• Bulletin of the Korean Chemical Society
• /
• v.10 no.1
• /
• pp.19-22
• /
• 1989

The suitability of BMPI (2-bromo-N-methyl pyridinium iodide) for solid-phase peptide synthesis was investigated. The coupling rate of BMPI/HOBT procedure. BMPI/HOBT was superior to DCC/HOBT couplings using the solid-phase peptide bond formation proceeded to a greater degree of completion than DCC/HOBT method did. Double couplings with 2 equiv. of Bocamino acids and 1.5 equiv. of BMPI and $NEt_3$ and 2 equiv. of HOBT in DMF/MC (1:1 v/v) gave the best result for the preparation of a model compound. Stepwise solid phase peptide synthesis using BMPI/HOBT procedure was successfully utilized for the preparation of $(D-Ala)^2$-dynorphine A. BMPI/HOBT procedure for the synthesis of $(D-Ala)^2$-dynorphine gave better yield (20%) than DCC/HOBT procedure did.

• Bulletin of the Korean Chemical Society
• /
• v.31 no.5
• /
• pp.1187-1191
• /
• 2010

$^1H-^{15}N$ heteronuclear dipolar coupling solid-state NMR experiments on lipid bilayer or bicelle samples are very useful for the structural studies of membrane proteins. However, to study these biological samples using solid-state NMR, a specific probe with high efficiency and high capability is required. In this paper, we describe the optimized design, construction, and efficiency of a 400 MHz wide-bore $^1H-^{15}N$ solid-state NMR probe with 5-mm solenoidal rf coil for high power, multi-pulse sequence experiments, such as 2D PISEMA or 2D SAMMY.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
• /
• v.18 no.4
• /
• pp.509-516
• /
• 2020

An important property of glass and ceramic solid waste forms is processability. Tellurite materials with low melting temperatures and high halite solubilities have potential as solid waste forms. Crystalline TiTe3O8 was synthesized through a solid-state reaction between stoichiometric amounts of TiO2 and TeO2 powder. The resultant TiTe3O8 crystal had a three-dimensional (3D) structure consisting of TiO6 octahedra and asymmetric TeO4 seesaw moiety groups. The melting temperature of the TiTe3O8 powder was 820℃, and the constituent TeO2 began to evaporate selectively from TiTe3O8 above around 840℃. The leaching rate, as determined using the modified American Society of Testing and Materials static leach test method, of Ti in the TiTe3O8 crystal was less than the order of 10-4 g·m-2·d-1 at 90℃ for durations of 14 d over a pH range of 2-12. The chemical durability of the TiTe3O8 crystal, even under highly acidic and alkaline conditions, was comparable to that of other well-known Ti-based solid waste forms.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2005.10a
• /
• pp.322-325
• /
• 2005

The shrinking critical dimensions of modern technology place a heavy requirement on optimizing feature shapes at the micro- and nano scale. In addition, the use of ion beams in the nano-scale world is greatly increased by technology development. Especially, Focused ion Beam (FIB) has a great potential to fabricate the device in nano-scale. Nevertheless, FIB has several limitations, surface swelling in low ion dose regime, precipitation of incident ions, and the re-deposition effect due to the sputtered atoms. In recent years, many approaches and research results show that the re-deposition effect is the most outstanding effect to overcome or reduce in fabrication of micro and nano devices. A 2D string based simulation software AMADEUS-2D $(\underline{A}dvanced\;\underline{M}odeling\;and\;\underline{D}esign\;\underline{E}nvironment\;for\;\underline{S}putter\;Processes)$ for ion milling and FIB direct fabrication has been developed. It is capable of simulating ion beam sputtering and re-deposition. In this paper, the 2D FIB simulation is demonstrated and the characteristics of ion beam induced direct fabrication is analyzed according to various parameters. Several examples, single pixel, multi scan box region, and re-deposited sidewall formation, are given.

• Korean Journal of Human Ecology
• /
• v.21 no.3
• /
• pp.539-550
• /
• 2012

In-depth knowledge of fabric microstructure is essential for understanding clothing comfort since it plays a significant role in heat and mass transfer between the human body and clothing. In this study, a novel method was employed for investigating 3D surfaces and solid construction characteristics of specific fabrics by using a reverse engineering technique. The surface construction data were obtained by a confocal laser scanning microscope and then manipulated by a 3D analysis program. Triangle mesh was used for connecting each 3D point, with clouds and fabric surface characteristics created by rendering techniques. For generating a 3D solid model, determinants of radius of curvature was used. According to the proposed method, actual surface expression of the real fabric was achieved successfully. The results from this methodology can be applied to the detailed analysis of clothing comfort that is highly influenced by the microstructure of the fabric.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2009.10a
• /
• pp.1371-1374
• /
• 2009

According to depth cues of an image, the optical engine of the solid volumetric true 3D display can project a sequence of slices of a 2D image to corresponding display at a set of liquid shutters (LC) locating at different depth. A single DLP optical engine developed for a solid volumetric true 3D display consists of a lamp, reflector, color wheel, hollow integrator, relays, DMD, and projection lens. The simulation results show that the optical engine designed for single DLP volumetric true 3D display satisfies the requirements.

• Journal of the Korean Institute of Telematics and Electronics S
• /
• v.35S no.2
• /
• pp.79-88
• /
• 1998

We developed a method for the solid angle estimation of acetabular coverage of the femoral head in 3D space. The superior half of the femoral head is modeled as part of a sphere. And the tangent lines connecting from a set of points of the acetabular outline to the center of the fitted sphere are obtained. The lines passthrough the unit sphere whose center is the same as that of the femoral head. The interesecting points form a boundary on the unit sphere. With the points on the unit sphere, we calculate the covered area of the femoral headand estimate the solid angle. Solid angle is defined asthe suface area within the boundary on the unit sphere. In this measurements, the solid angle of normal subjects is on an average 4.3(rad) and the corresponding acetabular coverage is 68%. Unlinke the conventional methods, this solid angle estimation shows real 3D acetabular coverage.

• Progress in Superconductivity and Cryogenics
• /
• v.21 no.3
• /
• pp.47-50
• /
• 2019

The paper gives the results of the experiments with a model two-section REBCO solenoid cooled by either gaseous helium (GHe) or sub-cooled/solid nitrogen (SN2) in (50-77) K temperature range. The major cooling source was a single-stage cryocooler Sumitomo CH-110 with the cooling power of 175 W and 130 W at 77 K and 50 K respectively. The coil itself was not directly conduction cooled. We compare the time taken by both coolants to obtain the temperature of the magnet of about 50 K and the homogeneity of the temperature distribution within the cryostat. Test results for the coil operation in solid nitrogen together with the comparison of its critical properties in SN2 and GHe are also presented.

• Journal of the Korean Society for Precision Engineering
• /
• v.16 no.9
• /
• pp.25-34
• /
• 1999

In spite of the advance of 3D solid modeling technology, there are some distinct areas where 2D CAD S/W are still dominant, and more competent comparing with 3D CAD S/W. For example, in the manufacturing of 2D-shaped electrical parts, most related manufacturing tools have 2D geometric features by nature, and 3D solid models applied to these parts have substantial overheads. Nevertheless, most 2D CAD S/W have no topological inquiry services because they have no such information on their geometrical database inherently. Thus, it is needed to extract such information from 2D CAD database for developing more advanced application such as automated drafting/design S/W. In this paper, the extraction of topological information from 2D CAD has been performed in general way using concept of B-rep. A general extraction algorithm, data structure and meta file format for 2D topological object have been developed and successfully applied to the development of the automated lead frame die design system in Samsung Aerospace. it is also possible to provide a flexible, powerful topology-oriented functionality on any common 2D CAD S/W.

• 제어로봇시스템학회:학술대회논문집
• /
• 2002.10a
• /
• pp.91.1-91
• /
• 2002

1. Introduction Present study presents the basic concept of a Solid Freeform Fabrication System using a rapid prototyping procedure and optimal control for a transferring and accumulating system. And it developed a novel rapid prototyping process that can use ceramic or metal as well as polymer as a basic material. 2. Solid Freeform Fabrication System 2.1 Basic Theory A 3D CAD data of the model is converted to the 2D cross-section data of the slides. A ceramic or metal tape of thickness 0.5-1.5mm is cut by a laser beam with the cross-section data of the slide. A 3D model was obtained by transferring and accumulating the slides. The final product is manufactured by sin...