• Title/Summary/Keyword: 3D 합성

Search Result 1,546, Processing Time 0.024 seconds

Synthesis of a Nitrogen-rich Insensitive Energetic Material, DNAM(Dinitroammeline) (고질소 둔감에너지 물질인 DNAM(Dinitroammeline) 합성공정 개발)

  • Sul, Minjung;Kim, Minjun;Kim, Jinseuk;Kim, Seunghee
    • Journal of the Korean Society of Propulsion Engineers
    • /
    • v.20 no.1
    • /
    • pp.50-57
    • /
    • 2016
  • We studied the Lab-scale process for the development of DNAM in aspect of safety and overall efficiency. Melamine is used for starting material of process, DNAM was synthesized by oxidation and nitration reaction. In order to optimize the process parameters with the product in higher yield and purity, a systematic study with variation of different parameters like molar ratio of nitrating mixture, conditioning time and order of reactant was carried out. The optimized reaction conditions for the synthesis of DNAM were : conditioning time of $3{\pm}3.5$ hour and nitrating mixture in 1:1.4 molar ratio. In order to proceed a stable reaction, melamine was added with enough time to relieve reaction heat. From these reaction condition, DNAM could be obtained in a yield of more than 60%.

Syntheses and realization of Quaternary Galois Field Sum-Of-Product(QGFSOP) expressed 1-variable functions Permutational Literals (치환리터럴에 의한 Quaternary Galois Field Sum-Of-Product(QGFSOP)형 1-변수 함수의 합성과 실현)

  • Park, Dong-Young;Kim, Baek-Ki;Seong, Hyeun-Kyeong
    • Journal of Advanced Navigation Technology
    • /
    • v.14 no.5
    • /
    • pp.710-717
    • /
    • 2010
  • Even though there are 256 possible 1-qudit(1-variable quantum digit) functions in quaternary logic, the most useful functions are 4!=24 ones capable of representing in QGFSOP expressions by possible permuting of 0,1,2, and 3. In this paper, we propose a permutational literal(PL) representation and a QPL(Quaternary PL) gate which use the operands of a multiplicand A and an augend D in $Ax^C$+D(GF4) operation as a control variable of multi-cascaded PLs. And we also present new PL synthesis algorithms to synthesize QGFSOP expressed 24 (1-qudit) functions by applying three PL operators as ab(mutual permutation), + D(addition), and XA (multiplication). Finally architectures, circuits, and a CMOS implementation to realize proposed PL synthesis algorithms for $Ax^C$+D(GF4) functions are presented.

A Study on Kernel Size Variations in 1D Convolutional Layer for Single-Frame supervised Temporal Action Localization (단일 프레임 지도 시간적 행동 지역화에서 1D 합성곱 층의 커널 사이즈 변화 연구)

  • Hyejeong Jo;Huiwon Gwon;Sunhee Jo;Chanho Jung
    • Journal of IKEEE
    • /
    • v.28 no.2
    • /
    • pp.199-203
    • /
    • 2024
  • In this paper, we propose variations in the kernel size of 1D convolutional layers for single-frame supervised temporal action localization. Building upon the existing method, which utilizes two 1D convolutional layers with kernel sizes of 3 and 1, we introduce an approach that adjusts the kernel sizes of each 1D convolutional layer. To validate the efficiency of our proposed approach, we conducted comparative experiments using the THUMOS'14 dataset. Additionally, we use overall video classification accuracy, mAP (mean Average Precision), and Average mAP as performance metrics for evaluation. According to the experimental results, our proposed approach demonstrates higher accuracy in terms of mAP and Average mAP compared to the existing method. The method with variations in kernel size of 7 and 1 further demonstrates an 8.0% improvement in overall video classification accuracy.

Dimensional Stability of Poly(ethylene/propylene naphthalate) as a Flexible Substrate Application (유연 기판 소재로 응용을 위한 폴리(에틸렌/프로필렌 나프탈레이트)의 치수안정성 연구)

  • Kim, Jae-Hyun;Heo, Hye-Young;Jung, Tae-Houng;Han, Joon-Hee;Kang, Ho-Jong
    • Polymer(Korea)
    • /
    • v.33 no.4
    • /
    • pp.371-376
    • /
    • 2009
  • The 1,3-propane diol has been introduced as a co-monomer with ethylene glycol to polymerize the poly(ethylene/propylene naphthalate) in order to improve the dimensional stability of poly(ethylene naphthalate) for a possible flexible substrate material. Based on $^1H$-NMR results, it was found that poly (ethylene/propylene naphthalate) has been synthesised successfully. Introducing 1,3-propane diol resulted in the amorphous state in polyester as well as lowering of glass transition and thermal degradation temperature. Coexisting relatively longer propylene segment compared with ethylene in synthesized polyester caused less orientation behavior and reducing thermal expansion coefficient. This is a promising result for poly (ethylene/propylene naphthalate) to apply a flexible substrate.

Retro-synthesis of Analogues of Ginsenosides (역합성법에 의한 진세노사이드 유사체의 합성)

  • Chang, Eun-Ha;Je, Nam-Gyung;Im, Kwang-Sik
    • YAKHAK HOEJI
    • /
    • v.40 no.2
    • /
    • pp.163-169
    • /
    • 1996
  • Glycosidation of 20(S)-protopanaxadiol obtained by the alkaline hydrolysis of total ginsenosides with 2,3,4,6-tetra-O-acetyl-${\alpha$-D-glucopyranosyl bromide in the presence of $CdCO_3$ in benzene-dioxane gave a mixture of acetylated monoglucosides and diglucosides in a total yield of 68%. Under the same condenstion condition, 20-dehydroxyglucosides were formed by dehydration of 12-O-glucosides. The structures of produced glycosides were elucidated as 3-O-${\beta$-D-glucopyranosyl-20(S)-protopanaxadiol, 12-O-${\beta$-D-glucopyranosyl-dammar-20(22), 24-dien-$3{\beta},12{\beta}$-diol, 3,12-di-O-${\beta}$-D-glucopyranosyl-dammar-20(22), 24-dien-$3{\beta},\;12{\beta}$-diol, respectively.

  • PDF

Design of W Band Frequency Synthesizer Using Frequency Tripler (주파수 3체배기를 이용한 W 밴드 주파수 합성기 설계)

  • Cho, Hyung-Jun;Cui, Chenglin;Kim, Seong-Kyun;Kim, Byung-Sung
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
    • /
    • v.24 no.10
    • /
    • pp.971-978
    • /
    • 2013
  • This work presents a W band frequency synthesizer which is composed of 26 GHz VCO, Phase Locked Loop and frequency tripler using 65 nm RF CMOS process. Frequency tuning range of 26 GHz VCO covers the band from 22.8~26.8 GHz and final output frequency of the tripler is from 74 to 75.6 GHz. The fabricated frequency synthesizer consumes 75.6 mW and its phase noise is -75 dBc/Hz at 1 MHz offset, -101 dBc/Hz 10 MHz offset respectively.

A Study on the Synthesis of High-Purity ${\alpha}-Al_2O_3$ Ultra-Fine Powders by Wet Chemical Method (습식 합성법에 의한 고순도 ${\alpha}-Al_2O_3$ 미세분말의 합성 연구)

  • Jin-Ho Choy;Jong-Seok Yoo;Yang-Su Han;Joon Kim;Hyeon-Kook Lee;Hyuk-Nyun Kim
    • Journal of the Korean Chemical Society
    • /
    • v.35 no.3
    • /
    • pp.275-279
    • /
    • 1991
  • Ultra-fine alumina, ${\alpha}-Al_2O_3$, with ${\phi}$ = 0.1∼0.5 ${\mu}$m was obtained from pure ammonium aluminum sulfate(alum) as the thermal decomposition product. Pure alum(> 99.7%) could be prepared by the precepitation and the successive recrystallization in an acidic aqueous solution at pH = 1.5∼2.5, which was theoretically predicted by only considering the concentrations of hydroxide and carbonate for aluminum and sodium in the solution, and also experimentally confirmed as the optimum precepitation condition for alum without forming any impurities like aluminum hydroxide or sodium one.

  • PDF

Design and fabrication of SSPA module in X-band for Radar (X-대역 레이더용 SSPA 모듈 설계 및 제작)

  • Yang, Seong-Soo
    • The Journal of the Korea institute of electronic communication sciences
    • /
    • v.13 no.5
    • /
    • pp.943-948
    • /
    • 2018
  • In this paper, SSPA Module for X-band radar was designed and fabricated by using GaN MMIC. For the purpose of configuring the high power SSPA module, the drive steamers are composed of 2-layers of GaN MMIC with considering Gain Loss. In addition, the power divider and power combiner used a 4way approach by designing a 4-stage power amplifier. The power divider has a loss of -3.0dB or more, and the I/O has a loss of -0.2dB in the power combiner and the phase difference between the ports are good at $2^{\circ}$ on average. The fabricated SSPA module got the measurement results that satisfy a Gain 48dB, P(sat)=88.3W(49.46 dBm), PAE=30.3% or more efficiency in condition of frequency range 9~10GHz. The fabricated X-Band SSPA module can be applied in RF performance improvement for SSPA module whit improvement of power divider/combiner.

A study on 3-D shape measurement for the composition of human bust (인체흉상 합성을 위한 3차원 형상 측정에 관한 연구)

  • 안중근;강영준;최정표;유원재
    • Proceedings of the Korean Society of Precision Engineering Conference
    • /
    • 1997.10a
    • /
    • pp.220-223
    • /
    • 1997
  • Moire topography method is a well-known non-contacting 3-D measuement method. Recently, the automatic 3-D measurement by moire topography has been required since the method was frequently applied to the engineering and medical fields. 3-D measurement using projection moire topography is very attractive because of it's high measuring speed and high sensitivity. In this paper, using two-wavelength method of projection moire topography tested to measuring object with the 2x-ambiguity problem. Experimental results prove that the proposed scheme is capable of finding absolute fringe orders, so that the 2x-ambiguity problem can be effectively overcome so as to treat large step discontinuities in measured objects.

  • PDF

Synthesis and characterization of Y2O3 : Eu3+ red nano phosphor powders using RF thermal plasma (RF 열플라즈마를 이용한 Y2O3:Eu3+ 적색 나노 형광체 분말 합성)

  • Lee, Seung-Yong;Koo, Sang-Man;Hwang, Kwang-Taek;Kim, Jin-Ho;Han, Kyu-Sung
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.25 no.6
    • /
    • pp.272-279
    • /
    • 2015
  • $Y_2O_3:Eu^{3+}$ is an excellent red-emitting phosphor, which has been widely used for display devices due to highly luminescent property and chemical stability. In this study, $Y_2O_3:Eu^{3+}$ red phosphors were prepared using the solid state reaction and RF thermal plasma synthesis. The particle size of $Y_2O_3:Eu^{3+}$ phosphors obtained by the solid state reaction varied from 10 to $20{\mu}m$, and 30~100 nanometer sized $Y_2O_3:Eu^{3+}$ particles were obtained from a liquid form of raw material through RF thermal plasma synthesis without an additional heat treatment. Photoluminescence measurements of the obtained $Y_2O_3:Eu^{3+}$ particles showed a red emission peak at 611 nm ($^5D_0{\rightarrow}^7F_2$). PL intensity of red nano phosphors prepared by RF thermal plasma synthesis was comparable to that of red phosphors prepared by the solid state reaction, indicating that nano-sized $Y_2O_3:Eu^{3+}$ red phosphors could be successfully synthesized using one-step process of RF thermal plasma.