• Advances in nano research
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• v.15 no.4
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• pp.305-313
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• 2023

This study is aimed to investigate the electrically conductive properties of epoxy nanocomposites exposed to an acidic environment under various mechanical loads. For simultaneous assessment of the acidic environment and mechanical load on the electrical conductivity of the samples, the samples with and without carbon nanotubes were exposed to the acidic environment under three different loading conditions for 20 days. Then, the aged samples' strength and flexural stiffness degradation under crude oil and bending stress were measured using a three-point flexural test. The aged samples in the acidic environment and under 80 percent of their intact ultimate strength revealed a 9% and 26% reduction of their electrical conductivity for samples with and without CNTs, respectively. The presence of nanoparticles declined flexural stiffness by about 16.39%. Scanning electron microscopy (SEM) images of the specimen were used to evaluate the dispersion quality of CNTs. The results of this study can be exploited in constructing conductive composite electrodes to be used in petroleum environments such as crude oil electrostatic tanks.

• Advances in nano research
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• v.15 no.4
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• pp.285-294
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• 2023

This study is aimed to investigate the electrically conductive properties of epoxy nanocomposites exposed to an acidic environment under various mechanical loads. For simultaneous assessment of the acidic environment and mechanical load on the electrical conductivity of the samples, the samples with and without carbon nanotubes were exposed to the acidic environment under three different loading conditions for 20 days. Then, the aged samples' strength and flexural stiffness degradation under crude oil and bending stress were measured using a three-point flexural test. The aged samples in the acidic environment and under 80 percent of their intact ultimate strength revealed a 9% and 26% reduction of their electrical conductivity for samples with and without CNTs, respectively. The presence of nanoparticles declined flexural stiffness by about 16.39%. Scanning electron microscopy (SEM) images of the specimen were used to evaluate the dispersion quality of CNTs. The results of this study can be exploited in constructing conductive composite electrodes to be used in petroleum environments such as crude oil electrostatic tanks.

• Structural Engineering and Mechanics
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• v.65 no.4
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• pp.381-388
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• 2018

Dynamic behaviour of beam carrying masses has attracted attention of many researchers and engineers. Many studies on the analytical solution of beam with concentric tip mass have been published. However, there are limited works on vibration analysis of beam with an eccentric three dimensional object. In this case, bending and torsional deformations of beam are coupled due to the boundary conditions. Analytical solution of equations of motion of the system is complicated and lengthy. Therefore, in this study, Differential Transform Method (DTM) is applied to solve the relevant equations. First, the Timoshenko beam with 3D tip attachment whose centre of gravity is not coincident with beam end point is considered. The beam is assumed to undergo bending in two orthogonal planes and torsional deformation about beam axis. Using Hamilton's principle the equations of motion of the system along with the possible boundary conditions are derived. Later DTM is applied to obtain natural frequencies and mode shapes of the system. According to the relevant literature DTM has not been applied to such a system so far. Moreover, the problem is modelled by Ansys, the well-known finite element method, and impact test is applied to extract experimental modal data. Comparing DTM results with finite element and experimental results it is concluded that the proposed approach produces accurate results.

• Steel and Composite Structures
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• v.49 no.4
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• pp.381-392
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• 2023

This study experimentally investigates the flexural behavior of steel-UHPC composite slabs composed of an innovative negative Poisson's ratio (NPR) steel plate and Ultra High Performance Concrete (UHPC) slab connected via demountable high-strength bolt shear connectors. Eight demountable composite slab specimens were fabricated and tested under traditional four-point bending method. The effects of loading histories (positive and negative bending moment), types of steel plate (NPR steel plate and Q355 steel plate) and spacings of high-strength bolts (150 mm, 200 mm and 250 mm) on the flexural behavior of demountable composite slab, including failure mode, load-deflection curve, interface relative slip, crack width and sectional strain distribution, were evaluated. The results revealed that under positive bending moment, the failure mode of composite slabs employing NPR steel plate was distinct from that with Q355 steel plate, which exhibited that part of high-strength bolts was cut off, part of pre-embedded padded extension nuts was pulled out, and UHPC collapsed due to instantaneous instability and etc. Besides, under the same spacing of high-strength bolts, NPR steel plate availably delayed and restrained the relative slip between steel plate and UHPC plate, thus significantly enhanced the cooperative deformation capacity, flexural stiffness and load capacity for composite slabs further. While under negative bending moment, NPR steel plate effectively improved the flexural capacity and deformation characteristics of composite slabs, but it has no obvious effect on the initial flexural stiffness of composite slabs. Meanwhile, the excellent crack-width control ability for UHPC endowed composite members with better durability. Furthermore, according to the sectional strain distribution analysis, due to the negative Poisson's ratio effect and high yield strength of NPR steel plate, the tensile strain between NPR steel plate and UHPC layer held strain compatibility during the whole loading process, and the magnitude of upward movement for sectional plastic neutral axis could be ignored with the increase of positive bending moment.

• Journal of KSNVE
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• v.7 no.1
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• pp.43-53
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• 1997

This paper investigated the practical use for measuring the structural intensity (power flow per width of cross section) in a uniform semi-infinite beam in flexural vibration. The structural intensity is obtained as a vector at a measurement point, One-dimensional structural intensity can be obtained from 4-point cross spectral measurement, or 2-point measurement on the assumption of far field. The measurement errors due to finite difference approximation and phase mismatch of accelerometers are examined. For precise measurements, it would be better to make the value of k$\delta$(wave number x space between accelerometers) between 0.5 and 1.0. Formulation of the relation between bending waves in structures and structural intensity makes it possible to separate the wave components by which one can get a state of the vibration field. Experimental results are obtained from 2- and 4-point measurement performed at 200mm (near field) and 400mm (far field) apart from excitation point in random excitation. the results are compared with the theoretical values and measured values of input power spectrum in order to verify the accuracy of structural intensity method, 2-point method is suggested as the practical structural intensity method.

• Journal of the Microelectronics and Packaging Society
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• v.19 no.1
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• pp.55-60
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• 2012

In order to develop electroless-plated Nickel Phosphate (Ni-P) as a contact material for high efficient low-cost silicon solar cells, we evaluated the effect of ambient thermal annealing on the degradation behavior of interfacial adhesion energy between electroless-plated Ni-P and silicon solar cell wafers by applying 4-point bending test method. Measured interfacial adhesion energies decreased from 14.83 to 10.83 J/$m^2$ after annealing at 300 and $600^{\circ}C$, respectively. The X-ray photoelectron spectroscopy analysis suggested that the bonding interface was degraded by environmental residual oxygen, in which the oxidation inhibit the stable formation of Ni silicide phase between electroless-plated Ni-P and silicon interface.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.1740-1743
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• 2007

In this study, two types of fatigue tests were conducted. First, cyclic bending tests were performed using the micro-bending tester. A four-point bending test method was adopted, because it induces uniform stress fields within a loading span. Second, thermal fatigue tests were conducted using a pseudo power cycling machine which was newly developed for a realistic testing condition. The pseudo-power cycling method makes up for the weak points in a power cycling and a chamber cycling method. Two compositions of solder are tested in all test condition, one is lead-free solder (95.5Sn4.0Ag0.5Cu) and the other is eutectic lead-contained solder (63Sn37Pb). In the cyclic bending test, the solder that exhibits a good reliability can be reversed depending on the load conditions. The lead-contained solders have a longer fatigue life in the region where the applied load is high. On the contrary, the lead-free solder sustained more cyclic loads in the small load region. A similar trend was detected at the thermal cycling test. A three-dimensional finite element analysis model was constructed. A finite element analysis using ABAQUS was performed to extract the applied stress and strain in the solder joints. A constitutive model which includes both creep and plasticity was employed. Thermal fatigue was occurred due to the creep. And plastic deformation is main damage for bending failure. From the inelastic energy dissipation per cycle versus fatigue life curve, it can be found that the bending fatigue life is longer than the thermal fatigue life.

• Magazine of the Korean Society of Agricultural Engineers
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• v.24 no.3
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• pp.92-99
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• 1982

The objective of this study was to investigate the compressive and bending strength characteristics of epoxy resin mortar, which is still in an early stage of its use and study in Korea. The results obtained are summarized as follows; 1. The compressive strengths of epoxy resin mortar after 1 day, 2 days and 3 days were gained 87%, 91% and 95%, respectively, in view of that of mortar at the age of 7 days. This result showed that the initial compressive strength within 1 day was very high. 2. The highest compressive strength of epoxy resin mortar was 914 kg/cm2 at the point of having the mixing ratio of one to two. It reached up to 3.7 times that of the normal portland cement mortar at the age of 28 days. 3. The bending strengths of epoxy resin mortar after 1 day, 2 days and 3 days came up to 88%, 93% and 97%, respectively, in comparing that of mortar at the age of 7 days. It was expressed to be simielar to the tendency of compressive strength. 4. The highest bending strength of epoxy resin mortar was 384 kg/cm2 at mixing ratio of one to two. It came up to as much as 6.5 times in comparing with that of the normal portland cement mortar at the age of 28 days. Therefore, the epoxy resin mortar would be effective for promoting the bending strength of structural members. 5. The regression equation between compressive and bending strength was obtained as follows; oo~=0.391 oc+27.54 (r=0.99) And the estimated value of bending strength was corresponded to about 44 per cent in comparing with that of the compressive strength.

• Journal of Mechanical Science and Technology
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• v.20 no.7
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• pp.1002-1011
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• 2006

In this study, we describe the conventional hot pressing (CHP) of layered $Al-B_4C$ composites and their characterization. The matrix alloy Al-5 wt.%Cu was prepared from elemental powder mixtures. The metal and B4C powders were mixed to produce either $Al-Cu-10vol.%B_4C$ or $Al-Cu-30vol.%B_4C$ combinations. Then, these powder mixtures were stacked as layers in the hot pressing die to form a two-layered composite. Hot pressing was carried out under nitrogen atmosphere to produce $30\times40\times5mm$ specimens. Microstructural features and age hardening characteristics of composites were determined by specimens cut longitudinally. The flexural strength of both layered composites and their monolithic counterparts were investigated via three point bending tests. In the case of layered specimens of both $10vol.%B_4C$ and $30vol.%B_4C$ containing layers were loaded for three-point test. The results show that a homogeneous distribution of $B_4C$ particles in the matrix alloy which is free of pores, can be obtained by CHP method. The ageing behavior of the composites was found to be influenced by the reinforced materials, i.e. higher hardness values were reached in 8 hrs for the composites than that for the matrix alloy. Flexural strength test showed that two-layered composites exhibited improved damage tolerance depending on layer arrangement. Microstructural investigation of the fracture surfaces of the bending specimens was performed by means of scanning electron microscope (SEM). While layer with lower reinforcement content exhibited large plastic deformation under loading, the other with higher reinforcement content exhibited less plastic deformation.

• Composites Research
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• v.12 no.6
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• pp.53-64
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• 1999

Microstructural morphology and bending strengths of moulded composites of thermotropic liquid crystalline polymer(LCP) and polyamide 6 (PA6) have been studied as a function of epoxy fraction. Injection-moulding of a composite plaque at a temperature below the melting point of the LCP fibrils generated a multi-layered structure: the surface skin layer with thickness of $65\;-\;120{\mu\textrm{m}}$ exhibiting a transverse orientation; the sub-skin layer with an orientation in the flow direction; the core layer with arc-curved flow patterns. The plaques containing epoxy 4.8vol% exhibited superior bending strength and large fracture strain. With an increase of epoxy fraction equal to and beyond 4.8vol%, geometry of LCP domains was changed from fibrillar shape to lamella-like one, which caused a shear-mode fracture. An analysis of the bending strength of the composite plaques by using a symmetric layered model beam suggested that addition of epoxy component altered not only the microstructural geometry but also the elastic moduli and strengths of the respective layers.