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Dielectric properties of the $Pb(Fe_{1/2}Nb_{1/2})O_3-Pb(Fe_{2/3}W_{1/3})O_3- Pb(Mg_{1/3}Nb_{2/3})O_3$ ceramics ($Pb(Fe_{1/2}Nb_{1/2})O_3-Pb(Fe_{2/3}W_{1/3})O_3- Pb(Mg_{1/3}Nb_{2/3})O_3$ 세라믹의 유전특성)

  • 박인길;류기원;이성갑;이영희
    • Electrical & Electronic Materials
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    • v.6 no.2
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    • pp.122-128
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    • 1993
  • 본 연구에서는 0.45Pb(Fe$_{1}$2/Nb$_{1}$2/)O$_{3}$- (0.55-xPb(Fe$_{2}$3/W$_{1}$3/)O$_{3}$ (x=0.20, 0.25, 0.30) 세라믹을 950~990[.deg.C]에서 2시간 유지시켜 일반소성법으로 제작하였다. 제작된 시편에 대해 적층 세라믹 캐패시터로의 응용가능성을 고찰하기 위해 조성비와 소결온도에 따른 구조적, 유전적 특성을 조사하였다. PMN의 첨가량이 증가할수록 결정립 크기는 감소하였으며 상전이 온도는 증가하였다. 소결밀도는 970[.deg.C]에서 소결된 0.45PFN-0.30PFW-0.25PMN 시편에서 7.86[g/cm$_{3}$]의 최대값을 나타내었다. 유전상수는 990[.deg.C]에서 소결된 0.45PFN-0.25PFW-0.30PMN 시편에서 20,751의 최대값을 나타내었으며 유전손실은 모든 조성에서 5[%]이상을 나타내었다.

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Electrical properties of sol-gel derived $ PbZrO_3$-$PbTiO_3$-$Pb(Ni_{1/3}Nb_{2/3})O_3$ thin film (Sol-Gel 법에 의한$ PbZrO_3$-$PbTiO_3$-$Pb(Ni_{1/3}Nb_{2/3})O_3$)

  • 임무열;구경완;한상옥
    • Electrical & Electronic Materials
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    • v.10 no.2
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    • pp.134-140
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    • 1997
  • PbTiO$_{3}$-PbZrO$_{3}$-Pb(Ni$_{1}$3/Nb $_{2}$3/O$_{3}$)(PZT-PNN) thin films were prepared from corresponding metal organics partially stabilized with diethanolamine by the sol-gel spin coating method. Each mol rates of PT:PZ:PNN solutions were #1(50:40:10), #2(50:30:20), #3(45:35:20) and #4(40:40:20), respectively. The spin-coated PZT-PNN films were sintered at the temperature from 500.deg. C to 600.deg. C for crystallization. The P-E hysteresis curve was drawn by Sawyer-Tower circuit with PZT-PNN film. The coercive field and the remanent polarization of #4(40:40:20 mol%) PZT-PNN film were 28.8 kV/cm and 18.3 .mu.C/cm$^{2}$, respectively. Their dielectric constants were shown between 128 and 1120, and became maximum value in MPB(40:40:20 mol%). The leakage currents of PZT-PNN films were about 9.4x 10$^{-8}$ A/cm$^{2}$, and the breakdown voltages were about 0.14 and 1.1 MV/cm. The Curie point of #3(45:35:20 mol%, sintered at 600.deg. C) film was 330.deg. C.

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Study on the Improvement of Strength for 12% Chromium Steel Rotor (12% Cr 로터강의 강도 개선에 관한 연구)

  • Jang, Yun-Seok;O, Se-Uk
    • Journal of Ocean Engineering and Technology
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    • v.3 no.2
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    • pp.125-137
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    • 1989
  • To check technical improvement in the soundness and strength of 12% Cr steel rotor, a 25 tons of rotor with 65 tons of ingot was made in real size and was cut to pieces to take test samples, and the various mechanical tests such as impact, tensile, creep, and fatigue were carried out. The strengths are compared with those of 1% Cr-Mo-V rotor of same size. Microstructures of the samples are examined and reviewed. The results can be summarized as follows. 1) Fracture appearance transition temperatures are 80.deg. C at the center part and 60.deg. C near surface of 12% Cr rotor, and 8.deg. C near surface of 1% Cr-Mo-V rotor. 2) Comparative rapid softening occurs at higher temperatures above 600.deg. C for 12% Cr steel and 550.deg. C for 1% Cr-Mo-V steel in tension tests. 3) Fatigue crack propagation rate of 12% Cr steel is almost same as that of 1% Cr-Mo-V steel at the same corresponding surface part of the rotors. The crack growth rate of center part of 12% Cr rotor is faster than near surface part of the rotor, and the crack growth rate at the load condition of R=0.04 is slower than that of the load condition of R=0.5 for both 12% Cr steel and 1% Cr-Mo-V steel. 4) Crack growth rate of radial direction near surface of 12% Cr rotor is faster than that of transverse direction at the same part because of the difference in residual stresses. 5) Both creep and fatigue strengths of 12% Cr steel are superior to those of 1% Cr-Mo-V steel and the difference is thought the effect of climb and glide controlled creep by solid solution of alloying elements and dispersion of carbides.

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Study on the Improvement of Strength for 12% Chromium Steel Rotor (12% Cr 로터강의 강도 개선에 관한 연구)

  • Jang, Yun-Seok;O, Se-Uk
    • Journal of Ocean Engineering and Technology
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    • v.3 no.2
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    • pp.625-625
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    • 1989
  • To check technical improvement in the soundness and strength of 12% Cr steel rotor, a 25 tons of rotor with 65 tons of ingot was made in real size and was cut to pieces to take test samples, and the various mechanical tests such as impact, tensile, creep, and fatigue were carried out. The strengths are compared with those of 1% Cr-Mo-V rotor of same size. Microstructures of the samples are examined and reviewed. The results can be summarized as follows. 1) Fracture appearance transition temperatures are 80.deg. C at the center part and 60.deg. C near surface of 12% Cr rotor, and 8.deg. C near surface of 1% Cr-Mo-V rotor. 2) Comparative rapid softening occurs at higher temperatures above 600.deg. C for 12% Cr steel and 550.deg. C for 1% Cr-Mo-V steel in tension tests. 3) Fatigue crack propagation rate of 12% Cr steel is almost same as that of 1% Cr-Mo-V steel at the same corresponding surface part of the rotors. The crack growth rate of center part of 12% Cr rotor is faster than near surface part of the rotor, and the crack growth rate at the load condition of R=0.04 is slower than that of the load condition of R=0.5 for both 12% Cr steel and 1% Cr-Mo-V steel. 4) Crack growth rate of radial direction near surface of 12% Cr rotor is faster than that of transverse direction at the same part because of the difference in residual stresses. 5) Both creep and fatigue strengths of 12% Cr steel are superior to those of 1% Cr-Mo-V steel and the difference is thought the effect of climb and glide controlled creep by solid solution of alloying elements and dispersion of carbides.

New candidates of 1 < z < 2 galaxy clusters in 13.6 $deg^2$ of ELAIS-N1/N2 fields with a new colour-colour selection technique

  • Hyun, Minhee;Im, Myungshin;Kim, Jae-Woo;Lee, Seong-Kook
    • The Bulletin of The Korean Astronomical Society
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    • v.38 no.2
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    • pp.50.2-50.2
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    • 2013
  • Galaxy clusters, the largest gravitationally bound systems, are an important means to place constraints on cosmological models. Moreover, they are excellent places to test galaxy evolution models in connection to the environments. To this day, massive clusters have been found unexpectedly at high redshfit (Kang & Im 2009, Durret et al. 2011, Tashikawa et al. 2012), and evolution of galaxies in cluster has not been fully understood. Finding galaxy cluster candidates at z > 1 in wide, deep imaging survey data will enable us to solve such issues of modern extragalactic astronomy. We report new candidates of galaxy clusters in the wide and deep survey fields, European Large Area ISO Survey North1(ELAIS-N1) and North2(ELAIS-N2) fields, covering sky area of $8.75deg^2$ and $4.85deg^2$ each. We also suggest a new useful colour-colour selection technique to separate 1 < z < 2 galaxies from low-z galaxies by combining multi-wavelength data from the UKIRT Infrared Deep Sky Survey Deep Extragalactic Survey (UKIDSS DXS, JK bands), Spitzer Wise-area InfraRed Extragalactic survey (SWIRE, Optical-Infrared bands), Canada France Hawaii Telescope (CFHT, z band) and Infrared Medium-deep Survey(IMS, J band).

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Microwave dielectric properties of the 0.15(B $a_0.95$S $r_ 0.05$)O-0.15S $m_2$ $O_3$-0.7TiO $_2$ ceramics (0.15(B $a_0.95$S $r_ 0.05$)O-0.15S $m_2$ $O_3$-0.7TiO $_2$ 세라믹스의 마이크로파 유전특성)

  • 박인길;정장호;배선기;이영희
    • Electrical & Electronic Materials
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    • v.8 no.2
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    • pp.224-228
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    • 1995
  • 0.15(B $a_{0.95}$ S $r_{0.05}$)O-0.15S $m_{2}$ $O_{3}$-0.7Ti $O_{2}$ ceramics were fabricated by the mixed-oxide method. Microwave dielectric properties were investigated with sintering conditions. Increasing the sintering temperature from 1300 to 1375[.deg. C], the sintered density was increased from 5.44 to 5.63[g/c $m^{3$]. Increasing the sintering temperature, dielectric constant and quality factor were increased and temperature coefficient of resonant frequency was independent of sintering temperature. In the specimen sintered at 1375[.deg. C], dielectric constant, quality factor and temperature coefficient of resonant frequency were 80.79, 2784(at 3[GHz]), +11.07[ppm/.deg. C], respectively..

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Study on the preparation of low loss Mn-Zn-Fe ferrite (저손실 Mn-Zn-Fe 페라이트의 제조에 관한 연구)

  • 문현욱;서강수;최희태;신용진
    • Electrical & Electronic Materials
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    • v.3 no.3
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    • pp.205-214
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    • 1990
  • 본 논문은 저손실 Mn-Zn-Fe 페라이트 제조에 관하여 연구한 것이다. Mn-Zn-Fe 페라이트는 16mol% Xno, 31mol% MnO 및 53mol% Fe$_{2}$O$_{3}$로 조성하였으며 0.1wt% $Na_{2}$SiO$_{3}$ 0.05wt% $Na_{2}$SiO$_{3}$ 0.1%wt% CaO 0.05% SiO$_{2}$ 및 0.05wt% SiO$_{2}$ 및 0.05wt% $Na_{2}$SiO$_{3}$ 0.1% CaO 0.05wt% $Al_{2}$O$_{3}$를 미량 첨가하였다. 그리고 하소와 분쇄과정을 거친 분말은 충진성을 높이기 위하여 과립화하였다. 소결 1250, 1300 및 1350.deg.C에서 이루어졌고, 평형 산소분압은 소오킹 시 PO$_{2}$는 6%부터 시작하여 점차 감소시켰으며 900.deg.C에서 순수한 질소 분위기로 냉각시켰다. 초투자율, 손실계수 및 고유저항 등의 자기적인 특성은 1300.deg.C에서 소결했을 경우의 것이 가장 우수하였다. 즉, 초투자율은 2*$10^{3}$~$10^{3}$의 높은 값을 얻을 수 있었으며 tan.delta./.mu.i값은 100KHz~ 400KHz의 고파수대에서 9*10$_{-6}$~21*10$_{-6}$이었으며 고유저항 값은 485~680 .OMEGA.-cm의 높은 값을 나타내어 중간주파수대의 자심재료에 적합한 페라이트임을 확인하였다.

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A study on the dielectric properties of the $Pb(Fe_{1/2}Nb_{1/2})O_3-Pb(Fe_{2/3}W_{1/3})O_3-Ba(Cu_{1/2}W_{1/2})O_3$ ceramics ($Pb(Fe_{1/2}Nb_{1/2})O_3-Pb(Fe_{2/3}W_{1/3})O_3-Ba(Cu_{1/2}W_{1/2})O_3$세라믹의 유전특성에 관한 연구)

  • 정장호;류기원;이영희
    • Electrical & Electronic Materials
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    • v.4 no.2
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    • pp.150-158
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    • 1991
  • 본 연구에서는 0.80Pb(F $e_{1}$2/N $b_{1}$2/) $O_{3}$-(0.20-x)Pb(F $e_{2}$3/ $W_{1}$3/) $O_{3-x}$Ba(C $u_{1}$2/ $W_{1}$2/) $O_{3}$ (x=0.01, 0.02, 0.03) 세라믹을 소결온도 및 시간을 각각 860~960[.deg.C], 2시간으로 하여 일반 소성법으로 제작하였다. 시편의 조성비와 소결온도에 따른 구조적, 유전적 특성을 조사하였으며 유전손실 특성의 개선을 위해 조성 0.80Pb(F $e_{1}$2/N $b_{1}$2/) $O_{3}$-0.18Pb (F $e_{2}$3/ $W_{1}$3/) $O_{3}$-0.02Ba(C $u_{1}$2/ $W_{1}$2/) $O_{3}$시편에 Mn $O_{2}$를 0~1.25[wt%]로 첨가한 후 유전특성의 변화를 관찰하였다. Mn $O_{2}$의 첨가량이 증가함에 따라 결정립의 크기와 유전상수는 점차 감소하였다. 소결밀도는 900[.deg.C]에서 소결시킨 시편의 경우 최대값을 나타내었다. Ba(C $u_{1}$2/ $W_{1}$2/) $O_{3}$의 양이 0.01에서 0.03[mol]로 증가함에 따라 상전이온도는 38[.deg.C]에서 2[.deg.C]로 감소하였다. 조성 0.80Pb(F $e_{1}$2/N $b_{1}$2/) $O_{3}$0.18Pb(F $e_{2}$3/ $W_{1}$3/) $O_{3}$-0.02Ba(C $u_{1}$2/ $W_{1}$2/) $O_{3}$에 Mn $O_{2}$가 0.25[wt%] 첨가된 시편의 20[.deg.C]에서의 유전상수는 16,700으로 최대값을 유전손실을 1.28[%]로 최소값을 나타내었다. 또한 모든 시편은 온도 및 주파수에 따라 유전상수가 완만하게 변화하는 유전이완 특성을 나타내었다.다.

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The Overexpression of Subtilisin Enzyme Using Mutations on Transition State Regulatory Proteins of AprE Promoter and Development of Bacillus subtilis Host System (AprE Promoter전이상태 조절인자 변이주를 이용한 공업적 효소의 과발현과 고초균 숙주계의 개발)

  • 류성호;박승환김병기
    • KSBB Journal
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    • v.11 no.1
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    • pp.8-14
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    • 1996
  • Bacillus subtillis strains with transition state regulator mutations and a spore mutation were developed for the overexpression of apsE and for the enhancement of expression level. Among the many regulator genes, degU and hpr were chosen as a representative positive and negative regulator for the aprE, respectively. Spo II G was used for the construction of asporogeneous strains. All the mutants were constructed from two protease-deleted strain DB104 and the apsE gene was transformed with an integration vector pMK101. DB104(deg$U^h$(32) $his^+$)::pMK101(Cm) and DB104($\Delta$her(Em))::pMKl01(Cm) show 7-fold and about 2-fold increase in aprE expression level, respectively. But the effect of transition state regulator mutation on the aprE expression was diminished when the integrated aprE gene was amplified by the high concentration of chloramphenicol, i. e. 30 $\mu\textrm{g}$/ml. DB104($\Delta$spoIIG(Pm) degUh(32) his+)::pMK101(Cm) and DB104($\Delta$spoIIG(Pm) $\Delta$hpr(Em))::pMK101 double mutant show 10-fold and 3-fold increase in aprE expression level, respectively. The results suggest that sporulation mutation and transition state regulator mutation have independent and additive effect on the aprE expression, and the same gene dosage effect on the transition state regulator mutation was also identified.

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Extursion of viscoplastic material (점소성재료의 압출)

  • Oh, Hung-Kuk
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.5 no.2
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    • pp.77-81
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    • 1981
  • 1200.deg.C-1300.deg.C 의 열간 단조작업에서의 강철은 스트레인 속도에 민감하고 그 기계적인 특성방정식은 .delta.=.delta.$_{0}$ .epsilon.$^{m}$ 이다. 이 연구는 열간압출시 필요고 하는 작용력을, 상계이론을 사용하여 해석하고 쟤료의 기계적 특성상수들을 대입하여, 계산한다. 이 결과를 실험치와 비교하고 압출각, 마찰계수, 스트레인 속도와 점성계수등의 일반적인 영향에 대해서도 토의하였다.특히 변형역내의 평균스트레인 속도에 의한 일정 항복용력을 사용하였을 경우에 대해서도 비교 검토되었다.