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Properties of Epoxy Adhesive Modified with Siloxane-imide (실록산 이미드로 개질된 변성 에폭시 수지의 물성)

  • Kim, W.;Gong, H.J.
    • Elastomers and Composites
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    • v.43 no.1
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    • pp.39-48
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    • 2008
  • Peel strength of epoxy adhesives can be increased by adding some amounts of XNBR. In this case, thermal resistance of the adhesive will be decreased by decrease of glass transition temperature of the adhesive. Epoxy resin modified with siloxane-imide was synthesized to improve thermal resistance and peel strength of the adhesive, after that the properties of modified epoxy resin were compared with the commercial epoxy resin. When 5% XNBR was added to 30% modified epoxy resin, this adhesive showed 0.42 N/mm of peel strength and $155^{\circ}C$ of glass transition temperature. These properties are enough compared to the required properties by the industry, i.e., 0.3 N/mm and $150^{\circ}C$, respectively. Weight loss of the modified epoxy resin by the treatment of nitric acid and 0.1N NaOH was reduced, but weight gain by the humid condition was increased by the presence of benzene ring and imide ring. 30% modified epoxy resin blended with 5% XNBR showed 220% improvement in tensile strength and elongation compared to the case of common epoxy resin. This is due to the flexibility of the siloxane in the modified epoxy resin.

A Study of Resistance of Fatigue Crack in Aluminum Alloy Plate Bonded with FRP (FRP 본딩한 알루미늄 판재의 피로균열 저항성에 관한 연구)

  • 윤한기;오세욱;박원조;허정원
    • Journal of Welding and Joining
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    • v.12 no.4
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    • pp.117-126
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    • 1994
  • APAL (Aramid Patched ALuminum alloy) was manufactured, which was a material that was consisting of a A12024-T3 aluminum alloy plate bonded to single-side of it with aramid/epoxy laminates. The aramid/epoxy laminates were bonded to it in condition of 1, 2 ply and fiber orientation of .+-.45, 0.deg./90.deg. Fatigue crack propagation tests were performed at stress ratio R-0.2, 0.5 with Al 2024-T3, APAL 45-1P, APAL 0/90-1P, APAL 45-2P, APAL 0/90-2P specimens to examine behavior of retardation in fatigue crack propagation. All the APAL specimens showed superior fatigue crack resistance. Number of cycle spended for crack to propagate from $a_{M}$=37 to $a_{M}$=65 mm in case of APAL 0/90-2P specimen was half that of Al 2024-T3 specimen. Fatigue crack propagation rate of APAL 0/90 specimens were retarded more compared to APAL 45 specimens and the amounts of retardation at R=0.5 were larger than that at R=0.2. It was found that the retardation in fatigue crack propagation was caused by intact fibers in the wake of crack.ack.

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The Effect of Moisture Content on the Compressive Properties of Korean Corn Kernel (함수율(含水率)이 옥수수립(粒)의 압축특성(壓縮特性)에 미치는 영향(影響))

  • Lee, Han Man;Kim, Soung Rai
    • Korean Journal of Agricultural Science
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    • v.13 no.1
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    • pp.113-122
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    • 1986
  • In order to promote mechanization of corn harvesting in Korea, this study was conducted to find out the effect of moisture content on compressive properties such as force, deformation, energy and modulus of stiffness to the bioyield and the rupture point for Korean corn kernel. In this study, the loading positions of corn were flat, edge, longitude and the moisture contents were about 13, 17, 21, 25% in wet basis. The compression test was carreied out with flat plate by use of dynamic straingage for three varieties of Korean corn under quasi-static force when the loading rate was 1.125mm/min. The results of this study are summarized as follows; 1. When the moisture content of corn ranged from 12.5 to 24.5 percent, at flat position, the bioyied force was in the range of 13.63-26.73 kg and the maximum compressive strength was in the range of 21.55-47.65kg. Their values were reached minimum at about 17% and maximum at about 21% moisture content. The bioyield force was in the range of 13.58-6.70kg at edge position and the maximum compressive strength which was 16.42 to 7.82kg at edge position was lower than that which was 18.55-9.05kg at longitudinal position. 2. Deformation of corn varied from 0.43 to 1.37 mm at bioyield point and from 0.70 to 2.66mm at rupture point between 12.5 to 24.5% moisture content. As the moisture content increased, deformation was increased. 3. The moduli of resilience and toughness of corn ranged from 2.60 to 8.57kg. mm and from 6.41 to 34.36kg. mm when the moisture content ranged from 12.5 to 24.5 percent, respectively. As the moisture content increased, the modulus of toughness was increased at edge position and decreased at longitudinal position. And their values were equal each other at 22-23% moisture content. 4. The modulus of stiffness was decreased with increase in the moisture content. Its values ranged from 32.07 to 5.86 kg/mm at edge position and from 42.12 to 18.68kg/mm at flat position, respectively. Also, the values of Suweon 19 were higher than those of Buyeo. 5. It was considered that the compressive properties of corn at flat position were more important on the design data for corn harvesting and processing machinery than those of edge or longitudinal position. Also, grinding energy would be minimized when a corn was processed between about 12.5 to 17% moisture content and corn damage would be reduced when a corn was handled between about 19 to 24% moisture content in wet basis.

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Real-time Internal Stress of Nickel Sulfamate Electroform (니켈쌀파메이트 전주층의 실시간 잔류응력)

  • Kim I.;Kang K.;Lee J.;Kwon S.C.;Kim M.;Lee J.Y.
    • Journal of Surface Science and Engineering
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    • v.38 no.1
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    • pp.14-20
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    • 2005
  • The control of internal stress is extremely important in electroforming because of the deliberately low adhesion between the electro form and the mandrel. Excessive tensile or compressive stress can cause distortion, separation problem, curling, peeling or separation of electroform prematurely from the mandrel, buckling and blistering. Nickel sulfamate bath has been widely used in electroforming because of its low internal stress and moderate hardness. In this study, real-time stress sensor has been used for stress control in chloride-free nickel sulfamate bath for 400 mm x 300 mm x 500 ㎛ nickel electroform. It was found that compressive stress found at low current density indicated the contamination of electrolyte, which is very useful in procuring buckling and peeling of electroform. No compressive stress is allowed for plate electroform. The real-time stress can also be used for accurate stress control of nickel electroform. The tensile stress was found to be increased slightly with increase in nickel electroform thickness, i.e., from initial 1.47 ksi to 2.02 ksi at 320 ㎛.

A Development of Small-diameter Composite Helical Spring for Reinforcement of Optical Fiber Jumper Cord (OJC) (광점퍼코드 (OJC) 보호용 미소 직경 복합재료 스프링 개발)

  • 윤영기;박성도;이연수;윤희석;이우일
    • Composites Research
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    • v.15 no.4
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    • pp.17-22
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    • 2002
  • Small diameter composite helical springs (CS) are developed using a hot plated mold for reinforcement of common optical fiber jumper cord (OJC). The outer diameters of the springs are about 2 ~ 3mm. These springs are inserted into the OJC to protect the damage of an optical fiber from the sudden lateral load. Two types of CS, Yarn type (Y-type) and Band type (B-type), are manufactured to compare the effectiveness for the damage protection. The experimental works were conducted to check the effect of the CS covered around OJC on the mechanical and optical properties. Experimental observations show a considerable effect on the flexural resistance, hence slowing down the deterioration of the optical power by the internal damage of the fiber. Obtained main results are as follows: (1) Y-type CS has better protection abilities to lateral loading than B-types. (2) Compared with bare OJC, CS-OJC has less power loss under the loading. (3) OJC covered with the composite coil spring has a possibility for a practical usage with full fruits.

Splice Length of GFRP Rebars Based on Flexural Tests of Unconfined RC Members (RC 부재 휨 실험에 의한 GFRP 보강근의 이음길이 제안)

  • Choi, Dong-Uk;Chun, Sung-Chul;Ha, Sang-Su
    • Journal of the Korea Concrete Institute
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    • v.21 no.1
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    • pp.65-74
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    • 2009
  • Glass fiber reinforced polymer (GFRP) bars are sometimes used when corrosion of conventional reinforcing steel bar is of concern. In this study, a total of 36 beams and one-way slabs reinforced using GFRP bars were tested in flexure. Four different GFRP bars of 13 mm diameter were used in the test program. In most test specimens, the GFRP bars were lap spliced at center. All beams and slabs were tested under 4-point loads so that the spliced region be subject to constant moment. Test variables were splice lengths, cover thicknesses, and bar spacings. No stirrups were used in the spliced region so that the tests result in conservative bond strengths. Average bond stresses that develop between GFRP bars and concrete were determined through nonlinear analysis of the cross-sections. An average bond stress prediction equation was derived utilizing two-variable linear regression. A splice length equation based on 5% fractile concept was then developed. As a result of this study, a rational equation with which design splice lengths of the GFRP bars can be determined, was proposed.

An Experimental Study on the Turbulent Flow of a 45$^{\circ}C$ Free Cross Jet (450自由衝突 噴射 의 亂流流動 에 관한 實驗的 硏究)

  • 노병준;김장권
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.8 no.5
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    • pp.442-449
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    • 1984
  • Turbulent jet flow has been studied in many ways; a plane jet, a rectangular jet, an annular jet, a round jet, a wall jet, a parallel jet, a valve jet, a cross jet, a slit jet and etc. In this report, a 45.deg. cross jet flow was tried by using two same dimensioned nozzels(dia..phi.20)which were set up at the exit of the subsonic wind tunnel. Each jet flows to the direction of 22.5.deg. to the axis of downstream of the mixed flow. The centerline of each jet meets at the distance of 217.3mm and their mixing flow could be imagined to develop beyond that distance, so the measurement was effectuated at X/X$_{0}$=1.2-1.5. The section of the mixed flow a elliptic circle which is formed by the 22.5.deg. inclined flows to the X direction. This experimental study aimed at the investigation of the turbulent mixing process of two jets; the mean velocities, the turbulent shear stresses, the correlation coefficients, and the momentum were respectively measured. The mean velocity distribution profiles of the down-stream component measured in the Y direction coincide well with the empirical equation of Gortler and those measured in the Z direction agree with the equation of H. Schlichting. Other mean velocities V over bar and W over bar components were randomly distributed. The higher values with same order of the intensity of turbulence were largely distributed at the central part of the flow. The momentum was decreased up to 70% by the shock losses and the development of intense turbulences, but it kept its value constantly beyond X/d=14. Two-channel hot-wire anemometer systems (model 1050 series), X-type hot-wire made of tungsten (dia. .phi.e.mu.m, long 3mm, model 0252 T5), a computer(model HP 9845B0, and a plotter (model HP 9872C) were used for the experiments and the analyses.s.

Mechanical Properties of Lightweight Foamed Concrete Using Polymer Foam Agent (고분자 기포제를 이용한 경량 기포 콘크리트의 역학적 특성 (II))

  • 박상순;송하원;변근주
    • Magazine of the Korea Concrete Institute
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    • v.9 no.1
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    • pp.173-181
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    • 1997
  • The objective of this study is to obtain the mechanical characteristics of prefoarmed lightweight foamed concrete using the polymer ham agent which has high lightness. flowability and strength. For this purpose, the prefoarmed lightweight foamed concrete which was developed to have flow value over 180mm. unit weight between 0.38t/$m^3$ and 0.64t/$m^3$, and compressive strength about 30kg/$cm^2$ was used. This paper presents extensive test data on Young's modulus. Poisson's ratio, stress-strain curve, the characteristics of strength of the foamed concrete and also presents the mechanical characteristics of the foamed concrete with different foam sizes. It is expected that this study provides an importance guide to design and manufacture lightweight foam concrete, so that it helps to expand its structural use.

Finite element analysis of stress distribution on supporting bone of cement retained implant by loading location (하중 위치에 따른 시멘트 유지형 임플란트 지지골의 유한요소법 응력 분석)

  • Kim, Kap-Jin
    • Journal of Technologic Dentistry
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    • v.38 no.3
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    • pp.143-149
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    • 2016
  • Purpose: The purpose of this study is to evaluate the effect of two different oblique mechanical loading to occlusal surfaces of cement retained implant on the stress distributions in surrounding bone, using 3-dimensional finite element method. Methods: A 3-dimensional finite element model of a cement retained implant composed of three unit implants, simplified ceramic crown and supporting bone was developed according to the design of ement retained implant for this study. two kinds of surface distributed oblique loads(100 N) are applied to following occlusal surfaces in the single crowns; 1) oblique load on 2 occlusal points(50N for each buccal cusp, 2 buccal cusps exist), 2) oblique load on 4 occlusal points(25N for each buccal and lingual cusp, 2 buccal and 2 lingual cusps exist) Results: The results of the comparison of the stress distributions on surrounding bone are as follows. In the condition of oblique load on 2 occlusal points, VMS was 741.3 Mpa in the M1(Ø$4.0{\times}13mm$) model and 251.2 Mpa in the M2(Ø$5.0{\times}13mm$) model. It means the stress on the supporting bone is decreased. The results of oblique load on 4 occlusal points are similar to this one. Conclusion: Increasing the diameter of the implant fixture is helpful to distribute the stress on the supporting bone. Also, to obtain the structural stability of the supporting bone, it is effective to distribute the load evenly on the occlusal surface of crown in producing single crown implant.

Characteristics of High Frequency Induction-Hardened Bearing Steel Produced by VIM (VIM에 의해 제조된 고주파 유도경화 베어링강의 특성에 관한 연구)

  • Choe, Byeong-Yeong;Jang, Jeong-Seok
    • Korean Journal of Materials Research
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    • v.8 no.12
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    • pp.1176-1181
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    • 1998
  • Characteristics of high frequency induction- hardened bearing steel have been investigated using 0.55wt.% C-1.68wt.% Mn specimens produced by vacuum induction melting (VIM). The K4 value in DIN 57602 of the specimens was assessed to be 6.41, high level of cleanliness. The specimens were high frequency induction-hardened to form heterogeneous submicron- lath martensite in the surface hardened layer with about 2.5mm in effective depth. Rolling contact fatigue tests were conducted in elasto-hydrodynamic lubricating conditions under a maximum Hertzian contact stress of$ 492kgmm^{-2}$ . It was found that microhardness in the subsurface, up to about $500\mu\textrm{m}$ in depth, below the raceway of rolling contact fatigued specimens was increased in comparison with that of induction-hardened layers. The depth of maximum microhardness- increased region was about $100\mu\textrm{m}$ from surface, showing white etching area. Crack initiation and propagation in the white etching area below the raceway of rolling contact fatigued specimens were observed.

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