonation system) 발파공법에서는 각 발파공의 공간적 또는 시간적 순서에 따라 정기폭과 역기폭을 교대로 적용한다. 공간적 순서에 따라 교대 적용하는 공법을 SMDS (spatial MDS), 시간적 순서에 따르는 공법을 TMDS (temporal MDS)라 부른다. 또 하나의 변종으로서 MMDS (modified MDS)가 있는데, 이 공법은 비산문제가 있는 현장을 위한 특수공법이다. 본 연구에서는 암석파괴 효과의 측면에서 MDS 발파공법을 종래공법과 비교한다. 비교는 LS-DYNA 상에서 2열 벤치발파 모델에 대한 수치적 시뮬레이션으로 이루어진다. 수치모델에서는 SPH-FEM 연계기법을 적용한다. SPH 요소는 발파공 부근의 근거리 영역의 암석에 적용하고, FEM 요소는 그 바깥의 원거리 영역에 적용한다. 암석에 대한 재료모델은 RHT 모델을 사용한다. 실제로 시뮬레이션을 수행한 결과, 벤치고 3.0 m, 저항선 1.6 m의 경우에 SMDS 발파공법이 종래공법에 비해 최대 0.4 m 더 깊은 파괴영역을 보였다. 덧붙여, MMDS 발파공법의 경우, 여타 공법들에 비해 벤치면 전방으로의 암편의 비산속도가 약 2.0 m/s 더 낮게 나타났다.