• Title/Summary/Keyword: 2D solid

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Efficient Isolation of Dihydrophaseic acid 3'-O-β-D-Glucopyranoside from Nelumbo nucifera Seeds Using High-performance Countercurrent Chromatography and Reverse-phased High-performance Liquid Chromatography

  • Rho, Taewoong;Yoon, Kee Dong
    • Natural Product Sciences
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    • v.24 no.4
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    • pp.288-292
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    • 2018
  • High-performance countercurrent chromatography (HPCCC) coupled with reversed-phase highperformance liquid chromatography (RP-HPLC) method was developed to isolate dihydrophaseic acid 3'-O-${\beta}$-D-glucopyranoside (DHPAG) from the extract of Nelumbo nucifera seeds. Enriched DHPAG sample (2.3 g) was separated by HPCCC using ethyl acetate/n-butanol/water system (6:4:10, v/v/v, normal-phase mode, flow rate: 4.0 mL/min) to give 23.1 mg of DHPAG with purity of 88.7%. Further preparative RP-HPLC experiment gave pure DHPAG (16.3 mg, purity > 98%). The current study demonstrates that utilization of CCC method maximizes the isolation efficiency compared with that of solid-based conventional column chromatography.

Physical Properties of PNN-PMN-PZT Doped with Zinc Oxide and CLBO for Ultrasonic Transducer

  • Yoo, Juhyun;Kim, Tahee;Lee, Eunsup;Choi, Nak-Gu;Jeong, Hoy-Seung
    • Transactions on Electrical and Electronic Materials
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    • v.18 no.6
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    • pp.334-337
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    • 2017
  • In this paper, to develop the ceramics with high $d_{33}$ and high $Q_m$ for ultrasonic transducer applications, $0.10Pb(Ni_{1/3}Nb_{2/3})O_3-0.07Pb(Mn_{1/3}Nb_{2/3})O_3-0.83Pb(Zr_{0.5}Ti_{0.5})_{0.83}O_3$ (PNN-PMN-PZT) ceramics were sintered at $940^{\circ}C$ using $CuO-Li_2CO_3-Bi_2O_3$ (CLBO) as a sintering aid by a traditional solid-state technique. The influence of zinc oxide additive on the physical properties of the prepared ceramics were systematically investigated. The R-T (rhombohedral-tetragonal) phase coexistence was found in the ceramics without zinc oxide additive and with increasing amounts of ZnO additive, the specimens showed a tetragonal phase. The formation of a liquid phase between ZnO and $Bi_2O_3$ contributed significantly to the grain growth of specimens. For the 0.1 wt% ZnO ceramics, the optimal physical properties of $d_{33}=370pC/N$, ${\varepsilon}_r=1,344$, $k_p=0.621$, and $Q_m=1,523$ were obtained.

AP224 based Feature Translation from 3D CAD through STEP Part111 (3차원 CAD에서 STEP Part111을 통한 AP224 특징형상 데이터 번역)

  • Kim, J.H.
    • Korean Journal of Computational Design and Engineering
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    • v.11 no.4
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    • pp.303-314
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    • 2006
  • The exchange of CAD (Computer Aided Design) models between different CAD systems and to downstream applications such as manufacturing has become very important to modem industry. One serious current issue is that the process cannot automatically import existing 3-D solid models in a variety of commercial CAD formats into the process without manually re-mastering the model in current standard including "SIEP AP(Application Protocol) 203 Edition 1" To fully integrate technical data from the design agency to the shop floor, design intent and validated 3D geometry of feature based parametric CAD model should be brought into the standardized processes. To overcome this limitation, AP203 Edition 2 (Ed.2) and its related STEP parts such as Part55, Part108, Part109, Part111 and Part112 are starting to be available to handle this problem. The features in Part111 are harmonized with the machining features available in AP224. This paper is focused on two mapping technologies: CAD to Part111 mapping and Pat111 to AP224 mapping including case studios and it will provide the guideline about what should be done next in the AP203 Ed.2 to AP224 mapping. The final goal of this project is to integrate technical data from CAD to AP224 based manufacturing information through AP203 Ed.2.

Effect of Photo Initiator Content and Light Exposure Time on the Fabrication of Al2O3 Ceramic by DLP-3D Printing Method (광개시제 함량과 노광 시간이 DLP기반 알루미나 3D 프린팅 공정에 미치는 영향)

  • Kim, Kyung Min;Jeong, Hyeondeok;Han, Yoon Soo;Baek, Su-Hyun;Kim, Young Do;Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.26 no.4
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    • pp.327-333
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    • 2019
  • In this study, a process is developed for 3D printing with alumina ($Al_2O_3$). First, a photocurable slurry made from nanoparticle $Al_2O_3$ powder is mixed with hexanediol diacrylate binder and phenylbis(2,4,6-trimethylbenzoyl) phosphine oxide photoinitiator. The optimum solid content of $Al_2O_3$ is determined by measuring the rheological properties of the slurry. Then, green bodies of $Al_2O_3$ with different photoinitiator contents and UV exposure times are fabricated with a digital light processing (DLP) 3D printer. The dimensional accuracy of the printed $Al_2O_3$ green bodies and the number of defects are evaluated by carefully measuring the samples and imaging them with a scanning electron microscope. The optimum photoinitiator content and exposure time are 0.5 wt% and 0.8 s, respectively. These results show that $Al_2O_3$ products of various sizes and shapes can be fabricated by DLP 3D printing.

Structure Determination of Syndecan-4 Transmembrane Domain using PISA Wheel Pattern and Molecular Dynamics simulation

  • Choi, Sung-Sub;Jeong, Ji-Ho;Kim, Ji-Sun;Kim, Yongae
    • Journal of the Korean Magnetic Resonance Society
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    • v.18 no.2
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    • pp.58-62
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    • 2014
  • Human transmembrane proteins (hTMPs) are closely related to transport, channel formation, signaling, cell to cell interaction, so they are the crucial target of modern medicinal drugs. In order to study the structure and function of these hTMPs, it is important to prepare reasonable amounts of proteins. However, their preparation is seriously difficult and time-consuming due to insufficient yields and low solubility of hTMPs. We tried to produce large amounts of Syndecan-4 transmembrane domain (Syd4-TM) that is related to the healing wounds and tumor for a long time. In this study, we performed the structure determination of Syd4-TM combining the Polarity Index at Slanted Angle (PISA) wheel pattern analysis based on $^{15}N-^1H$ 2D SAMPI-4 solid-state NMR of expressed Syd4-TM and Molecular Dynamics (MD) simulation using Discovery Studio 3.1.

A Study on Establishment of 3D Digital Restoration of Cheongju Townscape in the 1960s - Focused on the Simplified Modeling of Nammun-ro 2ga dong - (1960년대 청주 도심경관의 3차원 디지털 복원모델 구축에 관한 연구 - 남문로 2가동의 간략화 모델작성을 중심으로 -)

  • Kim, Tai-Young;Cho, Sang-Min;Son, In-Bin
    • Journal of the Regional Association of Architectural Institute of Korea
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    • v.21 no.6
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    • pp.31-40
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    • 2019
  • This study aims to establish Nammun-ro 2ga in Cheongju city in the 1960s as three-dimensional digital information data for the restoration of urban archetypes. For this purpose, referring to the existing restoration map and model of Cheongju urban area in the 1960s, and the results of this study are as follows. Firstly, the buildings that can be generally classified are prepared through the modeling of parametric families. Secondly, the untypical models(combined and broken roofs, atypical and large scale buildings) of them are simply performed through solid modeling. And then, these simplified models are simulated through a sky view, a walking sight, and information analysis. Through this study, it will be possible to visualize and regenerate the low and dense area of Cheongju city in the 1960s.

A parametric investigation on seismic performance of ageing Sarıyar dam

  • Ahmad Yamin Rasa;Ahmet Budak
    • Structural Engineering and Mechanics
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    • v.91 no.2
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    • pp.123-133
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    • 2024
  • The assessment of seismic behavior and seismic performance of ageing Sarıyar concrete gravity dam constructed on Sakarya River in Türkiye is the main focus of this paper. For this purpose, the impact of sediment domain, ageing of concrete material under the impact of chemical and mechanical actions, and dam-water-sediment interaction are included in the two-dimensional (2D) finite element (FE) model developed in FORTRAN 90 environment. In the FE model, the dam and age dependent sediment domains are modeled by solid elements, while reservoir domain is modeled by Lagrangian fluid elements. The radiation of reflected waves to the unbounded water domain is modeled by infinite Lagrangian fluid elements, while unbounded sediment domain is modeled by infinite solid elements. The coupled system was assumed to be under the simultaneous impact of Vertical (V) and Horizontal (H) ingredients of 1976 Koyna earthquake and the coupled system was analyzed in Laplace domain by direct method. Due to the deterioration of the concrete, the H and V displacement responses together with the fundamental period of the body, elongate throughout the lifetime and this reduce the seismic safety of the dam. It was deduced that the ageing dam body will not experience major damages under the Koyna earthquake both at the earlier and later ages. Furthermore, at the heel of the dam, the hydrodynamic pressure responses are decreased by rising the sediment domain depth.

The Study of Nutrient Intakes of Formula-Fed Infants from Formula and Solids in Early Infancy (인공영양아의 에너지, 칼슘 및 철분 섭취에 관한 연구)

  • 배현숙
    • Journal of Nutrition and Health
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    • v.29 no.5
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    • pp.517-527
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    • 1996
  • The food consumption of 148 healthy infants from 4 to 6 months of age have been measured. Three groups were assigned to change of feeding pattern. Formula group(FF, n=102) were fed formula from birth till 6 months of age. Convert 1 group (C1F, n=14) and Convert 2 group (C2F, n=32) were fed breast milk and mixed milk at 2months of age afterthat switched to formula milk, respectively. All infants received solids (solid foods) from 4 months of age. No significant difference was found in the intake of nutrients among three feeding groups excluding carbohydrate intake of C1F-female at 4 months of age. No significant difference was found in the intake of nutrients among three feeding groups excluding carbohydrate intake of C1F-female at 4 months of age. The FF-female(70.9g/d) and C2F-female(66.9g/d) had significantly higher carbohydrate intake when compared to the C1F-female (54.3g/d). The average total energy intake at 4, 6 months were 648.3 and 709.7kcal/d among all infants. At 4 and 6 months of age, mean intake of nutrients was as follows. Calcium intake was 526.7mg/d and 760.0mg/d at 4 and 6 months of age respectively. Iron intake was 8.3mg/d and 10/5mg/d at 4 and 6 months of age respectively. Calories from solids provided 22.5% of total energy intake at 4 months of age, and nearly 32% at 6 months of age. The average energy and protein intakes of all infants were less than the RDA for calcium and iron at 4, 6 months of age.

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Mass production of potato shoots by liquid culture (액체배지를 이용한 조직배양 감자줄기의 대량증식)

  • Kim, Jae-Whune;Choi, Eun-Gyung;Kim, Jeong-Kook
    • Journal of Plant Biotechnology
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    • v.36 no.1
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    • pp.1-6
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    • 2009
  • A study was conducted to investigate in vitro micro propagation of four potato cultivars of Daese, Jasim, Chubaek and Haryeng in MS medium and PM medium (a medium containing half concentration of $NH_4NO_3$ and $KNO_3$, two fold concentration of $CaCl_2$ as compared to MS medium). During $1{\sim}2$ weeks of culture, Daese and Jasim showed better shoot elongation on the solid MS medium than Chubaek and Haryeng whereas Chubaek and Haryeng did better shoot elongation on the solid PM medium. But no difference was observed after 4 weeks of culture. As compared to shoot elongation on the solid medium, it was delayed at early stage of culture in the liquid medium without shaking. Shoot formation ratio of potato (above 4 cm of shoot length) began to increase significantly after 1 week of culture and kept on increasing until 4 weeks. The four cultivars showed the different patterns of shoot growth in bioreactor. The PM medium with a quarter salt strength was effective for the regeneration of axillary buds as well as shoot elongation of Jasim and Chubaek. Daese showed vigorous regeneration of axillary buds in the PM medium with a half salt strength. On the other hand, Haryeng showed slower growth than the other three cultivars.

Studies on Thermal Resistance of Selected Yeast Strain for Pasteurization of Solid Packed Peach (복숭아 Solid Pack 적정(適定) 살균조건(殺菌條件) 구명(究明)을 위(爲)한 선발(選拔) 효모(酵母)의 열저항성(熱抵抗性)에 관(關)한 연구(硏究))

  • Koo, Young-Jo;Lee, Dong-Sun;Shin, Dong-Hwa;Yu, Tae-Jong
    • Korean Journal of Food Science and Technology
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    • v.13 no.1
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    • pp.43-52
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    • 1981
  • A series of thermal destruction studies of the most heat resistant yeast strain No. 15 among 61 isolates were conducted in order to establish the optimum pasteurization condition of peach solid pack. The results obtained are summarized as follows: 1. A survival curve of the selected yeast strain No. 15 at $58^{\circ}C$ consisted of heat labile and heat stable fraction, showing broken curve. 2. The actively growing cell showed less recovery rate than 10 day rested cell after agitation-growing for 90 hr. For heating menstrua, peptone solution gave higher recovery rate than peach juice. For recovery medium, YM agar gave higher recovery rate than peach juice agar. The selected yeast was more resistant to heat at pH 4.0 than at pH 3.5 in both heating menstrua and recovery medium. 3. Z value of TDT curve of the selected yeast (heating : at pH 3.5 in peach juice. recovery: at pH 3.5 in peach juice agar) was $4.8^{\circ}C$. 4. The selected yeast No. 15 was identified as Torulopsis candida. 5. In the inoculated pack test of 4 oz can, it was concluded that the optimum P.U. 70/5 was 168 (center temp; $78.5^{\circ}C$, initial temp; $18^{\circ}C$, processing time; 18 min, initial yeast count; $1.0{\times}10^7$ per can).

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