• 제목/요약/키워드: 4-point bending

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Influence of nano alumina coating on the flexural bond strength between zirconia and resin cement

  • Akay, Canan;Tanis, Merve Cakirbay;Mumcu, Emre;Kilicarslan, Mehmet Ali;Sen, Murat
    • The Journal of Advanced Prosthodontics
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    • 제10권1호
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    • pp.43-49
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    • 2018
  • PURPOSE. The purpose of this in vitro study is to examine the effects of a nano-structured alumina coating on the adhesion between resin cements and zirconia ceramics using a four-point bending test. MATERIALS AND METHODS. 100 pairs of zirconium bar specimens were prepared with dimensions of $25mm{\times}2mm{\times}5mm$ and cementation surfaces of $5mm{\times}2mm$. The samples were divided into 5 groups of 20 pairs each. The groups are as follows: Group I (C) - Control with no surface modification, Group II (APA) - airborne-particle-abrasion with $110{\mu}m$ high-purity aluminum oxide ($Al_2O_3$) particles, Group III (ROC) - airborne-particle-abrasion with $110{\mu}m$ silica modified aluminum oxide ($Al_2O_3+SiO_2$) particles, Group IV (TCS) - tribochemical silica coated with $Al_2O_3$ particles, and Group V (AlC) - nano alumina coating. The surface modifications were assessed on two samples selected from each group by atomic force microscopy and scanning electron microscopy. The samples were cemented with two different self-adhesive resin cements. The bending bond strength was evaluated by mechanical testing. RESULTS. According to the ANOVA results, surface treatments, different cement types, and their interactions were statistically significant (P<.05). The highest flexural bond strengths were obtained in nano-structured alumina coated zirconia surfaces (50.4 MPa) and the lowest values were obtained in the control group (12.00 MPa), both of which were cemented using a self-adhesive resin cement. CONCLUSION. The surface modifications tested in the current study affected the surface roughness and flexural bond strength of zirconia. The nano alumina coating method significantly increased the flexural bond strength of zirconia ceramics.

CFRP 적층쉘의 적층구성 및 곡률 변화에 따른 관통 특성 (Penetration Characteristics of CFRP Laminated shells according to Stacking Sequence and Curvature)

  • 조영재;김영남;양인영
    • 한국정밀공학회지
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    • 제22권2호
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    • pp.164-171
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    • 2005
  • This study aims to examine an effect of stacking sequence and curvature on the penetration characteristic of a composite laminated shell. For the purpose, we manufactured specimens with different stacking sequences and curvatures, and conducted a penetration test using an air-gun. To examine an influence according to stacking sequence, as flat plate and curvature specimen had more plies, their critical penetration energy was higher, Critical penetration energies of specimen A and C with less interfaces somewhat higher than those of B and D with more interfaces. The reason that with less interfaces, critical penetration energy was higher is pre-impact bending stiffness of composite laminated shell with less interfaces was lower than that of laminated shell with more interfaces, but bending stiffness after impact was higher. And it is because interface, the weakest part of the composite laminated shell, was influenced by transverse impact. As curvature increases, critical penetration energy increases linearly. It is because as curvature increases, resistance to in-plane deformation as well as bending deformation increases, which need higher critical penetration energy. Patterns of cracks caused by penetration of composite laminated shells include interlaminar crack, intralaminar crack, and laminar fracture. A 0$^{\circ}$ply laminar had a matrix crack, a 90$^{\circ}$ply laminar had intralaminar crack and laminar fracture, and interface between 0$^{\circ}$and 90$^{\circ}$laminar had a interlaminar crack. We examined crack length and delamination area through a penetration test. For the specimen A and C with 2 interface, the longest circumferential direction crack length and largest delamination area were observed on the first interface from the impact point. For the specimen B and D with 4 interface, the longest crack length and largest delamination area were observed on the third interface from the impact point.

Mechanical Properties of CVD Diamond

  • Yoshikawa, Masanori;Hirata, Atsushi
    • The Korean Journal of Ceramics
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    • 제2권4호
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    • pp.212-215
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    • 1996
  • This paper focuses the strength and wear resistance of CVD diamond films. The strength of free-standing CVD diamond films synthesized by microwave plasm CVD, DC plasma CVD, RF plasma CVD and arc discharge plasma jet CVD has been measured by three-point bending test. The wear resistance of CVD diamod films has been evaluated by the pin-on-disk type testing. diamond films coated on the base of sintered tungsten carbide pin by hot filament CVD have been rubbed with a sintered diamond disk in muddy water. Volume removed wear of CVD diamond has been compared with stellite, WC alloy and bearing steel.

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NITINOL 형상기억합금의 열적/기계적 특성 평가 (Evaluation of Thermomechanical Characteristics of NITINOL Shape Memory Alloy)

  • 윤성호
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2001년도 춘계학술대회 논문집
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    • pp.683-686
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    • 2001
  • The thermomechanical characteristics of NITINOL shape memory alloy were evaluated using DSC with small samples and DMA with three-point bending specimens. The shape memory alloy of 54.4Ni/45.5Ti wt.% was used so that the austenite finish temperature was in the range of $50~100^{\circ}C$. Two types of sample were tested in the experiments corresponding to as-received and annealed conditions. Simple beam bending theory was used to calculate the dynamic moduli of the shape memory alloy. According to the results, a large discrepancy in transformation temperatures was found between DSC and DMA techniques. Annealing treatment was found to suppress the R-phase transformation during cooling and the secondary plateau in the austenite transformation. Such a heat treatment was also significantly influenced to raise the transformation temperatures and the moduli of the shape memory alloy.

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선박 공조닥트의 특성분석에 관한 사례 연구 - 유지관리용 로봇의 이동 알고리즘 개발을 위한 분석 - (A Case Study on the Analysis of Characteristics of Marine HVAC Duct - For the Development of Maintenance Robot's Movement Algorithm -)

  • 황광일
    • Journal of Advanced Marine Engineering and Technology
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    • 제30권2호
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    • pp.211-217
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    • 2006
  • This study is focused on the analysis of the characteristics of marine HVAC duct. These results will be applied to develope a robot which is for maintaining a cabin comfort, convenience and healthy through HVAC duct. The followings are the results of this study. (1) The evaluated items which proposed by at the view point of robot's function can be adapted to other vessels for the same purpose, (2) For the case of round type duct. the maximized conditions which robot has to have are straight length of 40.152mm, inclination of $45^{\circ}$. horizontal bending of $90^{\circ}$. increasing diameter of 1.28 times, and 0.625 times decreasing diameter in branch. (3) For the case of rectangular type duct. the maximized conditions are straight length of 15.987mm. aspect ratio of 4.17:1, inclination of $18.92^{\circ}$. horizontal bending of $90^{\circ}$, and 0.65 times decreasing diameter in branch.

섬유기기용 $Al_2O_3$계 세라믹스의 강도 특성 (Strength Properties of $Al_2O_3$ Ceramics with Textile Machinery)

  • 안병건;안석환;박인덕;남기우
    • 동력기계공학회지
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    • 제8권4호
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    • pp.44-48
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    • 2004
  • For many years researchers have been attempting to establish the relations among the preparation history, structure and properties of ceramics. In this study, the strength property of $Al_2O_3$ ceramics with components and giudes of the textile machinery was investigated. The optimized conditions of ressureless sintering were investigated in order to obtain the maximum strength of $Al_2O_3$ ceramics for using at the textile machinery. As the sintering conditions, $1,400{\sim}1,700^{\circ}C$ of temperatures and $30{\sim}150$ minutes of times were applied. Three-point bending test was conducted on the sintered materials to obtain the strength property. From test results, the optimum sintering temperature has $1,600^{\circ}C$. And the optimum sintering time in $1,600^{\circ}C$ has about 100 minutes.

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CeO2 안정화 정방정 Zirconia 다결정체(Ce-TZP)에 관한 연구(II) : Ce-TZP의 고온 기계적 성질과 파괴거동의 변화 (A Study on the Ceria Stabilized Tetragonal Zirconia Polycrystals(Ce-TZP)(II) : Mechanical Properties of Ce-TZP and its Fracture Behavior at Elevated Temperature)

  • 강대석;김문일;박정현;문성환;백승수
    • 한국세라믹학회지
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    • 제26권6호
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    • pp.789-794
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    • 1989
  • The high-temperature strength of Ce-TZP was measured at 200, 650 and 100$0^{\circ}C$ by 4-point bending test. And its fracture behavior was observed by SEM. Below $650^{\circ}C$ of the temperature, where monoclinic fraction was almost zero, the decreasing rate of bending strength was relatively slow, but above this temperature, high temperature strength was largely decreased as a result of the decrease of stress-induced transformation of zirconia. The observation of fracture surface bended at 100$0^{\circ}C$ indicated that the fracture mode changed from intergranular-into transgranular-form with regardless of ceria contents.

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Characteristics of Graphene/Metal Grid Hybrid Transparent Conductive Films

  • Kim, Sung Man;Kang, Seong Jun
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.429-429
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    • 2013
  • We present a systematic study of the electrical, optical and electromechanical properties of flexible graphene/metal grid hybrid transparent conductive electrodes using 4-point prove method, ultraviolet/visible spectrometer and inner/outer bending test system. The hybrid electrodes were synthesized by depositing a silver grid on a graphene surface. The sheet resistance of hybrid electrodes was as low as 30 Ω/square, while the transmittance was 90%. The electromechanical properties as a function of the change of bending radius were evaluated by measuring the change in resistance. The result will be presented in detail. We believe that these results will provide useful information for the flexible optoelectronic devices based on graphene transparent electrodes.

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감육된 탄소강배관의 변형과 파괴거동 (Deformation and Fracture Behavior of Wall Thinned Carbon Steel Pipes)

  • 안석환;남기우
    • 한국해양공학회지
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    • 제20권4호
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    • pp.17-23
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    • 2006
  • Monotonic four-point bending tests were conducted on straight pipe specimens, 102 mm in diameter with local wall thinning, in order to investigate the effects of the depth, shape, and location of wall thinning on the deformation and failure behavior of pipes. The local wall thinning simulated natural erosion/corrosion metal loss. The deformation and fracture behavior of the straight pipes with local wall thinning was compared with that of non wall-thinning pipes. The failure modes were classifiedas local buckling, ovalization, or crack initiation, depending on the depth, shape, and location of the local wall thinning. Three-dimensional elasto-plastic analyses were carried out using the finite element method. The deformation and failure behavior, simulated by finite element analyses, coincided with the experimental results.

세라믹스/금속 접합계면에서의 파괴력학적 강도평가에 관한 연구 (A study on the Fracture Mechanical Strength Evaluation in Joint Interface of Ceramics and Metal)

  • 최병기
    • 한국안전학회지
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    • 제11권3호
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    • pp.20-24
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    • 1996
  • Indentation fracture method and 4-point bending test are carried out to measure the residual stresses and the bending strength, and to investigate the mechanism of fracture mechanics in the bonded interface of ceramic and metal. The results obtained are as follows ; 1) The fracture patterns of bonded materials shows that the delamlnatlon fracture of Interfaces is stablely developed from the interfaces of ceramic/active metallic bonded materials at the specimen center, and the fracture is unstablely generated through a refraction on the middle ceramic. 2) Distribution of residual stresses is quantitatively investigated on the ceramic side of bonded materials. 3) It Is found that the residual stresses of interface vertical direction are concentrated on the bonded interface at the ceramic side.

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