• Title/Summary/Keyword: 3D FE

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Protective Effect of Plantago asiatica L. Extract Against Ferric Nitrilotriacetate (Fe-NTA) Induced Renal Oxidative Stress in Wistar Rats (차전초 추출물을 투여한 랫드에서의 Fe-NTA 유발 산화스트레스에 대한 신장보호 효과)

  • Hong, Chung-Oui;Hong, Seung-Teak;Koo, Yun-Chang;Yang, Sung-Yong;Lee, Ji-Young;Lee, Yanhouy;Ha, Young-Min;Lee, Kwang-Won
    • Journal of Food Hygiene and Safety
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    • v.26 no.2
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    • pp.107-113
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    • 2011
  • Plantago asiatica L. (PA), which is widely distributed in Korea, Japan and China, has traditionally been used as a popular folk medicine for the treatment of liver diseases. A variety of activities of PA was reported, that is hepatoprotective, anti-inflammatory, anti-glycation and anti-oxidant effect. Ferric nitrilotriacetate (Fe-NTA) is a potent nephrotoxic agent and has been reported to induce renal proximal tubular necrosis. In the present study, pre-treatment with PA extract (PAE) in Wistar rat followed by Fe-NTA i.p. treatment (13.5 mg Fe/kg body weight) was performed to detect the renal protective effect of PAE. Only Fe-NTA treated group showed increases in the level of serum blood urea nitrogen (BUN) and serum creatinine (Cr), and renal tissue malondialdehyde (MDA), product of lipid peroxidation. Moreover, the level of biomarkers indicate the antioxidants status, reduced glutathione (GSH), glutathione-S-transferase (GST) and glutathione reductase (GR) were decreased. However, PAE pre-treated group showed decreases in the levels of serum BUN, serum Cr and renal tissue MDA in concentration dependent manner and increases in the level of GSH, GST and GR. These results are significantly different (p < 0.05) to the other groups. Our data suggest that PAE may be used as an chemopreventive material against Fe-NTA-mediated renal oxidative stress.

Sample Pretreatment for the Determination of Metal Impurities in Silicon Wafer (실리콘 웨이퍼 중의 금속 불순물 분석을 위한 시료 전처리)

  • Chung, H.Y.;Kim, Y. H.;Yoo, H.D.;Lee, S.H.
    • Journal of the Korean Chemical Society
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    • v.43 no.4
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    • pp.412-417
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    • 1999
  • The analytical results obtained by microwave digestion and acid digestion methods for sample pretreatment to determine metal impurities in silicon wafer by inductively coupled plasma-mass spectrometry (ICP-MS) were compared. In order to decompose the silicon wafer, a mixed solution of $HNO_3$ and HF was added to the sample and the metal elements were determined after removing the silicon matrix by evaporating silicon in the form of Si-F. The recovery percentages of Ni,Cr and Fe were found to be 95∼106% for both microwave digestion and acid digestion methods. The recovery percentage of Cu obtained by the acid digestion method was higher than that obtained by the microwave digestion method. For Zn, however, the microwave digestion method gave better result than the acid digestion method. Fe was added to a silicon wafer using a spin coater. The concentration of Fe in this sample was determined by lCP-MS, and the same results were obtained in the two pretreatment methods.

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Electric and Magnetic Properties of Hetero-Epitaxially Deposited BiFeO3 Thin Films (이종에피에 의해 증착한 BiFeO3 박막의 전기 및 자기특성)

  • Lee Eun Gu;Viehland D.
    • Korean Journal of Materials Research
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    • v.14 no.10
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    • pp.707-712
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    • 2004
  • $BiFeO_3$ films grown on (111) $SrTiO_3$ substrate have a rhombohedral structure, identical to that of single crystals. On the other hand, films grown on (110) or (001) $SrTiO_3$ substrate are monoclinically distorted from the rhombohedral structure due to the epitaxial constraint. The easy axis of spontaneous polarization is close to [111] for the variously oriented films. Dramatically enhanced polarization and magnetization have been found for hetero-epitaxially grown $BiFeO_3$ thin films comparing to that of $BiFeO_3$ crystals. The results are explained in terms of an epitaxially-induced transition between cycloidal and homogeneous spin states, via magneto-electric interactions.

Efficient FE-Analysis Method with Equivalent Models for Metallic Sandwich Plates with Inner Dimpled Shell Subject to 3-Point Bending (등가 모델을 이용한 3점 굽힘 하중을 받는 딤플형 금속 샌드위치판재의 효율적 해석)

  • Seong D. Y.;Jung C. G.;Yoon S. J.;Yang D. Y.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.130-133
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    • 2005
  • Efficient finite element method has been introduced for metallic sandwich plates subject to 3-point bending. A full model 3-point bending FE-analysis shows that plastic behavior of inner structures appears only at the load point. So, Unit structures of sandwich plates are defined to numerically calculate the bending stiffness with recurrent boundary condition of pure bending. And then equivalent models with same bending stiffness and strength of full models are designed analytically. It is demonstrated that results of both models are almost same and FE analysis method with equivalent models can reduce analysis time effectively.

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Warpage Simulation by the CTE mismatch in Blanket Structured Wafer Level 3D packaging

  • Kim, Seong Keol;Jang, Chong-Min;Hwang, Jung-Min;Park, Man-Chul
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.1
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    • pp.168-172
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    • 2013
  • In 3D wafer-stacking technology, one of the major issues is wafer warpage. Especially, The important reason of warpage has been known due to CTE(Coefficient of Thermal Expansion) mismatch between materials. It was too hard to choose how to make the FE model for blanket structured wafer level 3D packaging, because the thickness of each layer in wafer level 3D packaging was too small (micro meter or nano meter scale) comparing with diameter of wafer (6 or 8 inches). In this study, the FE model using the shell element was selected and simulated by the ANSYS WorkBench to investigate effects of the CTE on the warpage. To verify the FE model, it was compared by experimental results.

Microstructure and Mechanical Properties of CoCrFeMnNi-type High-entropy Alloy Fabricated by Selective Laser Melting: A Review (선택적 레이저 용융법으로 제조된 CoCrFeMnNi계 고엔트로피합금의 미세조직 및 기계적 물성 연구 동향)

  • Park, Jeong Min
    • Journal of Powder Materials
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    • v.29 no.2
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    • pp.132-151
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    • 2022
  • The CoCrFeMnNi high-entropy alloy (HEA), which is the most widely known HEA with a single face-centered cubic structure, has attracted significant academic attention over the past decade owing to its outstanding multifunctional performance. Recent studies have suggested that CoCrFeMnNi-type HEAs exhibit excellent printability for selective laser melting (SLM) under a wide range of process conditions. Moreover, it has been suggested that SLM can not only provide great topological freedom of design but also exhibit excellent mechanical properties by overcoming the strength-ductility trade-off via producing a hierarchical heterogeneous microstructure. In this regard, the SLM-processed CoCrFeMnNi HEA has been extensively studied to comprehensively understand the mechanisms of microstructural evolution and resulting changes in mechanical properties. In this review, recent studies on CoCrFeMnNi-type HEAs produced using SLM are discussed with respect to process-induced microstructural evolution and the relationship between hierarchical heterogeneous microstructure and mechanical properties.

Compositional Change of MgO Barrier and Interface in CoFeB/MgO/CoFeB Tunnel Junction after Annealing

  • Bae, J.Y.;Lim, W.C.;Kim, H.J.;Kim, D.J.;Kim, K.W.;Kim, T.W.;Lee, T.D.
    • Journal of Magnetics
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    • v.11 no.1
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    • pp.25-29
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    • 2006
  • Recent experiments have demonstrated high TMR ratios in MTJs with the MgO barrier [1,2]. The CoFeB/MgO/CoFeB junctions showed better properties than the CoFe/MgO/CoFe junctions because the MgO layer had a good crystalline structure with (001) texture and smooth and sharp interface between CoFeB/MgO [3]. The amorphous CoFeB with 20 at%B starts the crystallization at $340^{\circ}C$ [4] and this crystallization of the CoFeB helps obtaining the high TMR ratio. In this work, the compositional changes in the MgO barrier and at the interface of CoFeB/MgO/CoFeB after the CoFeB crystallization were studied in annealed MTJs. XPS depth profiles were utilized. TEM analyses showed that the MgO barrier had (100) texture on CoFeB in the junctions. B in the bottom CoFeB layer diffused into the MgO barrier and B-oxide was formed at the interface of CoFeB/MgO/CoFeB after the CoFeB crystallization.

Study on the Effect of Gas Pressure on Bottle Wall Thickness in the Blow Molding Process (블로우 몰딩 공정에서 분사 압력이 성형 두께에 미치는 영향에 관한 연구)

  • Kim, Dong-Hwan;Seol, Sang-Seok
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.4
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    • pp.36-44
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    • 2020
  • This study analyzed the deformation behavior of the high density polyethylene (HDPE) bottle in the blow molding process. We carried out finite element (FE) simulations using ANSYS Polyflow. First, the axisymmetric model was executed by 2D FE-simulation to determine the change of bottle wall thickness during the molding process. Then, the square model of the bottle was executed by 3D FE-simulation to gauge the effects of gas pressure on the change of wall thickness. The experiment results showed that the FE-simulations were able to upgrade the quality of the HDPE bottle in the blow molding process. These results can be used as guidance in adjusting gas pressure, as well as be extended for further study to determine process parameters such as temperatures, forming velocity, parison shape, etc.

Fabrication and characteristics of La1-xSrxMO3(M = Fe, Co, Mn) formaldehyde gas sensors (La1-xSrxMO3(M = Fe, Co, Mn) 물질을 이용한 포름알데히드 가스센서의 제조와 특성)

  • Kim, H.J.;Choi, J.B.;Kim, S.D.;Yoo, K.S.
    • Journal of Sensor Science and Technology
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    • v.17 no.3
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    • pp.203-209
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    • 2008
  • Thick film formaldehyde (HCHO) gas sensors were fabricated by using $La_1_{-x}Sr_xMO_3$ (M= Fe, Co, Mn) ceramics. The powders of $La_1_{-x}Sr_xMO_3$ (M=Fe, Co, Mn) were synthesized by conventional solid-state reaction method. By using the $La_1_{-x}Sr_xMO_3$ (M=Fe, Co, Mn) paste, the thick-film formaldehyde sensors were prepared on the alumina substrate by silkscreen printing method. The experimental results revealed that $La_1_{-x}Sr_xMO_3$ (M= Fe, Co, Mn) ceramic powder has a perovskite structure and the thick-film sensor shows excellent gas-sensing characteristics to formaldehyde gas (sensitivity of $La_{0.8}Sr_{0.2}FeO_3$, S= 14.7 at operating temperature of $150^{\circ}C$ in 50 ppm HCHO ambient).

Oxychlorination of methane over FeOx/CeO2 catalysts

  • Kim, Jeongeun;Ryou, Youngseok;Hwang, Gyohyun;Bang, Jungup;Jung, Jongwook;Bang, Yongju;Kim, Do Heui
    • Korean Journal of Chemical Engineering
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    • v.35 no.11
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    • pp.2185-2190
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    • 2018
  • Methane activation through oxychlorination is in the spotlight due to the relatively mild reaction conditions at atmospheric pressure and in the temperature range of $450-550^{\circ}C$. Although $CeO_2$ is known to exhibit good activity for methane oxychlorination, significant amounts of by-products such as $CO_2$, CO and carbon deposits are produced during the reaction over $CeO_2$. We investigated the effect of iron in $FeO_x/CeO_2$ catalysts on methane oxychlorination. $FeO_x/CeO_2$ with 3 wt% iron shows the maximum yield at $510^{\circ}C$ with 23% conversion of methane and 65% selectivity of chloromethane. XRD and $H_2$ TPR results indicate that iron-cerium solid solution was formed, resulting in the production of more easily reduced cerium oxide and the suppression of catalysts sintering during the reaction. Furthermore, the selectivity of by-products decreased more significantly over $FeO_x/CeO_2$ than cerium oxide, which can be attributed to the facilitation of HCl oxidation arising from the enhanced reducibility of the former sample.