• Title/Summary/Keyword: 100 nm

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Preparation of Nano-Sized ITO Powder from Waste ITO Target by Spray Pyrolysis Process (폐(廢) ITO 타겟으로부터 분무열분해(噴霧熱分解) 공정(工程)에 의한 ITO 나노 분말(粉末) 제조(製造))

  • Yu, Jae-Keun;Kang, Seong-Gu;Sohn, Jin-Gun
    • Resources Recycling
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    • v.16 no.1 s.75
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    • pp.28-36
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    • 2007
  • Nano-sized ITO powders with the average particle size below 50 nm were synthesized from complex acid solution dissolved the ITO target into hydrochloric acid by a spray pyrolysis process, and the influences of reaction factors as reaction temperature and concentration of raw material solution were investigated. As the reaction temperature increases from 800 to $1000^{\circ}C$, the average particle size of the ITO powder increases from 40 nm to 100 nm, the microstructure gradually becomes solid, individual particles independently appear with the shape of polygon, the particle size distribution becomes increasingly irregular, the XRD peak intensity gradually increases and the specific surface area decreases. As the concentration of the raw material solution increases from 50g/l to 400g/l, the average particle size of ITO powder gradually increases, yet the particle size distribution appears more irregular. When the concentration is at 50 g/l, the average particle size of ITO powder is below 30 nm and the particle size distribution appears comparatively uniform. Nevertheless, when the concentration reaches 400 g/l, which is close to e saturated concentration, the particle size distribution appears extremely irregular, and the particles with the size ranging from 20 nm to 100 nm coexist. Along with the concentration rise, the XRD peak intensity gradually increases, yet the specific surface area decreases.

Magnetic & Crystallographic Properties of Patterned Media Fabricated by Nanoimprint Lithography and Co-Pt Electroplating (나노임프린트 패터닝과 자성박막도금을 이용하여 제작한 패턴드미디어용 자기패턴의 자기적 및 결정구조특성에 관한 연구)

  • Lee, B.K.;Lee, D.H.;Lee, M.B.;Kim, H.S.;Cho, E.H.;Sohn, J.S.;Lee, C.H.;Jeong, G.H.;Suh, S.J.
    • Journal of the Korean Magnetics Society
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    • v.18 no.2
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    • pp.49-53
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    • 2008
  • Magnetic and crystallographic properties of patterned media fabricated by nanoimprint lithography and Co-Pt electroplating were studied. Thin films of Ru(20 nm)/Ta(5 nm)/$SiO_2$(100 nm) were deposited on Si(100) wafer and then 25 nm hole pattern was fabricated by nanoimprint lithography on substrate. The electroplated Co-Pt nano-dots have the diameter of 35 nm and the height of 27 nm. Magnetic dot patterns of Co-Pt alloy were created using electroplated Co-Pt alloy and then their properties were measured by MFM, SQUID, SEM, TEM and AFM. We observed single domain with perendicular anisotropy for each dot and achieved optimum coercivity of 2900 Oe. These results mean that patterned media fabricated by nanoimprint lithography and electroplating have good properties in view of extending superparamagnetic limit while satisfying the writability requirements with the present write heads.

High-performance 94 GHz MMIC Low Noise Amplifier using Metamorphic HEMTs (Metamorphic HEMT를 이용한 우수한 성능의 94 GHz MMIC 저잡음 증폭기)

  • Kim, Sung-Chan;An, Dan;Rhee, Jin-Koo
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.45 no.8
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    • pp.48-53
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    • 2008
  • In this paper, we developed the MMIC low noise amplifier using 100 nm metamorphic HEMTs technology in combination with coplanar circuit topology for 94 GHz applications. The $100nm\times60{\mu}m$ MHEMT devices for the MMIC LNA exhibited DC characteristics with a drain current density of 655 mA/mm, an extrinsic transconductance of 720 mS/mm. The current gain cutoff frequency $(f_T)$ and maximum oscillation frequency $(f_{max})$ were 195 GHz and 305 GHz, respectively. The realized MMIC LNA represented $S_{21}$ gain of 14.8 dB and noise figure of 4.6 dB at 94 GHz with an over-all chip size of $1.8mm\times1.48mm$.

Synthesis of Iron Nanopowder from FeCl3 Solution by Chemical Reduction Method for Recycling of Spent Neodymium Magnet (네오디뮴 폐자석 재활용을 위한 화학환원법을 이용한 철 나노 분말 제조)

  • Ha, Yonghwang;Gang, Ryun-Ji;Choi, Seung-Hoon;Yoon, Ho-Sung;Ahn, Jong-Gwan
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.12
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    • pp.6187-6195
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    • 2012
  • Recycling process of iron should be developed for efficient recovery of neodymium(Nd), rare metal, from acid-leaching solution of neodymium magnet. In this study, $FeCl_3$ solution as iron source was used for synthesis of iron nanoparticle with the condition of various factors, etc, reductant, surfactant. $Na_4O_7P_2$ and polyvinylpyrrolidone(PVP) as surfactants, $NaBH_4$ as reductant, and palladium chloride($PdCl_2$) as a nucleation seed were used. Iron powder was analyzed with instruments of XRD, SEM and PSA for measuring shape and size. Iron nanoparticles were made at the ratio of 1 : 5(Fe (III) : $NaBH_4$) after 30 min of reduction time. Size and shape of iron particles synthesized were round-form and 50 nm ~ 100 nm size. Zeta-potential of iron at the 100 mg/L of $Na_4O_7P_2$ was negative value, which is good for dispersion of metal particle. When $Na_4O_7P_2$(100 mg/L), PVP($FeCl_3$ : PVP = 1 : 4, w/w) and Pd($FeCl_3$ : $PdCl_2$ = 1 : 0.001, w/w) were used, iron nanoparticles which are round-shape, well-dispersed, near 100 nm-sized can be made.

Improvement in the Stabilities of White Organic Light Emitting Diodes Using a Partially Doped Emission Layer

  • Jeon, Hyeon-Sung;Oh, Hwan-Sool;Yoon, Seok-Beom
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.3
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    • pp.145-148
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    • 2010
  • White organic light emitting devices were fabricated to improve the stability through a structural change using the two peak emission method. The fabricated devices were composed of indium tin oxide (100 nm)/ $\alpha$-NPD (30 nm)/4,40-bis(2,20-diphenylvinyl)-1,10-biphenyl (DPVBi, d: variable)/DPVBi: Rubrene (40 nm)/2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline(5 nm)/ $Alq_3$(5 nm)/ Al (100 nm). A DPVBi for blue emissions was used as the host material in the emitters. The doping concentration of the Rubrene was fixed at 2.0% (by weight). The white emission with Commission Internationale De L'Eclairage coordinates of (0.3342, 0.3439) occurred at 14 V with a thickness d of 1 nm. It was insensitive to the drive voltage, and the devices had a maximum luminance of $211\;cd/cm^2$. At 19 V, the current density and maximum external quantum efficiency were $173\;mAcm^2$ and 0.478%, respectively.

Measurements of optical wavelength using an optical fiber retarder (광섬유 위상지연기를 이용한 광파장 측정)

  • 이현우;김용평
    • Korean Journal of Optics and Photonics
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    • v.12 no.1
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    • pp.5-9
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    • 2001
  • A wavemeter was realized using the phenomena that the phase lag between principal polarization states in an optical retarder is a function of wavelength. The change in the polarization state of the optical beam as it passes through the optical retarder is dependent on wavelength. The wavelength of the optical beam is determined by comparing the power difference between principal polarization states. A prototype wavemeter was successfully implemented using a polarization maintaining fiber with birefringence $3\times10^{-4}$ and length 100 mm as the optical retarder. The measurement resolution was 0.08 nm over a wavelength region of 1554.38 nm-1557.l9 nm, which agreed well with theoretically calculated results. In addition, the dependence of operating characteristics on temperature was analyzed theoretically and experimentally.mentally.

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White electroluminescent device by ZnS:Mn, Cu, Cl phosphors

  • Kim Jong-Su;Park Jae-Hong;Kim Gwang-Cheol;Gwon Ae-Gyeong;Park Hong-Lee
    • Proceedings of the Korean Society Of Semiconductor Equipment Technology
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    • 2006.05a
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    • pp.225-231
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    • 2006
  • .고상반응법 (solid state reaction)합성된 ZnS:Mn,Cu,Cl 형광체는 약 $20^{\sim}25{\mu}m$ 의 구형이고, Cubic/hexagonal 구조를 보였다. Electroluminescent device(ELD)는 실크 스크린된 형광층(ZnS:Mn,Cu,Cl)/유전체층 ($BaTiO_3$)으로 구성되었으며, 각층은 $30^{\sim}50{\mu}m,\;50^{\sim}60{\mu}m$ 정도로 도포 하였다. 100 V-400 Hz 의 구동조건에서, ELD 의 백색 발광은 450 nm, 480 nm 픽에서 각각 $Cl_s{\to}Cu^{+}\;_{Zn},\;Cl_s{\to}Cu^{2+}\;_{Zn}$ 전이에 의해 중첩된 청색, 녹색 밴드의 발광과, 580 nm 픽에서 Mn 의 $^{4}T_1{\to}^{6}A_1$ 전이에 의한 황색 밴드의 발광으로 이루어진다. Cu 농도의 증가에 따라 450 nm 의 발광 밴드의 휘도는 감소하며 580 nm 의 발광 밴드의 휘도가 증가하였고 발광 휘도가 향상되었다. 즉, 색온도가 높은 cold white(10000 K)에서 색온도가 낮은 Warm white(3000 K) 로 변한다. 이것은 450 nm 의 발광 밴드가 580 nm 의 발광 밴드에 흡수되는 에너지 전이 (Energy transfer) 현상에 기인한다. ZnS:Mn,Cu,Cl 의 Mn 1.5 wt %, Cu 2.5 wt.% 에서 최적 발광 휘도를 보이며, 100 V-400 Hz 에서 약 $12cd/cm^2$이였다.

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CHARACTERISTICS OF ORGANIC LIGHT-EMITTING DIODES FOR THE DEVICES WITH ELECTRON INJECTION LAYER (LIF AND $LI_2O$) (전자주입층(LiF와 $Li_2O$)을 사용한 유기 발광 소자의 특성)

  • Shin, Eun-Chul;An, Hui-Chul;Lee, Ho-Sik;Song, Min-Jong;Lee, Won-Jae;Han, Wone-Keun;Kim, Tae-Wan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.439-440
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    • 2007
  • To enhance the electron injection from the cathode of organic light-emitting diodes (OLEDs), We have studied characteristics of device that electron injection layer(EIL) is inserted between emissive layer and cathode. We fabricated bi-layer cathode $Li_2O$(x nm)/Al(100nm) and LiF(x nm)/Al(100nm) using LiF and $Li_2O$ as an electron injection layer. We analyzed the current efficiency, luminance efficiency, and external quantum efficiency of the device by varying the thickness of $Li_2O$ and LiF to be 0.5nm, 1nm, or 3nm. Using the EIL, we have obtained the efficiency of 7cd/A and the luminance of $20,000cd/m^2$. There is an improvement of efficiency by more than 3 times than the device without the $Li_2O$ layer.

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Crystal growth of nanosized α-Fe2O3 particles in frit (Frit에서의 나노사이즈 α-Fe2O3 입자의 결정 성장)

  • Hiroaki-Katsuki, Hiroaki-Katsuki;Choi, Eun-Kyoung;Lee, Won-Jun;Moon, Won-Jin;Kim, Ung-Soo;Hwang, Kwang-Taek;Cho, Woo-Seok
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.28 no.2
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    • pp.69-73
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    • 2018
  • Crystal growth of ${\alpha}-Fe_2O_3$ nanosized particles of 80~90 nm in size, which were hydrothermally prepared from 0.03 M $FeCl_3$ solution at $100^{\circ}C$, was investigated in Pb-containing and Pb-free frit. By heating ${\alpha}-Fe_2O_3$ nanosized particles in two frits at $800^{\circ}C$, the average diameter of particles in frits was increased to 200~210 nm and 150~160 nm, respectively, and the crystal growth due to the aggregation and sintering of several ${\alpha}-Fe_2O_3$ particles was observed. Formation ratios of larger particles over 100 nm in diameter were 54 % in Pb-free frit and 85 % in Pb-containing frit. After heating ${\alpha}-Fe_2O_3$ particles in frits at $800^{\circ}C$, 7~9 nm in average diameter of pores were formed in particles. Theses pores were derived from the porous structure of original ${\alpha}-Fe_2O_3$ particles and confined in particles during sintering.