• 제목/요약/키워드: 4M method

검색결과 11,369건 처리시간 0.043초

M10CN전자교환기 상태천이 Table의 재구성에 대한 연구

  • Lee, Yun-Bok;Kim, Hyeon-U
    • ETRI Journal
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    • 제5권4호
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    • pp.17-21
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    • 1983
  • Sine call handling for stored program control exchange can be regarded as finite state machine model of sequential process, the state transition concept is applied to describe its functions. Coding method of the state transition table applied to M10CN ESS call processing and concerned topics was discussed and proposed another method for reduction memory usage.

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Synthesis of galactosylglycerol from Melibiose as M-5 Intermediate (Melibiose로부터 M-5중간체 galactosylglycerol의 합성)

  • 차배천
    • YAKHAK HOEJI
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    • 제45권6호
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    • pp.575-581
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    • 2001
  • The galactolipid M-5, which showed anti-inflammatory activity is glycoglycerolipid isolated from the Okinawa marine sponge Phyllospongia foliascens. Glycolipids have been synthesized by various methods, especially it were generally known that synthetic method of M-5 analogue and synthetic method of various glycolipids by glycosidation after synthesis of glycerolipid part. The others, it was not suggested that synthetic method via glycosylglycerol obtained by degradation from diglycoside. This study was carried out to investigate the synthesis of galactosylglycerol from melibiose as M-5 intermediate. Synthesis of galactosylglycerol was accomplished by selective protection of hydroxy group of sugar and diol cleavage by Pb(OAc)$_4$. As a result, galactosylglycerol was synthesized by 8 steps pathway and their structures were elucidated by analysis instrument.

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Distance Estimation Using Convolutional Neural Network in UWB Systems (UWB 시스템에서 합성곱 신경망을 이용한 거리 추정)

  • Nam, Gyeong-Mo;Jung, Tae-Yun;Jung, Sunghun;Jeong, Eui-Rim
    • Journal of the Korea Institute of Information and Communication Engineering
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    • 제23권10호
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    • pp.1290-1297
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    • 2019
  • The paper proposes a distance estimation technique for ultra-wideband (UWB) systems using convolutional neural network (CNN). To estimate the distance from the transmitter and the receiver in the proposed method, 1 dimensional vector consisted of the magnitudes of the received samples is reshaped into a 2 dimensional matrix, and by using this matrix, the distance is estimated through the CNN regressor. The received signal for CNN training is generated by the UWB channel model in the IEEE 802.15.4a, and the CNN model is trained. Next, the received signal for CNN test is generated by filed experiments in indoor environments, and the distance estimation performance is verified. The proposed technique is also compared with the existing threshold based method. According to the results, the proposed CNN based technique is superior to the conventional method and specifically, the proposed method shows 0.6 m root mean square error (RMSE) at distance 10 m while the conventional technique shows much worse 1.6 m RMSE.

Studies on Isolative Determination of dl- Methylephedrine hydrochloride from Complex Preparation (복합제제(複合製劑) 성분중(成分中) dl-Methylephedrine hydrochloride의 분리정량(分離定量))

  • Kim, Byung-Hi;Yong, Jae-Ick
    • Journal of Pharmaceutical Investigation
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    • 제3권1_2호
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    • pp.5-15
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    • 1973
  • Fluorometric determination of dl-Methylephedrine hydrochloride from complex preparation were studied. According to the experimental results and considerations obtained the results for the following. (1) dl-Methylephedrine hydrochloride in Hydrochloric acid media occurs the fluorescens by Picrolonic acid and Cuppric acetate. (2) The maximum absorption fluorescence wave length of dl-Methylephedrine hydrochloride standard solution is $365m{\mu}$. (3) The relationship between the fluorescence proportions to concentration of standard solution at range of $4.2{\times}10^{-4}\;M$. $6{\times}10^{-4}M$. (4) dl-Methylephedrine hydrochloride was precisely determined even in the presence of various components, especially Chloropheniramine maleate, Dextromethorphan hydrobromide and Diphenylhydramine hydrochloride. (5) This method has high sensitivity and is simple in precedure. (6) This method be applicable with 99.79% accuracy and was 99.5% in complex preparation.

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Detection of Individual Tree Species Using Object-Based Classification Method with Unmanned Aerial Vehicle (UAV) Imagery

  • Park, Jeongmook;Sim, Woodam;Lee, Jungsoo
    • Journal of Forest and Environmental Science
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    • 제35권3호
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    • pp.181-188
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    • 2019
  • This study was performed to construct tree species classification map according to three information types (spectral information, texture information, and spectral and texture information) by altitude (30 m, 60 m, 90 m) using the unmanned aerial vehicle images and the object-based classification method, and to evaluate the concordance rate through field survey data. The object-based, optimal weighted values by altitude were 176 for 30 m images, 111 for 60 m images, and 108 for 90 m images in the case of Scale while 0.4/0.6, 0.5/0.5, in the case of the shape/color and compactness/smoothness respectively regardless of the altitude. The overall accuracy according to the type of information by altitude, the information on spectral and texture information was about 88% in the case of 30 m and the spectral information was about 98% and about 86% in the case of 60 m and 90 m respectively showing the highest rates. The concordance rate with the field survey data per tree species was the highest with about 92% in the case of Pinus densiflora at 30 m, about 100% in the case of Prunus sargentii Rehder tree at 60 m, and about 89% in the case of Robinia pseudoacacia L. at 90 m.

Determination of chlorophenols from the industrial wastewater by GC/MS (GC/MS를 이용한 산업폐수중의 염화페놀류 분석)

  • Myung, Seung-Woon
    • Analytical Science and Technology
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    • 제18권4호
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    • pp.320-328
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    • 2005
  • The most common five chlorophenols (4-chloro-3-methylphenol, 2,4,5-trichlorophenol, 2,4,6-trichlorophenol, 2,3,4,6-tetrachlorophenol, pentachlorophenol) were determined from the industrial wastewater by GC/MS. The samples were collected from the petrochemical company, textile company and leather making company. The developed analytical method was modified by USEPA Method 3510. The samples were extracted with dichloromethane under pH 2 and pH 5-6, and determined by the GC/MS with SIM mode. There were good linearities (above $R^2=0.9943$) on e ranges of the 0.1 ng/mL~10 ng/mL and 0.5 ng/mL~10 ng/mL, and the limit of detection were between 0.1 ng/mL and 0.5 ng/mL. The absolute recoveries were measured at the concentration of 1, 5, and 10 ng/mL, and the recovery was 71.6~98.9% except for PCP. The relative standard deviation (RSD) was 1.2~14.3% and it gave a good reproducibility for the assay. The bias, which shows the accuracy, was a good although it was a little high values (11.3~22.1%) at the low concentration (1 ng/mL).

Synthesis of $M(WO_4)$:Eu (M : Group 1 or 2) for LED and its Luminescent Properties

  • Park, Seung-Hyok;Kim, Chang-Hae;Park, Hee-Dong;Kim, You-Hyuk
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2002년도 International Meeting on Information Display
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    • pp.838-841
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    • 2002
  • $M(WO_4)$:Eu phosphor as a red emitting phosphor for LED was prepared by solid state method. Tungstate phosphors were exited at long wavelength ultra violet region. In special, the emission of Eu-doped $M(WO_4)$:Eu phosphor under the excitation of 410nm appeared at 613nm. $M(WO_4)$:Eu phosphors with M : Group 1 had a higher excitation intensity than those of the phosphors with M: Group 2 at long-wavelength UV.

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Direct Bonded (Si/SiO2∥Si3N4/Si) SIO Wafer Pairs with Four-point Bending (사점굽힘시험법을 이용한 이종절연막 (Si/SiO2||Si3N4/Si) SOI 기판쌍의 접합강도 연구)

  • Lee, Sang-Hyeon;Song, O-Seong
    • Korean Journal of Materials Research
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    • 제12권6호
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    • pp.508-512
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    • 2002
  • $2000{\AA}-SiO_2/Si(100)$ and $560{\AA}-Si_3N_4/Si(100)$ wafers, which are 10 cm in diameter, were directly bonded using a rapid thermal annealing method. We fixed the anneal time of 30 second and varied the anneal temperatures from 600 to $1200^{\circ}C$. The bond strength of bonded wafer pairs at given anneal temperature were evaluated by a razor blade crack opening method and a four-point bonding method, respectively. The results clearly slow that the four-point bending method is more suitable for evaluating the small bond strength of 80~430 mJ/$\m^2$ compared to the razor blade crack opening method, which shows no anneal temperature dependence in small bond strength.

Experimental and Kinetic Studies of Esterification of Glycerol Using Combustion Synthesized SO42-/CeO2-Al2O3

  • Veluturla, Sravanthi;Narula, Archna;Rao, D. Subba;Indraja., S;Kulkarni, Rajeswari. M.
    • Korean Chemical Engineering Research
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    • 제56권4호
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    • pp.592-599
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    • 2018
  • An increase in the global production of biodiesel has resulted in the newfound significance of its byproduct, glycerol. The synthesis of acetins is an economical avenue to enhance the value of glycerol derived from biodiesel. WE developed an eco-friendly process for the synthesis of fuel additives from glycerol using a mixed oxide $SO{_4}^{2-}/CeO_2-Al_2O_3$ as catalyst. The $CeO_2-Al_2O_3$ mixed oxide was synthesized by the combustion method and then sulfated. The characterization of the catalyst was by means of XRD, BET, FTIR, and SEM. The influence of temperature, mole ratio and catalyst loading on yield and selectivity of the acetins was studied for the esterification of glycerol. The reaction rate constants ($k_1$, $k_2$ and $k_3$) were estimated using optimization method in MAT lab, and the activation energies ($E_1$, $E_2$ and $E_3$) were determined by the Arrhenius equation. Furthermore, a kinetic model was developed.

Voltammetric Determination of Cobalt(Ⅱ) Using Carbon Paste Electrodes Modified with 1-(2-Pyridylazo)-2-naphthol

  • 배준웅;박유철;이상학;전우성;장혜영
    • Bulletin of the Korean Chemical Society
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    • 제17권11호
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    • pp.995-999
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    • 1996
  • A method for the determination of cobalt(Ⅱ) by differential pulse voltammetry using a carbon paste electrode constructed by incorporating 1-(2-pyridylazo)-2-naphthol(PAN) into a conventional carbon paste mixture composed of graphite powder and Nujol oil has been developed. Several influencing factors for the determination of cobalt(Ⅱ) were studied in detail and the optimum analytical conditions were found to be as follows: pH, 4.6; composition of electrode, 20%; temperature of deposition, 43 ℃; time of preconcentration, 15 min. Regeneration of the electrode surface for the continuous uses of the electrode was achieved by exposing the carbon paste electrode to an acidic solution. Response of the electrode was reproducible for the uses of five times and the relative standard deviations were 6.7 and 4.6% for 2.0×10-5 M and 4.0×10-6 M cobalt(Ⅱ), respectively. The calibration curve for cobalt(Ⅱ) obtained by differential pulse voltammetry was divided into two linear ranges of 1.7× 10-6-1.3×10-4 M and 2.0×10-7-8.0×10-7 M. The detection limit was estimated to be 1.3×10-7 M. The effects of coexisting ions were also investigated to test the applicability of the proposed method to the determination of cobalt(Ⅱ) in real samples.